NORWEGIAN JOURNAL OF GEOLOGY Ordovician and Silurian magmatism in the Upper Nappe, Uppermost Allochthon, Helgeland 121 Ordovician and Silurian magmatism in the Upper Nappe, Uppermost Allochthon, Helgeland Nappe Complex, north-central Norway Calvin G. Barnes, Kristin Reid, Carol D. Frost, Melanie A. Barnes, Charlotte M. Allen & Aaron S. Yoshinobu Barnes, C.G., Reid, K., Frost, C.D., Barnes, M.A., Allen, C.M. & Yoshinobu, A.S.: Ordovician and Silurian magmatism in the Upper Nappe, Uppermost Allochthon, Helgeland Nappe Complex, north-central Norway. Norwegian Journal of Geology, vol. 91, pp 121-136. Trondheim 2011. ISSN 029-196X. The structurally lowest parts of the Upper Nappe of the Helgeland Nappe Complex consist primarily of migmatitic quartzofeldspathic gneiss with intercalated calc-silicate gneiss. Detrital zircons in the gneiss indicate an Ordovician depositional age. Migmatization via biotite dehydration reactions occurred at ~480 Ma at pressures of ~700 MPa; some migmatites were mobilized into cross-cutting diatexites. Diverse gabbroic to granitic plutons and dikes of the Bindal Batholith were emplaced from 448–424 Ma. They range from calc-alkaline to alkalic and most have initial 87Sr/86Sr <0.707 and εNd from 0 to -4. Pressures of emplacement were ca. 300 MPa. Shear zones with reverse shear sense cut 437 Ma intrusions, suggesting that contraction accompanied magmatism. Calvin G. Barnes, Department of Geosciences, Texas Tech University, Lubbock, Texas, 79409-1053, USA. E-mail: cal.barnes@ttu.edu. Kristin Reid Department of Geosciences, Texas Tech University, Lubbock, Texas, 79409-1053, USA. Carol D. Frost, Department of Geology and Geophysics, University of Wyoming, 1000 East University Avenue, Laramie, Wyoming, 82071, USA. E-mail: frost@uwyo.edu. Melanie A. Barnes, Department of Geosciences, Texas Tech University, Lubbock, Texas, 79409-1053, USA. E-mail: melanie.barnes@ttu.edu. Charlotte M. Allen, Research School of Earth Sciences, The Australian National University, Canberra, ACT 0200, Australia. E-mail: Charlotte.Allen@anu.edu.au. Aaron S. Yoshinobu, Department of Geosciences, Texas Tech University, Lubbock, Texas, 79409-1053, USA. E-mail: aaron.yoshinobu@ttu.edu. Introduction The 478–424 Ma Bindal Batholith in north-central Norway is an excellent example of a long-lived orogenic magmatic province in which a complex combination of mantle melting, crustal melting, magma mixing, and assimilation contributed to magma compositions (Nordgulen and Sundvoll, 1992; Nordgulen, 1993; Nordgulen et al., 1993; Barnes et al., 1992; Birkeland et al., 1993; Barnes et al., 2007). Because the Batholith intrudes a number of nappe sheets in the Helgeland Nappe Complex (HNC), an understanding of the timing of regional migmatization and its relationship to generation and coalescence of plutonic magmas is crucial to reconstruction of the tectonic setting and thermal history of the region. Regional migmatization and crustal melting affected parts of the HNC from ~480 to 475 Ma (Yoshinobu et al., 2002; Barnes et al., 2007) and granites emplaced during this time are peraluminous to strongly peraluminous with high initial 87Sr/86Sr values, features taken to indicate predominantly crustal origins (Nordgulen and Sundvoll, 1992; Nordgulen, 1993; Birkeland et al., 1993). Younger magmatic activity in the Batholith (465 to 424 Ma; Nord­ gulen et al., 1993; Yoshinobu et al., 2002; Nissen et al., 2006; Barnes et al., 2007; this paper) was much more diverse and included crust- and mantle-derived magmas in various forms of hybridization (Birkeland et al., 1993; Barnes et al., 1992, 2002, 2005). Early mapping in the HNC (Kollung and Myrland, 1970; Myrland, 1974) recognized the presence of a number of migmatitic rock units in central Helgeland and a later study in the Velfjord–Tosen area (Thorsnes and Løseth­, 1991) showed that these migmatitic units belonged to discrete nappes that were separated from one another by non-migmatitic (lower grade) nappes. It was not clear on the basis of this work whether regional migmatization in different nappes was the result of a single early Ordo­ vician metamorphic event, or whether it represented temporally and/or spatially distinct thermal events. This paper reports a U–Pb geochronologic, thermo­ barometric, and petrologic study of a long, nearly continu­ ous road cut near Tosenfjord that exposes migma­titic rocks of a structurally low part of the Upper Nappe of the HNC. The migmatites underwent partial melting at ~480 Ma and then from 448 to 424 Ma were repeatedly intruded by mafic to granitic dikes. Local 122 C. G. Barnes et al. B Explanation Devonian - Permian basin fill Uppermost Allochthon Upper Allochthon Middle Allochthon Lower Allochthon Parauthochthonous rocks Proterozoic Baltic cratonal rocks Sauren-Torghatten Nappe onid Horta Nappe (carbonate/gneiss/migmatite) Undifferentiated metamorphic rocks Normal-sense shear zone hon Fig. 1C pe rA llo ch t Central Norway Basement Window Up 12°00' 65°00' 200 km 14°00' 65°30' st A l Lower Nappe (pelitic schist & migmatite/marble) weg ian Trondheim loch Middle Nappe ~442 Ma Andalshatten pluton thon Upper Nappe Nor Western Gneiss Region Ocean Ophiolitic rocks Cale d Atlantic Ocean Rødingsfjallet Nappe Complex (Uppermost Allochthon) <440 Ma Granitoid rocks ~465-440 Ma Granitoid rocks ~465-440 Ma Diorite & gabbro > 465 Ma Igneous rocks Atlantic es Fig. 1B Explanation - Helgeland Nappe Complex & Bindal