laboratory Name: Eurofins Lancaster Laboratories, Inc KY Lab ID#: 90088 EPA Category State OBP DBP SEC KY Category DBP DBP DBP Other SEC Other IOC IOC Other Other IOC iOC lOC IOC Other Other Other Analyte Code 1004 2920 2950 1927 1002 1074 1005 1010 1010 1075 1075 1015 1015 Request x x x x x x x x x x x x x x IOC Other Other Other Other Other Other 1017 1020 1020 SEC SEC IOC IOC IOC IOC IOC Other Other Other Other Other Other Other 1905 1905 1022 1022 1024 1025 1025 x x x x x SEC IOC Other 2905 1915 1028 1030 1031 x IOC IOC SEC IOC x x x x x Reference Method EPA300.0 KY Method Code SM5310C EPA524.2 SM 2320B EPA200.7 839 721 849 799 Certified EPA 200.8 797 Certified EPA200.8 Barium Barium Beryllium Beryllium Certified Certified Certified Certified EPA200.7 EPA200.8 EPA 200.7 797 799 Cadmium Cadmium Chloride Chromium (total) Chromium (total) Certified Certified Certified Certified Certified EPA200.8 EPA200.7 EPA200.8 EPA300.0 EPA200.8 EPA200.7 Color Color Copper Copper Cyanide (as free cyanide) Fluoride Fluoride Certified Certified Certified Certified Certified Certified Certified EPAll0.2 SM 2120B EPA200.7 EPA200.8 EPA 335.4 EPA300.0 SM4500F-C Foaming Agents Hardness (Total) SM 5540C Iron Lead Magnesium Certified Certified Certified Certified Certified Manganese Manganese Mercury (inorganic) Nickel Nickel Nitrate (as N) Certified Certified Certified Certified Certified Certified EPA 200.7 EPA 200.8 EPA 245.1 EPA200.7 Nitrate (as N) Nitrite (as N) Nitrite (as N) Nitrate · Nitrite pH pH Certified Certified Certified Certified Certified Certified Certified Certified EPA300.0 EPA 353.2 EPA353.2 EPA 150.l SM4500H+B EPA200.8 EPA 200.7 EPA200.7 EPA 300.0 SM 2550B Contaminant Bromide Total Organic Carbon (TOC) Total Trihalomethanes (TTHMs) Status Certified Certified Certified Alkalinity Aluminum Certified Certified Antimony Arsenic SEC IOC iOC Other Other Other Other SEC SEC IOC IOC IOC IOC IOC Other Other Other Other Other Other Other 1035 1036 1036 1040 1040 IOC IOC IOC Other Other Other 1041 1041 1038 SEC SEC IOC SEC Other Other x Other Other 1925 1925 1045 1050 State Other 1052 x Sodium SEC Other Other x x Sulfate SEC 1055 1996 Certified Certified Temperature Certified 1032 1032 x x x x x x x x x x x x x x x x Kentucky Drinking Water laboratory Certification - 2016 Selenium Silver SM 2340C EPA200.7 EPA 200.8 EPA 200.7 EPA200.8 EPA300.0 EPA353.2 720 797 799 797 799 797 720 797 799 957 829 799 797 716 720 807 MRL 0.25 0.5 0.1 0.7 0.0929 0.0003 0.00054 MRLUnits mg/L mg/L µg/L mg/L mg/L mg/L 0.0012 0.00092 0.0011 mg/L mg/L mg/L mg/L 0.000071 0.00064 0.00023 0.2 0.0007 0.002 mg/L mg/L mg/L mg/L mg/L mg/L 5 5 0.0032 0 .00040 0.005 0.05 0.03 cu cu 0.04 3.0 0.0333 mg/L mg/L mg/L mg/L mg/L mg/L 855 841 799 797 799 0.00013 0.0167 799 797 0.0012 0.00094 715 799 797 720 0.000056 0 .0025 0.00094 0.05 mg/L mg/L mg/L mg/L mg/L mg/L 709 720 709 709 734 0.04 0.05 0.015 0.04 mg/L mg/L mg/L mg/L N/A 0.01 0.0005 0.0018 0.167 SU SU mg/L mg/L mg/l 0.03 mg/L 0.01 ·c 835 797 799 799 720 830 mg/L mg/L mg/L mg/L 1 of3 .~ "IT\ 'C.. J) , . ,...., .. ,, .. Laboratory Name: Eurofins Lancaster Laboratories, Inc KY Lab ID#: 90088 EPA Category KY Category Other IOC Other SEC Analyte Code 1085 1930 M M Other Other 0100 SEC SEC Other 1095 Other oc oc oc oc oc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc soc voe voe voe voe voe voe voe voe voe 1095 2931 2110 2105 20Sl 20Sl 2047 State State State oc oc oc oc oc oc oc OC oc oc oc oc oc oc oc oc oc oc oc oc oc oc oc oc oc oc oc oc oc oc oc I 100 2044 2043 2050 2050 2306 2046 2031 203S 2039 2041 2063 200S 2946 2065 2067 2274 2042 2010 2015 2036 2326 2040 2037 2037 2981 2985 2977 2378 2968 2980 2983 2969 2990 Status Certified Certified Reference Method EPA200.8 SM 2540C KY Method Code 797 806 MRL 0.00015 10 MRLUnits mg/L mg/L Certified EPA 180.1 701 0.09 NTU Turbidity Zinc Certified Certified NTU mg/L Certified Certified Certified Certified Certified Certified Certified Certified Certified Certifi ed 831 799 797 719 703 703 707 711 710 710 710 707 0.14 Zinc l , 2-Dibromo-3-chloropropane (DBCP) 2,4,5·TP (Silvex) 2,4·0 Alachlor (Lasso) Alachlor (Lasso) Aldicarb Aldicarb Sulfone Aldicarb Sulfoxide SM 21308 EPA 200.7 EPA 200.8 EPA504.1 EPA 515.1 EPA515.l EPA507 EPA S25.2 EPA 531.1 EPA 531.1 EPA S31.1 EPA507 Certified Certified Certified Certified Certified Certified EPAS2S.2 EPA 525.2 EPA 531.1 EPA 515.1 EPA 52S.2 EPAS25.2 711 711 710 703 711 711 Certified EPAS15.l EPA 16138 EPA525.2 EPA S04.1 719 711 711 711 711 711 711 Contaminant Request x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x Kentucky Drinking Water Laboratory Certification - 2016 Thallium Total Dissolved Solids Turbidity Atrazine Atrazine Benzo(a)pyrene (PAHs) Carbofuran Dalapon Di(2-ethylhexyl) adipate Di{2-ethylhexyl) phthalate Dinoseb Dioxin (2,3,7,8-TCDD) Endrin Ethylene dibromlde Heptachlor Heptachlor epoxide Hexachlorobenzene Hexachlorocyclopentadlene Lindane Methoxychlor Oxamyl (Vydate) Pentachlorophenol Picloram Simazlne Slmazine 1,1,1-Trichloroethane 1,1,2·Trichloroethane 1,1- Dichloroethylene Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified EPA S2S.2 EPA 52S.2 EPA S2S.2 EPA S25.2 EPA 525.2 EPA 525.2 EPA 531.1 EPASlS.1 EPA S15.l Certified Certified Certified EPA 507 EPA 525.2 EPAS24.2 EPA 524.2 EPA 524.2 1,2.4-Trichlorobenzene 1,2·Dichlorobenzene (o-Dichlorobenzene) l ,2·Dichloroethane l ,2·Dichloropropane 1,4·Dichlorobenzene (p-Dichlorobenzene) Certified Certified Certified EPAS24.2 EPA S24.2 EPAS24.2 Certified Certified Benzene Certified EPA524.2 EPAS24.2 EPA524.2 0.0039 0.0074 0.01 0.1 0.15 0 .4 0.06 1.0 1.0 1.0 0.21 mg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L o.os µg/L 0.02 0.8 1.0 0.1 0.3 µg/L µg/L µg/L µg/L µg/L 703 0.2 µg/L 723 711 0.001 ng/L 0.2 0.01 µg/L µg/L 0.06 0 .1 0.05 0.05 0.06 0.04 710 703 703 707 711 721 721 721 721 721 721 721 721 721 1.0 µg/l µg/l µg/L µg/l µg/L µg/L µg/L 0.03 0.2 µg/L µg/l 0.2 0.07 0.1 0.1 0.1 µg/L µg/L µg/L µg/L µg/L 0.2 0.1 µg/L µg/L 0.1 0.1 0.1 0.1 µg/l µg/L µg/L µg/L 2 of3 Laboratory Name: Eurofins Lancaster Laboratories, Inc KY Lab ID It: 90088 EPA Category QC oc oc QC OC oc oc oc oc oc oc QC State State State KY Category voe voe voe voe voe voe voe voe voe voe voe voe State-SEC State- SEC State-SEC Analyte Code 2982 2989 Request 2991 2979 2984 2976 2955 1919 1044 x x x x x x x x x x x x x x 1064 x 2380 2964 2992 2996 2987 Contaminant Carbon tetrachloride Chlorobenzene cis-1,2-Dichloroethylene Dichloromethane (Methylene Chloride) Ethyl benzene Styrene Tetrachloroethylene (PCE) Toluene trans-1,2-Dichloroethylene Trichloroethylene (TCE) Vinyl chloride Xylenes (total) Calcium a-Phosphate Conductivity Reference Method EPA524.2 EPA524.2 EPA 524.2 EPA 524.2 EPA 524.2 EPA 524.2 EPA524.2 EPA 524.2 EPA524.2 EPA 524.2 EPA524.2 EPAS24.2 EPA 200.7 SM4500P E SM 2510 B Status Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Certified Kentucky Drinking Water Laboratory Certification - 2016 KY Method Code 721 721 721 721 721 721 721 721 721 721 721 721 799 861 845 MRL 0.1 0.1 0.1 0.3 0.1 0.1 0.1 0.1 0.1 0.1 0.1 .1 0.0347 0.03 1.7 MRLUnlts µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L µg/L mg/L mg/L mg/L 3 of3 -~ ·- .. --~• .