Batholith Up p er mo A NORWEGIAN JOURNAL OF GEOLOGY 14°00' 65°00' 25 km Vikna D C Velfjord 447±3 Ma Størborja G.A.S.P. ~ 500-700 MPa, ~800°C 2 Stromatic migmatite TF-304, melanosome TF-204, leucosome Diatexitic migmatite TF-104 Quartz-diorite pluton TF-404 Net-veined monzonitic dike N16.05 Biotite monzogranite TF-82 2 447±3.7 Ma 480.3±1.9 Ma 480.5, 479.4, 465.2 Ma 480.6±3.8 Ma 447.8—1.7 Ma 436.7±3.5 Ma ~ 424-470 Ma 420 MPa2 430±7 Ma1 2 445 Ma Tosbotn tunnel 65 N 64 64 76 Lande G.A.S.P. Poles to foliations, n = 17, average = 343/60 Lineations, n = 3 ~ 500-700 MPa, ~800°C To s en fjo rd 74 Diatexitic migmatite TF-77B 445.1±6.4 Ma Gabbro TF-70 436.9±4.4 Ma Tonalite dike TF-82 431.9±3.5 Ma Biotite monzogranite TF-82 424.7±5.6 Ma 10 km Figure 1. A. Tectonic map displaying allochthonous units within the Scandinavian Caledonides. B. Regional geologic map of the Helgeland Nappe Complex and Bindal Batholith, located within the Uppermost Allochthon. C. Simplified geologic map of the field area; legend as in B. Dike complex and migmatitic rocks are shown in grey and exposed along route 76 on the northwest shore of Tosenfjord. Regional structural trends are depicted by foliations with filled triangles. SHRIMP U-Pb zircon ages are shown in yellow; LA-ICP-MS U-Pb zircon ages are shown in white. Previously published age and depth measurements are from: 1 = Nordgulen et al., 1993; 2 = Yoshinobu et al., 2002. D. Lower-hemisphere stereonet showing poles to foliations and lineations from road side outcrop. NORWEGIAN JOURNAL OF GEOLOGY Ordovician and Silurian magmatism in the Upper Nappe, Uppermost Allochthon, Helgeland 123 deformation and development of metamorphic mineral assemblages in these dikes hint at a more or less continuous thermal pulse from ~437–424 Ma. Apparently, this exposure provides, in a km-long section, a significant portion of the Caledonian thermal history of the Upper Nappe and an important location by which to compare other parts of the Upper Nappe and the rest of the HNC. Geological setting Regional setting The Helgeland Nappe Complex is the structurally highest nappe complex of the Uppermost Allochthon (Fig. 1A; Roberts et al., 2007). In the Tosen–Velfjord–Brønnøy region, the HNC consists of four named nappes (Thorsnes and Løseth, 1991; Yoshinobu et al., 2002) and at least one additional nappe (Barnes et al., 2007). From structurally lowest to highest, these nappes are the informally named Horta nappe that is host to the Hortavær intrusion (Barnes et al., 2007), the Sauren-­ Torghatten, Lower, Middle, and Upper Nappes (Fig. 1A, B). Basal slivers of metaperidotite (serpentinite) and gabbro character­ ize the Sauren-Torghatten and Middle Nappes; these slivers are unconformably overlain by cover sequences of greenschist to amphibolite facies metasedimentary and metavolcanic rocks. The cover sequences include conglomerates and clastic metasediment­ ary rocks whose provenance ranges from volcanic to continental­shelf (Thorsnes and Løseth, 1991; Frost et al., 2006), sug­gestive of rapidly changing sediment sources. Moreover, the Sauren-Torghatten and Middle Nappes are evidently not overturned, as indicated by the east-­dipping contact­between the ultramafic and meta­sedimentary rocks which was interpreted to be an unconformable depositional contact by Thorsnes and Løseth (1991) and Yoshinobu et al. (2002). In contrast, the Lower and Upper Nappes contain a large proportion of high-grade semi-pelitic schist and gneiss, quartzofeldspathic gneiss, and marble (Gustavson, 1981; Thorsnes, 1987; Thorsnes and Løseth, 1991; Nord­gulen and Sundvoll, 1992). Most of the quartzofeldspathic gneissic rocks are migmatitic, with migmatite fabrics that range from stromatic (layered) and nebulitic (pod-like leucosomes) to diatexitic. Diatexitic migmatites are those in which original structure has been disrupted, generally by magmatic flow. In the Lower Nappe, which is domi­ nated by quartzofeldspathic gneiss and marble, with lesser calc-silicate gneiss, two migmatization events have been recognized. The older event (>477 Ma; Yoshinobu et al., 2002) was of regional extent and produced mildly to strongly peraluminous alkali-calcic granites (Barnes et al., 2002). The younger event was restricted to contact aureoles around mafic to intermediate plutons emplaced from 448 to 445 Ma (Barnes et al., 2002; Yoshinobu et al., 2002). This so-called contact migmatization began when the Lower Nappe was at ~700 MPa pressure, but ended after exhumation to ~400 MPa (Barnes and Prestvik, 2000). The focus of this study is on basal parts of the Upper Nappe (Fig. 1C; Thorsnes and Løseth, 1991). The Middle­ Nappe–Upper Nappe contact is ~1.6 km west of our study area, and is marked by the abrupt change structur­ ally upward from layered, amphibolite facies, non-­ migmatitic schists of the Middle Nappe to intercalated migmatitic and calc-silicate gneiss of the Upper Nappe. The latter rock types are characteristic of the Upper Nappe along Tosenfjord from Lande to Tosbotn (Fig. 1C), with lesser amounts of quartzofeldspathic gneiss and marble. Thus, the Upper Nappe contains rock types nearly identical to those of the Lower nappe, although in different proportions. The nappes are juxtaposed along east-dipping faults that were originally interpreted as thrusts (Thorsnes and Løseth­, 1991). Although initial reverse motion is likely on these faults, Yoshinobu et al. (2002) showed that final motion on the fault