•.-.,.•~.~-~~ C O-~:J:-Tf..1:-'-'J. ment Cabinet Has fulfilled the requirements governin~the Ceitification of Wastewater Laboratories and is h1 .. granted certification for the analytes and'q_ssoci~ methods listed on the annually updated tabl~ . .,;zs 1st dq.y of Jamtary, 2 This Certificate is valid until December 31, 201 Laboratory Name: Eurofins Lancaster Laboratories Environmental, LLC KY Lab ID#: 90088 KY Category Analyte CAS# Status Reference Method MDL Inorganic/Gen Chem N/A Acidity Certified SM 2310 B-1997 5 MRL 15 Inorganic/Gen Chem N/A 7664-41-7 Alkalinity Certified SM 2320 B-1997 0.7 2 mg/L Ammonia Certified EPA 350.1 R2 0.0678 0.2 mg/L Inorganic/Gen Chem Units Inorganic/Gen Chem N/A Biochemical Oxygen Demand (BODS) Certified SM 5210 B-2001 1.7 5.1 mg/L 7726-95-6 Certified EPA 300.0 Rev 2.1 0.25 0.5 mg/L Inorganic/Gen Chem N/A Bromide Carbonaceous Biochemical Oxygen Demand (CBODS) Certified SM 5210 B-2001 1.2 4 mg/L Inorganic/Gen Chem N/A Chemical Oxygen Demand Certified EPA410.4 12.8 50 mg/L Inorganic/Gen Chem 16887-00-6 Chloride Certified EPA 300.0 Rev 2.1 Inorganic/Gen Chem 18540-29-9 Chromium VI Certified SM 3500-Cr B-2009 Inorganic/Gen Chem 0.2 0.4 mg/L 0.015 0.05 mg/L 5 5 mg/L N/A Color Certified SM 2120 B-2001 Inorganic/Gen Chem N/A Cyanide - Available Certified SM 4500-CN-G 0.005 0.01 mg/L Inorganic/Gen Chem 57-12-5 Cyanide - Free Certified OIA-1677 0.0026 0.0077 mg/L Inorganic/Gen Chem 57-12-5 Cyanide - Total Certified EPA 335.4 0.005 0.01 mg/L Inorganic/Gen Chem 7782-41-4 Fluoride Certified EPA 300.0 Rev 2.1 0.09 0.2 mg/L Inorganic/Gen Chem N/A Hardness - Total Certified SM 2340 C-1997 3 10 mg/L Inorganic/Gen Chem Kjeldahl Nitorgen - Total (TKN) Certified EPA 351.2 Rev 2 0.5 1 mg/L Inorganic/Gen Chem N/A 14797-55-8 Nitrate (as N) Certified 0.1 1594-56-5 Nitrite (as N) Certified EPA 300.0 EPA 300.0 Rev 2.1 0.05 Inorganic/Gen Chem 0.05 0.1 mg/L mg/L mg/L Inorganic/Gen Chem N/A Oil and Grease Certified EPA 1664B 1.4 5 Inorganic/Gen Chem 98059-61-1 Ortho-phosphate Certified EPA 365.3 1.4 5 mg/L Inorganic/Gen Chem 7664-93-9 Sulfate Certified EPA 300.0 Rev 2.1 0.3 1 mg/L Inorganic/Gen Chem 9073-75-0 Sulfide Certified SM 4500-S2 D 2000 0.054 0.16 mg/L Inorganic/Gen Chem 80879-60-3 Sulfite Certified SM 4500-S03 B 1.5 5 mg/L Inorganic/Gen Chem N/A Surfactants Certified SM 5540 C-2000 0.04 0.12 mg/L Inorganic/Gen Chem 10052 Total Dissolved Solids Certified SM2540 C-1997 9.7 30 mg/L SM 2540 D-1997 1 3 mg/L Inorganic/Gen Chem 10050 Total Suspended Solids Certified Inorganic/Metals 7429-0-5 Aluminum Certified EPA 200. 7 Rev 4.4 0.0674 0.2 mg/L Inorganic/Metals 7429-0-5 Aluminum Certified EPA 200.8 Rev 5.4 8.17 100 ug/L Inorganic/Metals 7440-36-0 Antimony Certified EPA 200.7 Rev 4.4 0.0051 0.2 mg/L Inorganic/Metals 7440-36-0 Antimony Certified EPA 200.8 Rev S.4 0.33 1 ug/L Inorganic/Metals 7440-38-2 Arsenic Certified EPA 200.7 Rev 4.4 0.0072 0.02 mg/L Inorganic/Metals 7440-38-2 Arsenic Certified EPA 200.8 Rev 5.4 0.818 2 ug/L Inorganic/Metals 7440-39-3 Barium Certified EPA 200.7 Rev 4.4 0.00033 0.005 mg/L 7440-39-3 Barium Certified EPA 200.8 Rev 5.4 0.583 2 ug/L Inorganic/Metals 7440-41-7 Beryllium Certified EPA 200.7 Rev 4.4 0.00067 0.005 mg/L