separating the Lower and Middle Nappes was in a normal sense. The Sauren-Torghatten, Lower, Middle, and Upper nappes were intruded by the Andalshatten pluton (Fig. 1B; Nordgulen et al., 1992). High-precision TIMS dating of the Andalshatten pluton­ to 442 Ma (Anderson et al., 2008) places a minimum age on terrane amalgamation. A recent study of zircon inherit­ance in Lower Nappe plutons (Barnes et al., 2007) indicates that terrane amalgamation was even earlier, and was complete by ~478 Ma. Plutonic rocks of the Bindal Batholith span an age range of 478–424 Ma. The oldest plutons are primarily per­ aluminous to strongly peraluminous granites, have Sr, Nd, and Pb isotopic features consistent with origins by crustal melting (Nordgulen and Sundvoll, 1992; Birkeland et al., 1993; Marko et al., 2007), and locally conant enclaves of metasedimentary rocks tain abund­ (Nord­gulen, 1993; Marko et al., 2008). These plutons are referred to as “anatectic granites” (e.g., Nordgulen, 1993). Magmatism continued with emplacement of the ~466 and ~465 Ma Horta­vær and Svarthopen intrusions, respectively (Barnes et al., 2007). Then at about 450 Ma, a prolonged pulse of magmatism began with emplacement of the Troholmen pluton near Rødøy (Barnes et al., 2007), followed by the Velfjord plutons (Yoshinobu et al., 2002), the Andalshatten pluton (~442 Ma; Anderson et al., 2008), and then a broadly distributed, diverse range of plutons from c. 440 to 424 Ma. The 450–424 Ma magmatism encompasses alkali-calcic to calc-alkalic and gabbroic to granitic magmas (Nordgulen and Schouenborg, 1990; Nordgulen et al., 1993; Nissen et al., 2006; Barnes et al., 2007; this paper). The isotopic compositions of these rocks are quite variable and are broadly consistent with mixed crustal and mantle sources (Nordgulen and Sundvoll, 1992; Birkeland et al., 1993). 124 C. G. Barnes et al. NORWEGIAN JOURNAL OF GEOLOGY A A’ net-veined meta-diorite mingled (”net veined”) monzonite/diorite west N16.05 435.1 ± 2.8 Ma stromatic migmatite mingled (”net veined”) TF-204 diorite TF-304 480.2 ± 3.6 Ma diatexitic migmatite TF-77B: 443.0 ± 4.9 Ma TF-104: 480.6 ± 3.8 Ma A’ A’’ stromatic migmatite mingled dike TF-75 N17.05 biotite leucogranite TF-81 424.7 ± 5.6 Ma Figure 2. TF-82 431.9 ± 3.5 Ma biotite tonalite with stromatic migmatite enclaves stromatic migmatite east Figure 2. Composite photograph of the northern side of the road cut with a sketch showing the various rock units and their crosscutting relationships. Dated units are labeled and the specific locations of dated samples are shown, where known. Shear zones are shown with red lines. Table 1: Table 1. Summary of rock units and ages. Rock unit Rock types Age (Ma)* migmatitic gneiss stromatic (banded) gneiss with tonalitic leucosomes 480.3 ± 1.9 calc-silicate gneiss blocks in migmatite: diopside, garnet, plagioclase, calcite diatexitic (disrupted) migmatite massive–weakly banded garnet biotite tonalite migmatite gneissic metamorphic rocks pegmatitic leucogranite dike eastern pluton 480.6 ± 3.8 ----- augite biotite hornblende qtz diorite/qtz monzodiorite 447.8 ± 1.7 gabbroic blocks in leucogranite hornblende pyroxene gabbro 436.9 ± 4.4 net-veined monzonitic dikes monzonite (enclaves) cut by leucomonzonite veins 436.7 ± 3.5 homogeneous & mingled dikes homogeneous monzodiorite ----- composite tonalite (host)--qtz diorite (enclaves) ----- composite melagranite (host)--qtz diorite (enclaves) ----- gabbroic to granitic dikes granitic & tonalitic dikes muscovite-biotite granodiorite/tonalite biotite monzogranite *Ages reported for migmatites are interpreted to date partial melting. All other ages interpreted to date magma emplacement. 431.9 ± 3.5 ~424 NORWEGIAN JOURNAL OF GEOLOGY Ordovician and Silurian magmatism in the Upper Nappe, Uppermost Allochthon, Helgeland 125 Local setting The study area is located along highway 76 west of Tosenfjord and 1.4 km northeast of Lande (Fig. 1C). The main focus of research is a ~500-meter-long set of double­ road cuts into high-grade metamorphic rocks crosscut by mafic, felsic, and composite dikes. The western end of the road cut has the following UTM coordinates: zone 33, 397370 easting, 7239419 northing (WGS84). The sequence of crosscutting relationships involves three distinct metamorphic units and a number of cross-­cutting intrusive units diagrammatically illustrated in Figure 2 and summarized in Table 1. Photographs in Figure 3 show some of these relationships in greater detail and additional detail is presented in Appendix 1. The various rock units are described below in order of decreasing age, as determined by U–Pb (zircon) dating and inferred from crosscutting relationships. Migmatitic and calc-silicate gneiss. The oldest rocks in the road cut exposures are isoclinally folded semi-pelitic gneiss, migmatitic gneiss, and associated calc-silicate gneiss. These migmatites are banded (stromatic), with distinct peraluminous, tonalitic leucosomes and biotite­rich, garnet- and sillimanite-bearing melanosomes (Fig. 2; Appendix 1). A sample of the stromatic migmatite was collected for geochronology and was split into a leucosome fraction (TF-204) and a melanosome fraction (TF304). Migmatitic rocks exposed from the base of the Upper Nappe to Tosbotn are broadly similar to those in the road cut, but in some cases also contain staurolite and cordierite. Calc-silicate rocks are intercalated with the migmatites and are present as boudins or schollen in stromatic migmatite. They typically consist of variable proportions of diopside, garnet, plagioclase, and calcite. In the central part of the road cut, stromatic migmatite is crosscut by medium-grained, foliated diatexitic migmatite (Figs. 2, 3A). The diatexite is peraluminous, tonalitic to quartz dioritic in composition and contains biotite, garnet, sillimanite, and muscovite. Garnet is similar in composition to that in the stromatic migmatite (Appendix 1). The diatexite encloses blocks (m- to dm-scale) of stromatic migmatite and calc-silicate gneiss (Fig. 2) and is therefore interpreted to be intrusive. Two samples for U–Pb dating were collected (TF-104 and TF77B; Fig. 2). Figure 3. Outcrop photographs. A. Stromatic migmatite intruded by diatexite. Hammer handle is 38 cm long. B. Blocks of foliated, banded diorite (e.g., TF-70) intruded by leucogranite. Pen is 13 cm long. C. Net-veined diorite– monzonite intrusion cutting stromatic migmatite, showing the location of dated sample N16.05. Pen is 13 cm long. D. Circa 435 Ma mingled dike. Hammer is 59 cm long. diatexite A stromatic migmatite B C D sample N16.05 Figu 126 C. G. Barnes et al. Structural development within the migmatitic and calcsilicate gneiss is dominated by a moderate to steeply eastdipping, axial planar metamorphic foliation and outcrop-scale isoclinal folds. Gneissic banding and foliations are penetrative within the migmatitic rocks (Fig. 3). Discreet, cm- to m-scale shear bands occur throughout the road cut. In many cases, these shear bands are localized on leucosomes, indicating melt-present deformation. Three outcrop-scale shear bands approximately 3–10 cm thick are shown on Figure 2 and exhibit top-to-the west sense of displacement along east-dipping planes. However, asymmetric kinematic indicators were not widely observed within the outcrop; a few normal-sense (downto-the east), cm-scale shear bands were observed. A limited number of lineations defined by recrystallized aggregates of quartz, feldspar, and biotite plunge moderately to the east-northeast along northwest-trending foliation planes (Fig. 1D), consistent with west-directed thrusting (e.g., Thorsnes and Løseth, 1991; Yoshinobu et al., 2002). Pegmatitic leucogranite dikes. Near the western end of the road cut, white, pegmatitic leucogranitic dikes crop out. Grain size increases from medium-grained cores to very coarse-grained margins and the proportion of alkali feldspar increases toward the margins. Biotite reaches 4 cm in length and is oriented perpendicular to dike margins (Fig. A1). These dikes are interpreted to be accumulations of leucosome magma from adjacent migmatites, but have not been dated. Pluton east of main road cut. Approximately 100 m east of the section studied in detail, a small, medium- to coarsegrained pluton of augite biotite hornblende quartz diorite/quartz monzodiorite intrudes the stromatic migmatite. It contains rounded mafic magmatic enclaves and xenoliths of the host rocks. A sample of this pluton (TF404) was collected for U–Pb dating. Gabbroic to granitic dikes. The remaining intrusive rocks in the road cut range from gabbro to granite. They display an array of grain size, intrusive shapes (Fig. 2), mineral assemblages, chemical composition, deformation, and degree of metamorphic fabric development (see Appendix 1 for detailed descriptions and photographs). Many of the dikes are mingled and some show evidence of physical and chemical hybridization. U–Pb dating (see below) and field relationships show that they were emplaced from 437 to 424 Ma, and most were emplaced between 437 and 432 Ma. Green, fine-to coarse-grained mafic rocks crop out near the west-central part of the road cut where they form blocks and boudins in white leucogranite (Fig. 3B). The blocks range from coarse-grained and massive to medium-grained, foliated, and banded (Fig. 3B); they contain diopsidic pyroxene, poikilitic hornblende, biotite, and plagioclase (Appendix 1). In the field, these mafic blocks were interpreted to represent mafic intrusions emplaced prior to migmatization; however U-Pb NORWEGIAN JOURNAL OF GEOLOGY dating of a sample of banded diorite (TF-70) indicates that this is not the case (see below), at least for some of the mafic rocks. Fine- to medium-grained net-veined monzonitic dikes cut diatexite and stromatic migmatite (Fig. 3C). The dikes consist primarily of biotite hornblende augite monzonite, which occurs as enclaves surrounded by thin veins of hornblende ± augite monzonite/quartz monzonite. The enclave-dike margins are commonly interdigitated. Where the net-veined dikes are in contact with migmatite, 8–10 cm-wide zones of “hybrid” quartzbearing hornblende monzonite are present. A sample of enclave material from the largest net-veined dike (N16.05) was collected for U–Pb dating (Figs. 2, 3C). One of the net-veined dikes is deformed by a throughgoing, top-to-the-west shear zone (Fig. 2). Homogeneous and mingled dikes. The net-veined dikes are crosscut by dikes of fine-grained, dark gray, homogeneous hornblende monzodiorite and by fine- to mediumgrained, pillowed, composite dikes. There are two types of mingled dike: pale gray, biotite tonalite with enclaves of dark gray, hornblende biotite quartz diorite, and pale gray, porphyritic, biotite quartz diorite with enclaves of hornblende biotite melagranite (Fig. 3D). Deformation of these dikes is variable, from undeformed to strongly deformed and