Inorganic/Metals 7440-41-7 Beryllium Certified EPA 200.8 Rev 5.4 0.045 0.5 ug/L Inorganic/Metals 7440-42-8 Boron Certified EPA 200.7 Rev4.4 0.0084 0.05 mg/L Kentucky Wastewater Laboratory Certification - 2016 Keo!Y~ Method Mod mg/l Inorganic/Gen Chem Inorganic/Metals ATP 1of6 Laboratory Name: Eurofins Lancaster laboratories Environmental, LLC KY Lab ID#: 90088 Method KY Category Inorganic/Metals CAS# 7440-42-8 Analyte Boron Status Reference Method MDL MRL Certified EPA 200.8 Rev 5.4 11 so ug/L mg/L Units Inorganic/Metals 7440-43-9 Cadmium Certified EPA 200.7 Rev 4.4 0.00033 0.005 Inorganic/Metals 7440-43-9 Cadmium Certified EPA 200.8 Rev 5.4 0.171 0.5 ug/L Inorganic/Metals 7440-70-2 Calcium Certified EPA 200. 7 Rev 4.4 0.0334 0.2 mg/L Certified EPA 200.8 Rev 5.4 69.7 200 ug/L Certified EPA 200. 7 Rev 4.4 0.0013 0.015 mg/L Inorganic/Metals 7440-70-2 Calcium Inorganic/Metals 7440-47-3 Chromium Inorganic/Metals 7440-47-3 Chromium Certified EPA 200.8 Rev 5.4 0.5 2 ug/l Inorganic/Metals 7440-48-4 Cobalt Certified EPA 200.7 Rev 4.4 0.0010 0.005 mg/L Inorganic/Metals 7440-48-4 Cobalt Certified EPA 200.8 Rev 5.4 0.102 0.5 ug/L Inorganic/Metals 7440-50-8 Copper Certified EPA 200. 7 Rev 4.4 0.0028 0.01 mg/L Inorganic/Metals 7440-50-8 Copper Certified EPA 200.8 Rev 5.4 0.501 2 ug/l Inorganic/Metals 7439-89-6 Iron Certified EPA 200.7 Rev 4.4 0.0334 0.2 mg/L Inorganic/Metals 7439-89-6 Iron Certified EPA 200.8 Rev 5.4 13.1 100 ug/L Inorganic/Metals 7439-92-1 Lead Certified EPA 200. 7 Rev 4.4 0.0047 0.015 mg/L Inorganic/Metals 7439-92-1 lead Certified EPA 200.8 Rev 5.4 0.0824 1 ug/L Inorganic/Metals 7439-95-4 Magnesium Certified EPA 200.7 Rev 4.4 0.0167 0.1 mg/L Inorganic/Metals 7439-95-4 Magnesium Certified EPA 200.8 Rev 5.4 6.96 100 ug/l Inorganic/Metals 7439-96-5 Manganese Certified EPA 200.7 Rev4.4 0.00083 0.005 mg/L Inorganic/Metals 7439-96-5 Manganese Certified EPA 200.8 Rev 5.4 0.548 2 ug/L Inorganic/Metals 7439-97-6 Mercury Certified EPA 245.1 Rev 3 0.00006 0.0002 mg/l Inorganic/Metals 7439-98-7 Molybdenum Certified EPA 200.7 Rev 4.4 0.0017 0.01 mg/L Inorganic/Metals 7439-98-7 Molybdenum Certified EPA 200.8 Rev 5.4 0.25 0.5 ug/l Inorganic/Metals 7440-02-0 Nickel Certified EPA 200.7 Rev 4.4 0.0016 0.01 mg/L Inorganic/Metals 7440-02-0 Nickel Certified EPA 200.8 Rev 5.4 0.791 2 ug/L Inorganic/Metals 7440-09-7 Potassium Certified EPA 200. 7 Rev 4.4 0.1330 0.5 mg/l ug/L Inorganic/Metals 9/7/7440 Potassium Certified EPA 200.8 Rev 5.4 41.2 200 Inorganic/Metals 7782-49-2 Selenium Certified EPA 200. 7 Rev 4.4 0.0048 0.02 mg/L Inorganic/Metals 7782-49-2 Selenium Certified EPA 200.8 Rev 5.4 0.5 2 ug/l mg/L Inorganic/Metals 7440-22-4 Silver Certified EPA 200.7 Rev 4.4 0.0018 0.005 Inorganic/Metals 7440-22-4 Silver Certified EPA 200.8 Rev 5.4 0.125 0.5 ug/L Inorganic/Metals 7440-23-5 Sodium Certified EPA 200. 7 Rev 4.4 0.167 1 mg/l Inorganic/Metals 7440-23-5 Sodium Certified EPA 200.8 Rev 5.4 50 200 ug/L Inorganic/Metals 7440-28-0 Thallium Certified EPA 200. 7 Rev 4.4 0.0051 0.03 mg/L Inorganic/Metals 7440-28-0 Thallium Certified EPA 200.8 Rev 5.4 0.15 0.5 ug/L Inorganic/Metals 7440-31-5 Tin Certified EPA 200. 