mylonitic. Granitic and tonalitic dikes. The stromatic migmatite, diatexite, and homogeneous and net-veined monzonitic dikes are crosscut by dikes of white, fine- to coarsegrained, biotite monzogranite and pale gray muscovitebearing biotite granodiorite/tonalite. The largest example of the granodiorite/tonalite is exposed near the eastern end of the road cut and reaches at least 15 meters in width (Fig. 2); it was sampled for U–Pb dating (sample TF-82). The granodiorite/tonalite is cut by a pale gray, medium-grained biotite monzogranitic dike in a splayed array with both curved and angular contacts (Fig. 2). Two samples of this dike were dated (TF-81 and N17.05). Geochemistry Analytical methods. Analytical methods are presented in Appendix 2. In brief, mineral compositions were determined by electron microprobe at the University of Wyoming, major element rock compositions were measured by inductively-coupled plasma optical emission spectrometry at Texas Tech University, rare earth and other trace element concentrations were determined by inductively-­coupled plasma mass spectrometry (ICP-MS) at Washington State University, and isotope ratios by isotope dilution thermal ionization mass spectrometry at the University of Wyoming. U–Pb ages of zircon were determined by Sensitive High Resolution Ion Micro Probe-Reverse NORWEGIAN JOURNAL OF GEOLOGY Ordovician and Silurian magmatism in the Upper Nappe, Uppermost Allochthon, Helgeland 127 Geometry (SHRIMP-RG; Stanford University) and laser ablation (LA) ICP-MS at the Research School of Earth Sciences, Australia National University. The geochronologic data are given in Appendix Tables 1 (LA-ICP-MS) and 2 (SHRIMP-RG). probability plot at ~420 and ~460 Ma. These zircons have a relatively large range of U contents (Appendix Table 1), but there is no correlation between age and abundance of U. Using zircons in the 420–460 Ma range, an age of 436.7 ± 3.5 Ma is obtained (MSWD = 1.20). U–Pb dating Tonalitic dike. SHRIMP-RG analysis of sixteen zircons from the biotite tonalite (TF-82) yielded dates from 425 to 448 Ma (Fig. 4H). This population yielded an average age of 431.9 ± 3.5 Ma. Stromatic migmatite melanosome. Zircons from sample TF-304 were dated by LA-ICP-MS. Two crystals gave concordant ages at 717 and 773 Ma (Appendix Table 1). The remaining concordant zircon ages range from 467 to 498 Ma (Fig. 4A). An average of all ages in this range yields 480.2 ± 3.6 Ma (MSWD = 2.43). Exclusion of the three youngest and four oldest zircons results in a statistically identical age of 480.3 ± 1.9 Ma (MSWD = 0.73; Fig. 4A). Stromatic migmatite leucosome. The leucosome fraction (sample TF-204) yielded few zircons. Two zircons yielded concordant ages of 480.5 and 479.4 Ma with a third at 465.2 Ma. Five older concordant ages were obtained at 974, 1014, 1060, 1407, and 1735 Ma. Diatexitic migmatite. Two samples of diatexitic migmatite were dated, one (TF-104) by LA-ICP-MS (Appendix Table 1) and the other (TF-77B) by SHRIMP-RG (Appendix Table 2). Sample TF-104 yielded 13 concordant ages in the range 472–492 Ma (Fig. 4B) and others at 649, 796, 1021, 1401, and 1412 Ma. Within the age range 470–495 Ma, an average age of 480.6 ± 3.8 Ma was obtained. SHRIMP-RG data for sample TF-77B resulted in five approximately concordant detrital zircon ages of 602, 772, 1280, 1348, and 1565 Ma, along with two discordant ages of 463, and 473 Ma and a group of younger zircons whose average age is 445.1 ± 6.4 Ma (Fig. 4C & D). We call attention to the discrepancy in these ages compared to sample TF-104 at the end of this section. Pluton east of main road cut. The quartz dioritic intrusion sampled east of the main study area (TF-404) yielded 20 concordant dates by LA-ICP-MS (Fig. 4E) that average 447.3 ± 2.8 Ma. If the five youngest and four oldest dates are excluded, an average of 447.8 ± 1.7 Ma (MSWD = 0.27) is obtained. No inherited zircons were observed. Banded gabbro. SHRIMP-RG dating of the banded gabbro sample TF-70 yielded a range of concordant ages from 420 to 458 Ma (Fig. 4F). With the possible exception of the single date at ~458 Ma, no distinct break in the zircon age data is apparent, therefore all of the data were used to obtain an age of 436.9 ± 4.4 Ma. As with quartz diorite sample TF-404, no inherited zircons were observed. Net-veined monzonitic dike. Enclave material from a net-veined dike that cuts diatexite (N16.05) yielded zircons with LA-ICP-MS dates that span a range from ~415 to 479 Ma (Fig. 4G), with changes in the slope of the Late biotite monzogranite. Laser ablation ICP-MS analysis of zircons from sample N17.05, the biotite monzogranite that cuts the biotite tonalite dike (TF-82), showed a large variation in U content, from < 130 to >26,000 ppm. Moreover, within the normal limits used to define concordance, many zircons were classified as discordant. Figure 4I shows the age spectrum obtained when slightly less stringent limits were placed on concordancy. In this case, two zircons have ages at 424.0 ± 1.2 Ma, two at ~444 Ma, and a cluster of 8 analyses between 458 and 470 Ma. There is no correlation between age and U content. Six zircons from a second sample of this body (TF81) were analyzed by SHRIMP-RG. The average age for all six analyses is 425.2 ± 9.7 Ma and if two extreme samples (441 and 404 Ma) are rejected, the remaining four crystals yield an age of 424.7 ± 5.6 Ma. We interpret the SHRIMP and LA-ICP-MS data to indicate an age of ~424 Ma for this monzogranite, with inheritance at ~444 Ma as well as older ages. The small number of circa 424 Ma zircons is consistent with the monzogranite having crystallized from a low-T magma in which most zirconium in the sample was sequestered in inherited zircon. This conclusion is supported by zircon-saturation temperatures (Watson and Harrison, 1983) of 654–691 °C. Summary of U–Pb ages. We interpret the LA-ICP-MS ages determined for samples of the stromatic and diatexitic migmatites to indicate that crustal melting occurred in this part of the Upper Nappe at ~480–481 Ma. The discrepancy between the ca. 480 Ma age determined for diatexite sample TF-104 by LA-ICP-MS and the ~445 Ma age determined for TF-77B by SHRIMP is problematic. Some of the most intricate and difficult intrusive relationships exposed in this outcrop are leucocratic veins that appear to emanate from stromatic or diatexitic migmatite and then mingle with or cut various dike rocks. In the field, these relationships were interpreted to indicate that the migmatites were partly molten at the time of later dike emplacement. This observation was particularly important with regard to the net-veined monzodiorite that intrudes the diatexite (e.g., N16.05; Fig. 3C), because some rocks at the margin of this intrusion were interpreted to be hybrids of the net-veined dike and migmatite. However, the 436.7 ± 3.5 Ma age of sample N16.05 is interpreted to be an intrusive age because the dated zircons were separated from the mafic part of the dike. Because of this result, the ca. 445 Ma date obtained from diatexite sample TF-77B may be interpreted as (1) 128 C. G. Barnes et al. NORWEGIAN JOURNAL OF GEOLOGY 500 495 490 495 490 480.3 ± 1.9 0.73 (n=15) 485 485 date (Ma) date (Ma) 500 TF-304 stromatic migmatite melanosome 480 480 475 475 470 465 460 A -3 207 470 entire range: 480.2 ± 3.6 2.43 (n=21) 206 -2 -1 Pb/ Pb 0 stdev 1 465 460 2 3 TF-77B diatexite 0.066 0.058 480 0.054 440 420 470 13.0 13.4 13.8 14.2 238U/ 206 Pb 14.6 -3 460 -2 -1 0 stdev 1 2 3 TF-77B diatexite 445.1 ± 6.4 3.4 (n=13) 440 420 C 0.050 12.6 15.4 400 15.0 D TF-404 quartz diorite entire range 447.3 ± 2.8 Ma 1.24 (n=20) 465 460 455 date (Ma) 460 B 480 date (Ma) 0.062 TF-104 diatexitic migmatite 480.6 ± 3.8 1.17 (n=13) 450 445 440 435 447.8 ± 1.7 Ma 0.27 (n=11) 430 E 425 420 -3 Figure 4 -2 -1 0 stdev mis-sampling in the field, (2) evidence that the diatexite remained in a partly molten state for more than 40 m.y., (3) resetting of part, but not all of the zircons in the diatexite at ca. 447 Ma, (4) evidence that the migmatite was remelted during magma intrusion at ~437 Ma, permitting hybridization, or (5) contamination of the migmatite by younger leucocratic magmas. At present, we discount the first possibility because the chemical composition of TF-77B is similar to other migmatitic rocks (see below), and discount the second possibility because there is no evidence for similar long-term high temperatures elsewhere in the HNC. Resetting at ca. 447 Ma is 1 2 3 possible if the middle crust was sufficiently heated by magma emplacement at that time (e.g., Velfjord plutons). However, the nearest large plutons of this age crop out 10 km from the field area. The latter two explanations are quite possible, particularly in view of the intricate veins and dikes that were emplaced from 437–424 Ma. Further detailed geochronologic study of the Upper Nappe is needed to constrain better its thermal history. After migmatization, the next identifiable igneous event in the area is emplacement of the quartz dioritic pluton (TF-404) at 447.8 Ma. This is the same age NORWEGIAN JOURNAL OF GEOLOGY Ordovician and Silurian magmatism in the Upper Nappe, Uppermost Allochthon, Helgeland 129 470 480 TF-70 banded diorite 436.9 ± 4.4 Ma 460 2.4 (n=22) 460 440 450 430 440 420 400 430 420 F 460 TF-82 tonalitic dike 431.9 ± 3.5 Ma 450 0.89 (n=16) 440 410 G -3 -2 -1 0 stdev 1 2 3 480 470 460 date (Ma) date (Ma) 436.7 ± 3.5 Ma 1.20 (n=19) date (Ma) date (Ma) 450 410 N16.05 net-veined monzodiorite dike 470 450 440 430 430 420 410 H 420 410 N17.05 granitic dikes 424.0 ± 1.2 I -3 -2 -1 0 stdev 1 2 3 Figure 4. Results of U–Pb dating of zircon. A. Probability plot of results for stromatic migmatite melanosome TF-304. Uncertainties are 1 σ. The shaded area represents analyses selected to interpret the age of migmatization. B. Probability plot for diatexitic migmatite TF-104. C. Concordia plot for diatexite sample TF-77B. D. Age distribution of concordant zircons younger than 480 Ma in TF-77B. See text for discussion. E. Probability plot for quartz diorite pluton sample TF-404. The shaded area represents analyses selected to interpret the age of emplacement. F. Age distribution of zircons from banded diorite sample TF-70. G. Probability plot of net-veined monzodiorite sample N16.05. The shaded area represents analyses selected to interpret the age of emplacement.Figure H. Age 4 distribution of zircons from tonalitic dike TF-82. I. Probability plot for granitic dike N17.05. The shaded area represents analyses selected to interpret the age of emplacement. Data in panels A, B, E, G, and I were determined by LA-ICPMS, for panels C, D, F, and H by SHRIMP-RG. See text and Appendix 1 for details. as emplacement of voluminous dioritic to granitic plutons of the Velfjord area to the west (Fig. 1; Yoshinobu et al., 2002; Anderson et al., 2008). In the study area, there evidently