7 Rev 4.4 0.0024 0.02 mg/l Inorganic/Metals 7440-31-5 Tin Certified EPA 200.8 Rev 5.4 0.515 2 ug/l Inorganic/Metals 7440-32-6 Titanium Certified EPA 200.7 Rev 4.4 0.0017 0.01 mg/L Inorganic/Metals 7440-32-6 Titanium Certified EPA 200.8 Rev 5.4 4.02 15 ug/L Kentucky Wastewater Laboratory Certification - 2016 /(_~~ ATP Mod 2 of 6 Laboratory Name: Eurofins Lancaster Laboratories Environmental, LLC KY Lab ID#: 90088 KV Category CAS# Analyte Status Inorganic/Metals 7440-62-2 Vanadium Certified Reference Method EPA 200.7 Rev4.4 Inorganic/Metals 7440-62-2 Vanadium Certified EPA 200.8 Rev 5.4 0.22 0.5 ug/L Inorganic/Metals 7440-66-6 Zinc Certified EPA 200.7 Rev4.4 0.0020 0.02 mg/L MDL 0.0019 MRL 0.005 Units Inorganic/Metals 7440-66-6 Zinc Certified EPA 200.8 Rev 5.4 2.44 15 ug/L N/A Coliform, fecal Certified SM 92220 10 10 per 100 ml ORG/Dioxins 67562-39-4 1,2,3,4,6, 7,8-Heptachloro-dibenzofuran Certified EPA 16138 4 10 pg/L ORG/Dioxins 35822-46-9 1,2,3,4,6,7,8-Heptachloro-dibenzo-p-dioxin Certified EPA 16138 4 10 pg/L ORG/Dioxins 55673-89-7 1,2,3,4,7,8,9-Heptachloro-dibenzofuran Certified EPA 16138 3 10 pg/L ORG/Dioxins 70648-26-9 1,2,3,4, 7,8-Hexachloro-dibenzofuran Certified EPA 16138 3 10 pg/L ORG/Dioxins 39227-28-6 1,2,3,4,7,8-Hexachloro-dibenzo-p-dioxin Certified EPA 16138 3 10 pg/L pg/L ORG/Dioxins 57117-44-9 1,2,3,6,7,8-Hexachloro-dibenzofuran Certified EPA 16138 3 10 ORG/Dioxins 57653-85-7 1,2,3,6,7,8-Hexachloro-dibenzo-p-dioxin Certified EPA 16138 3 10 pg/L ORG/Dioxins 72918-21-9 1,2,3, 7,8,9-Hexachloro-dibenzofuran Certified EPA 16138 4 10 pg/L ORG/Dioxins 19408-74-3 1,2,3, 7,8,9-Hexachloro-dibenzo-p-dioxin Certified EPA 16138 4 10 pg/L ORG/Dioxins 57117-41-6 1,2,3, 7,8-Pentachloro-dibenzofuran Certified EPA 16138 3 10 pg/L ORG/Dioxins 40321-76-4 1,2,3, 7,8-Pentachloro-di benzo-p-dioxin Certified EPA 16138 3 10 pg/L ORG/Dioxins 60851-34-5 2,3,4,6, 7,8-Hexachloro-dibenzofuran Certified EPA 16138 3 10 pg/L 3 10 pg/L ORG/Dioxins 57117-31-4 2,3,4, 7,8-Pentachloro-dibenzofuran Certified EPA 16138 ORG/Dioxins 51207-31-9 2,3,7,8-Tetrachloro-dibenzofuran Certified EPA 16138 1 2 pg/L ORG/Dioxins 1746-01-6 2,3,7,8-Tetrachloro-dibenzo-p-dioxin Certified EPA 16138 1 2 pg/L ORG/Pest/Herb/PC8 72-54-8 4,4-DDD Certified EPA 608 0.0053 0.02 ug/L ORG/Pest/Herb/PC8 72-55-9 4,4-DDE Certified EPA 608 0.005 0.02 ug/L ORG/Pest/Herb/PC8 50-29-3 4,4-DDT Certified EPA 608 0.0052 0.02 ug/L ORG/Pest/Herb/PC8 309-00-2 Aldrin Certified EPA 608 0.002 0.01 ug/L ORG/Pest/Herb/PCB 86-50-0 Azinphos methyl (Guthion) Certified EPA 622 2 6 ug/L ORG/Pest/Herb/PCB 57-74-9 Chlordane Certified EPA 608 0.08 0.5 ug/L ORG/Pest/Herb/PCB 2921-88-2 Chlorpyrifos Certified EPA 622 2 6 ug/L ORG/Pest/Herb/PCB 8065-48-3 Demeton-0 Certified EPA 622 2 6 ug/L ORG/Pest/Herb/PCB 919-86-8 Demeton-S Certified EPA 622 2 6 ug/L ORG/Pest/Herb/PCB 333-41-5 Diazinon Certified EPA 622 2 6 ug/L ORG/Pest/Herb/PCB 60-57-1 Dieldrin Certified EPA 608 0.0051 0.02 ug/L ORG/Pest/Herb/PCB 298-04-4 Disulfoton Certified EPA 622 2 6 ug/L ORG/Pest/Herb/PCB 959-98-8 Endosulfan I Certified EPA 608 0.0051 0.01 ug/L ORG/Pest/Herb/PCB 33213-65-9 Endosulfan II Certified EPA 608 0.011 0.02 ug/L ORG/Pest/Herb/PCB 1031-07-8 Endosulfan Sulfate Certified EPA 608 0.005 0.02 ug/L ORG/Pest/Herb/PCB 72-20-8 Endrin Certified EPA 608 0.007 0.02 ug/L ORG/Pest/Herb/PCB 7421-93-4 Endrin aldehyde Certified EPA 608 0.02 0.1 ug/L Kentucky Wastewater Laboratory Certification - 2016 K~~ Method Mod mg/L Microbiology I ATP 3 of6 Laboratory Name: Eurofins Lancaster Laboratories Environmental, LLC KY Lab ID#: 90088 KY Category CAS# Analyte Status ORG/Pest/Herb/PCB 76-44-8 Heptachlor Certified Reference Method EPA 608 ORG/Pest/Herb/PCB 1024-57-3 Heptachlor epoxide Certified EPA 608 0.0026 0.01 ORG/Pest/Herb/PCB 58-89-9 Lindane (gamma-BHC) Certified EPA 608 0.0025 0.01 ug/L ORG/Pest/Herb/PCB 63653-66-7 Parathion methyl Certified EPA 622 2 6 ug/L ORG/Pest/Herb/PCB 12674-11-2 PCB-1016 Certified EPA 608 0.2 0.5 ug/L ORG/Pest/Herb/PCB 11104-28-2 PCB-1221 Certified EPA 608 0.2 0.5 ug/L MDL 0.0026 MRL 0.01 ug/L ug/L Units ORG/Pest/Herb/PCB 11141-16-5 PCB-1232 Certified EPA 608 0.2 0.5 ug/L ORG/Pest/Herb/PCB 53469-21-9 PCB-1242 Certified EPA 608 0.2 0.5 ug/L Certified EPA 608 0.2 0.5 ug/L ORG/Pest/Herb/PCB 12672-29-6 PCB-1248 ORG/Pest/Herb/PCB 11097-69-1 PCB-1254 Certified EPA 608 0.2 0.5 ug/L ORG/Pest/Herb/PCB 11096-82-5 PCB-1260 Certified EPA 608 0.3 0.5 ug/L ORG/Pest/Herb/PCB 8001-35-2 Toxaphene Certified EPA 608 0.3 1 ug/L ORG/Pest/Herb/PCB 319-84-6 a-BHC (Alpha-BHC) Certified EPA 608 0.0032 0.01 ug/L ORG/Pest/Herb/PCB 319-85-7 13-BHC (Beta-BHC) Certified EPA 608 0.0049 0.01 ug/L ORG/Pest/Herb/PCB 319-86-8 c5-BHC (Delta-BHC) Certified EPA 608 0.0038 0.01 ug/L ORG/Semi-Volatiles 95-94-3 1,2,4,5-Tetrachlorobenzene Certified EPA625 0.2 5 ug/L ORG/Semi-Volatiles 120-82-1 1,2,4-Trichlorobenzene Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 122-66-7 Certified EPA 625 0.2 5 ug/L ug/L ORG/Semi-Volatiles 39638-32-9 1,2-diphenylhydrazine 2,2 -Oxybis(2-chloro-propane) AKA bis(2chloroisopropyl)ether Certified EPA 625 0.3 5 ORG/Semi-Volatiles 95-95-4 2,4,5-trichlorophenol Certified EPA 625 0.4 5 ug/L ORG/Semi-Volatiles 88-06-2 2,4,6-Trichlorophenol Certified EPA 625 0.7 5 ug/L ug/L ORG/Semi-Volatiles 120-83-2 2,4-Dichlorophenol Certified EPA 625 0.3 5 ORG/Semi-Volatiles 105-67-9 2,4-Dimethylphenol Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 51-28-5 2,4-Dinitrophenol Certified EPA 625 10 30 ug/L ORG/Semi-Volatiles 121-14-2 2,4-Dinitrotoluene Certified EPA 625 0.4 5 ug/L ORG/Semi-Volatiles 606-20-2 2,6-Dinitrotoluene Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 91-58-7 2-Chloronaphthalene Certified EPA 625 0.2 5 ug/L ORG/Semi-Volatiles 95-57-8 2-Chlorophenol Certified EPA 625 0.3 5 ug/L 4 15 ug/L ORG/Semi-Volatiles 8071-51-0 2-Methyl-4,6-Dinitrophenol Certified EPA 625 ORG/Semi-Volatiles 88-75-5 2-Nitrophenol Certified EPA 625 0.4 5 ug/L ORG/Semi-Volatiles 91-94-1 3,3-Dichlorobenzidine Certified EPA 625 0.8 5 ug/L ORG/Semi-Volatiles 101-55-3 4-Bromophenyl phenyl ether Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 59-50-7 4-Chloro-3-methyl phenol Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 7005-72-3 4-Chlorophenyl phenyl ether Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 100-02-7 4-Nitrophenol Certified EPA 625 5 10 ug/L ORG/Semi-Volatiles 83-32-9 Acenaphthene Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 208-96-8 Acenaphthylene Certified EPA 625 0.3 5 ug/L Kentucky Wastewater Laboratory Certification - 2016 I(~~ ATP Method Mod 4of6 Laboratory Name: Eurofins Lancaster Laboratories Environmental, LLC KY Lab ID#: 90088 KY Category Method CAS# Analyte Status Anthracene Certified Reference Method EPA 625 92-87-5 Benzi dine Certified EPA 625 20 60 ug/L 56-55-3 Benzo(a}anthracene Certified EPA 625 0.2 5 ug/L ORG/Semi-Volatiles 50-32-8 Benzo(a)pyrene Certified EPA 625 0.3 5 ug/L ORG/5emi-Volatiles 205-99-2 Benzo(b}fluoranthene Certified EPA 625 0.3 5 ug/L 5 ug/L ORG/Semi-Volatiles 120-12-7 ORG/Semi-Volatiles ORG/Semi-Volatiles MDL MRL 0.2 5 Units ORG/5emi-Volatiles 191-24-2 Benzo(g,h,i)perylene Certified EPA 625 0.2 207-08-9 Benzo(K}fluoranthene Certified EPA 625 0.3 5 ug/L ORG/5emi-Volatiles 111-91-1 