was a magmatic lull until about 437 Ma. From ~437 to ~424 Ma, the Upper Nappe was intruded by mafic (gabbroic and dioritic), tonalitic, monzonitic, and granitic magmas, many of which were mingled. This time range is very similar to the ages of the large felsic plutons that characterize the eastern part of the Bindal Batholith (Nordgulen et al., 1993; Nissen et al., 2006). Major and trace element compositions Migmatites. The migmatite samples vary in SiO2 content from ~53 to 73% (Appendix Table 3; Fig. 5). Two samples of diatexite have SiO2 contents near 55%, whereas a bulk sample of the stromatic migmatite and two analyzed leucosomes range from 65 to 73% SiO2 (Fig. 5). All of the analyzed migmatites are strongly peraluminous, with A/ CNK > 1.1 (Fig. 5A). The melanosome has the highest A/CNK value (~2.1), which is indicative of its high biotite content. The migmatite samples have quite uniform values of FeO*/(FeO*+MgO) of ~0.74 (Fig. 5B). Such uniformity is not characteristic of magmatic suites (e.g., 130 C. G. Barnes et al. A mel A/CNK 2.0 1.5 leu dtx 1.0 vnA enAz hostB enA enB 0.5 leu 432 SiO2 B dia vnA 0 dia ic lc -ca li a alk enAz enB enB SiO2 50 55 60 65 D 70 75 80 vnA enB enAz enA hostB dia enAz 500 enB str enA SiO2 65 leu 432 enA 1000 60 str 2000 0.6 55 leu 1500 hostB 50 hostB leu 432 0.7 alic -alk calc cic cal ppm Sr FeO*/(FeO*+MgO) str leu dia104 mel dia -10 45 2500 magnesian mel 0.4 45 5 ferroan 0.8 0.5 lic alka -5 A=net-veined B=pillowed dike 0 C 10 str dtx 0.9 15 migmatite 448 Ma 437-432 Ma ~424 Ma Na2O+K2O-CaO 2.5 NORWEGIAN JOURNAL OF GEOLOGY 70 75 80 432 leu leu dia mel 0 0 1 2 CaO 3 4 5 6 7 8 9 Figure 5. Representative geochemical variation diagrams, with samples grouped according to approximate age, where known. Black triangles with dashed tie lines connect coexisting enclave (enA, enAz) and host vein (vnA) compositions in the 437 Ma net-veined dike. Black triangle labeled 432 is dated sample TF-82, the tonalite/granodioritic body at the eastern end of the road cut. Orange triangles connected by dashed tie lines represent a mingled (pillowed) dike with quartzdioritic/tonalitic host (vnB) and melagranitic enclaves (B). Abbreviations associated with migmatitic samples are: str = stromatic migmatite; dtx = diatexite; mel = melanosome; leu = leucosome. A. weight percent SiO2 vs. A/CNK, where A/CNK is molar Al2O3/CaO + Na2O + K2O. B. All igneous samples plot in the magnesian field of Frost et al. (2001). C. Samples of igneous rocks range from calc-alkalic to mildly alkalic according to the modified alkali-lime index (Frost et al., 2001). D. Plot of CaO versus ppm Sr showing the wide range of Sr contents, particularly among the most mafic samples. Note the lack of correlation of Sr content with CaO in the mafic and intermediate samples. Figure 5. Frost et al., 2001). Instead it is suggestive of uniform compositions of ferromagnesian phases in melanosomes, leucosomes, and diatexites. Among the migmatites, the melanosome has the highest rare earth element (REE) abundances (Fig. 6A) and in particular the highest abundances of heavy REE. Diatexite sample TF-104 has a similar pattern to the melanosomes; however, the pattern of diatexite TF-77B is distinct from the melanosome pattern in having much lower heavy REE abundances. Leucosomes are characterized by heavy REE concentrations, ~10x chondrites (Fig. 6A). One leucosome has lower light REE abundances than the other samples and a positive Eu anomaly, all of which suggest that this sample contains cumulate plagioclase. 448 Ma pluton. Two samples of the ~448 Ma quartz dioritic to quartz monzodioritic pluton east of the main road cut are metaluminous, magnesian, and span the boundary between calc-alkalic and alkali-calcic (Fig. 5). They have moderate REE slopes (normalized La/Lu = 33) and slight negative Eu anomalies (Fig. 6B). Younger intrusive rocks. Field relationships and U–Pb ages suggest that all of the post-migmatite intrusive rocks in the main road cut have ages from 437–424 Ma, and most range from ~437 to 432 Ma. Therefore, we have not attempted to subdivide these units into narrower age groups and instead discuss them as a single suite. Samples with SiO2 contents < 60 wt% are metaluminous, whereas those with higher SiO2 contents lie on or just Ordovician and Silurian magmatism in the Upper Nappe, Uppermost Allochthon, Helgeland 131 NORWEGIAN JOURNAL OF GEOLOGY Figure 6. Chondritenormalized REE diagrams. A. Migmatitic rocks and related (?) comb-layered dike. B. Samples from the 448 Ma pluton east of the main road cut and monzodioritic sample TF-79 (~437 Ma). C. Mingled dikes. D. Evolved dikes ≤ 435 Ma. 1000 1000 A stromatic migmatite diatexite (TF-104/TF-77B) TF -7 B leucosome/melanosome pair 3 comb-layered dike (TF-71) 100 100 leu co so me 10 10 TF-17 sample/chondrites TF-404 }448 Ma TF-79 (~435 Ma) 1 1000 La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er Tm Yb Lu 1000 C mingled dikes (437-432 Ma) La Ce Pr Nd D Sm Eu Gd Tb Dy Ho Er Tm Yb Lu tonalitic to granitic rocks 100 enclave felsic component hybrid (TF-66) 100 10 1 10 TF-74 TF-67 (~435 Ma) TF-64 TF-82 (431 Ma) TF-84 TF-81 (424 Ma) TF-72 ( 424 Ma) 1 La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er Tm Yb Lu 1 La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er Tm Yb Lu Figure 6 above the metaluminous–peraluminous boundary (Fig. 5A). All samples plot in the magnesian field of Frost et al. (2001), although two samples