bis(2-chloroethoxy}meth ane Certified EPA 625 0.5 5 ug/L ORG/Semi-Volatiles 111-44-4 bis(2-chloroethyl}ether Certified EPA 625 0.4 5 ug/L ORG/Semi-Volatiles 117-81-7 bis(2-ethylhexyl)phthalate Certified EPA 625 1 5 ug/L ORG/Semi-Volatiles 85-68-7 Butyl Benzyl Phthalate Certified EPA 625 0.8 5 ug/L ORG/Semi-Volatiles 218-01-9 Chrysene Certified EPA 625 0.2 5 ug/L ORG/Semi-Volatiles 53-70-3 Dibenzo(a,h}anthracene Certified EPA 625 0.4 5 ug/L ORG/5emi-Volatiles 84-66-2 Diethyl phthalate Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 131-11-3 Dimethyl phthalate Certified EPA625 1 5 ug/L ORG/Semi-Volatiles 84-74-2 Di-n-butyl phthalate Certified EPA 625 0.5 5 ug/L ORG/Semi-Volatiles 117-84-0 Di-n-octyl phthalate Certified EPA 625 0.5 5 ug/L ug/L ORG/Semi-Volatiles 206-44-0 Fluoranthene Certified EPA 625 0.3 5 ORG/Semi-Volatiles 86-73-7 Fluorene Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 118-74-1 Hexachlorobenzene Certified EPA 625 1 5 ug/L ORG/Semi-Volatiles 87-68-3 Hexachlorobutadiene Certified EPA 625 0.8 5 ug/L ORG/Semi-Volatiles 77-47-4 Hexachlorocyclopentadiene Certified EPA 625 2 15 ug/L ORG/Semi-Volatiles 67-72-1 Hexachloroethane Certified EPA 625 0.4 5 ug/L ug/L ORG/Semi-Volatiles 193-39-5 lndeno(l,2,3-cd}pyrene Certified EPA 625 0.3 5 ORG/Semi-Volatiles 78-59-1 lsophorone Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 91-20-3 Naphthalene Certified EPA 625 0.2 5 ug/L ORG/Semi-Volatiles 98-95-3 Nitrobenzene Certified EPA 625 0.5 5 ug/L ORG/Semi-Volatiles 924-16-3 N-Nitrosodibutylamine Certified EPA 625 0.5 5 ug/L ORG/Semi-Volatiles 55-18-5 N-Nitrosodiethylamine Certified EPA 625 0.5 5 ug/L ORG/Semi-Volatiles 62-75-9 N-Nitrosodimethylamine Certified EPA 625 2 5 ug/L ORG/Semi-Volatiles 621-64-7 N-Nitrosodi-n-propylami ne Certified EPA 625 0.4 5 ug/L ORG/Semi-Volatiles 86-30-6 N-Nitrosodiphenylamine Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 930-55-2 N-Nitrosopyrrolidine Certified EPA 625 0.5 5 ug/L ORG/Semi-Volatiles 608-93-5 Pentachlorobenzene Certified EPA 625 0.3 5 ug/L ORG/Semi-Volatiles 87-86-5 Pentachlorophenol Certified EPA 625 3 5 ug/L ORG/Semi-Volatiles 85-01-8 Phenanthrene Certified EPA 625 0.2 5 ug/L ORG/Semi-Volatiles 108-95-2 Phenol Certified EPA 625 0.4 5 ug/L Keo!!!~ Mod ug/L ORG/Semi-Volatiles Kentucky Wastewater Laboratory Certification - 2016 ATP 5 of 6 Laboratory Name: Eurofins Lancaster Laboratories Environmental, LLC KY Lab ID#: 90088 KY Category ORG/Semi-Volatiles CAS# 129-00-0 Pyrene ORG/Volatiles 71-55-6 1,1,1-Trichloroethane Certified EPA 624 1 5 ORG/Volatiles 79-34-5 1,1,2,2,-Tetrachloroethane Certified EPA 624 1 5 ug/L ORG/Volatiles 79-00-5 1, 1,2-Trichloroethane Certified EPA 624 1 5 ug/L Analyte Status Certified Reference Method EPA 625 MDL 0.2 MRL 5 Units ug/L ORG/Volatiles 75-34-3 1,1-Dichloroethane Certified EPA 624 1 5 ug/L 75-34-4 1,1-Dichloroethene Certified 0.9 5 ug/L ORG/Volatiles 95-50-1 1,2-Dichlorobenzene (o-Dichlorobenzene) Certified EPA 624 EPA 624 1 5 ug/L ORG/Volatiles 107-06-2 1,2-Dichloroethane Certified EPA 624 1 5 ug/L 5 ug/L ORG/Volatiles 78-87-5 1,2-Dichloropropane Certified EPA 624 1 ORG/Volatiles 541-73-1 1,3-Dichlorobenzene Certified 1 5 ug/L ORG/Volatiles 106-46-7 1,4-Dichlorobenzene (p-Dichlorobenzene) Certified EPA 624 EPA 624 1 5 ug/L ORG/Volatiles 110-75-8 2-Chloroethylvinyl ether Certified EPA 624 2 10 ug/L ORG/Volatiles 107-02-8 Acrolein Certified EPA 624 10 50 ug/L ORG/Volatiles 107-13-1 Acrylonitrile Certified EPA 624 10 so ug/L ORG/Volatiles 71-43-2 Benzene Certified EPA 624 0.9 5 ug/L ORG/Volatiles 75-27-4 Bromodichloromethane Certified EPA 624 0.7 5 ug/L ORG/Volatiles 75-25-2 Bromoform Certified EPA 624 0.8 5 ug/L ORG/Volatiles 74-83-9 Bromomethane (Methylbromide) Certified EPA 624 ORG/Volatiles 56-23-5 Carbon tetrachloride Certified EPA 624 2 5 ug/L 1 5 ug/L ORG/Volatiles 108-90-7 Chlorobenzene Certified EPA 624 0.8 5 ug/L ORG/Volatiles 75-00-3 Chloroethane Certified EPA 624 2 5 ug/L ug/L ORG/Volatiles 67-66-3 Chloroform Certified EPA 624 1 5 ORG/Volatiles 74-87-3 Chloromethane Certified EPA 624 2 5 ug/L ORG/Volatiles 542-75-6 cis-1,3-Dichloropropene Certified EPA 624 1 5 ug/L ORG/Volatiles 124-48-1 Dibromochloromethane Certified EPA 624 1 5 ug/L ORG/Volatiles 100-41-4 Ethyl benzene Certified EPA 624 0.8 5 ug/L ORG/Volatiles 75-09-2 Methylene chloride Certified EPA 624 2 5 ug/L ORG/Volatiles 127-18-4 Tetrachloroethene Certified EPA 624 1 5 ug/L 0.8 5 ug/L ug/L ORG/Volatiles 108-88-3 Toluene Certified EPA 624 ORG/Volatiles 156-60-5 trans-1,2-Dichloroethene Certified EPA 624 1 5 ORG/Volatiles 99614-02-5 trans-1,3-Dichloropropene Certified EPA624 0.6 5 ug/L ORG/Volatiles 79-01-6 Trichloroethene Certified EPA 624 1 5 ug/L ORG/Volatiles 75-69-4 Trichlorofluoromethane Certified EPA 624 2 5 ug/L ORG/Volatiles 75-01-4 Vinyl chloride Certified EPA 624 2 5 ug/L Kentucky Wastewater Laboratory Certification - 2016 l(~i!i!JA Method Mod ug/L ORG/Volatiles I ATP 6 of6 STEVEN L. BESHEAR LEONARD K. PETERS GOVERNOR SECRETARY ENERGY AND ENVIRONMENT CABINET DEPARTMENT FOR ENVIRONMENTAL PROTECTION DIVISION OF WASTE MANAGEMENT UNDERGROUND STORAGE TANK BRANCH 200 FAIR OAKS, 2ND FLOOR FRANKFORT, KENTUCKY 40601 http://waste.ky.gov/ust December 2, 2014 BARBARA F REEDY EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL LLC 2425 NEW HOLLAND PIKE LANCASTER PA 17605-2425 Laboratory Certification #: 89 AI: 108139 Dear Ms. Reedy: The Underground Storage Tank (UST) Branch has received your current A2LA accreditation submitted on November 19, 2014. We have updated our database to reflect your expiration dates from November 30, 2014 to November 30, 2016. This above certification is intended for the use of the Kentucky UST Branch. The approval is based on accreditation by either The American Association for Laboratory Accreditation (A2LA) OR by an approved state to accredit environmental laboratories in accordance with the National Environmental Laboratory Accreditation Program (NELAP) requirements and standards. Approved laboratories must be certified to conduct all required analysis using the acceptable methods listed in tables A and B of 401 KAR 42:060 and 401 KAR 42:070. For other analysis directed by the UST Branch not listed in tables A and B of 401 KAR 42:060 and 401 KAR 42:070; the laboratory performing the directed analysis must be currently accredited by either A2LA OR by an approved state to accredit environmental laboratories in accordance with the NELAP requirements and standards. The UST Branch does not regulate or certify those laboratories providing analysis of waste required by an accepting facility. More information, including the UST Branch regulations, outlines, forms and updates, can be found online at http://waste.ky.gov/ust. If you have any questions regarding this letter, please contact me at 502-564-5981, ext. 4772. Sincerely, Cheryl Yunt Claims and Payment Section UST Branch KentuckyUnbridledSpirit.com An Equal Opportunity Employer M/F/D