associated with the 437 Ma net-veined unit plot near the magnesian–ferroan boundary (Fig. 5B). In the modified alkali-lime index diagram (Fig. 5C), compositions vary from calc-alkalic to alkalic. The single sample that plots in the calcic field is a 437 Ma banded gabbro that is probably an augite cumulate. This suite of dikes is characterized by relatively high Sr contents (Fig. 5D). Most dikes with less than 3% CaO have >1000 ppm Sr and in this compositional range, no correlation exists between the Sr and CaO contents. In contrast, the older 448 Ma quartz diorite has lower Sr contents than the younger dikes (~750 ppm; Fig. 5D) and the ~424 Ma granitic dike has <500 ppm Sr. Figure 6C shows REE patterns for mingled dikes and related rocks. All show similar patterns, with slight negative Eu anomalies. In two of the enclave-host pairs, the net-veined dike (TF 74) and the pillowed dike (TF-84), the REE abundances of the host are higher than in the enclaves. In contrast, for the mingling zone at the west end of the exposure (samples TF-64 & 66; see Appendix 1), the REE patterns of the enclave and host cross, with higher light REE and lower heavy REE in the host rock (Fig. 6C). The hybrid rock associated with TF-64 (sample TF-66; Fig. 6C) has REE abundances that are generally intermediate between the enclave and host. Figure 6D shows REE patterns for 437–424 Ma felsic dikes. Samples TF-67 and TF-72 have patterns similar 132 C. G. Barnes et al. to those of the felsic parts of mingled dikes TF-74 and TF-84 (Fig. 6C), whereas sample TF-81 has lower heavy REE, similar to the felsic part of mingled dike TF-64 (Fig. 6C). The pattern for the dated granodiorite (TF-82) shows low REE abundances and a positive Eu anomaly which are typical for plagioclase accumulation. NORWEGIAN JOURNAL OF GEOLOGY 2 Nd (t) 0 A Nd and Sr isotope data All three samples of migmatitic rocks analyzed for Nd and Sr isotopic compositions (Appendix Table 4; Fig. 7) have low initial εNd values (-7 to -8) and high initial 87Sr/86Sr values (0.714–0.718). The diatexitic migmatite sample has distinctly lower initial 87Sr/86Sr than the stromatic migmatite and the leucosome. In view of the concentrations of Sr in all migmatite samples (332–622 ppm) this variation is probably related to isotopic heterogeneity in the sedimentary protolith rather than differences in the growth of radiogenic Sr after migmatization. The 448 Ma quartz dioritic pluton east of the main road cut has initial εNd and 87Sr/86Sr values of -4.8 and 0.71043, respectively (Appendix Table 4). These isotope ratios are quite distinct from those of the 437–432 Ma dike rocks, which have εNd from -0.2 to -2.4 and initial 87Sr/86Sr between 0.706 and 0.708. This rather narrow range of isotopic values encompasses rocks from 50 to 65 wt% SiO2 and 1.2–8% MgO. Within this group, there is no correlation between initial 87Sr/86Sr and SiO2 or 1/Sr, although the two samples with the highest 1/Sr values also have the highest initial 87Sr/86Sr. In contrast, a weak negative correlation exists between εNd and 1/Nd (and SiO2 content). The youngest sample analyzed for isotope ratios (424 Ma leucogranite TF81) has isotopic compositions nearly identical to the 448 Ma quartz diorite (Fig. 7). In the preceding field descriptions, we noted field evidence that suggested significant interaction between migmatitic rocks and younger dikes. One specific case was the possible interaction of magma of the net-veined dike with adjacent diatexite (Fig. 2). The isotopic compositions of the enclave and the vein material from this dike are nearly identical, and show no evidence of a mixing line with the adjacent migmatite (field A on Fig. 7). In a broader sense, isotopic compositions of the majority of the 437–432 Ma dike rocks are difficult to explain as hybrids of a mafic end member and migmatitic rocks (or magmas). This is because such hybridization should result in a decrease in the Sr content of the igneous rocks, with corresponding negative correlation of Sr and initial 87 Sr/86Sr with SiO2. Neither correlation is observed. Pressure and temperature estimates Migmatitic rocks. We attempted to use Fe-Mg exchange equilibria between garnet and biotite to estimate temperature (Reid, 2004). migmatite 448 Ma 437-432 Ma <425 Ma Velfjord plutons enB -2 hostB -4 424 Ma 448 Ma -6 -8 0.705 dia 0.710 0.715 87 leu str 0.720 86 initial Sr/ Sr Figure 7. εNd (t) plotted versus initial 87Sr/86Sr. Symbols as in Figure 5. The unpatterned field (A) is the range of compositions in the net-veined dike (TF-74A, 74B, N16.05). Samples from pillowed dike (B) are connected by a tie line. The horizontally-hachured field is the range of compositions of the Velfjord plutons (Barnes et al., 2002). However, temperatures estimated on this basis result in values that are below the wet solidus (ca. 640°C), which Figure 7. indicates that biotite compositions were reset during cooling. Temperature was also estimated on the basis of Ti-in-zircon thermometry (Watson et al., 2006) with activities of SiO2 and TiO2 set to unity. A decrease in the activity of TiO2 to 0.9 would increase estimated T by 10–20°C. No pressure correction was applied (see discus­ sion in Fu et al., 2008). Temperature was calculated for each zircon that was used in the U–Pb age determin­ ations. Nineteen zircons separated from melanosome of the stromatic migmatite yielded an average temperature of 811 ± 24 °C and 11 zircons from the diatexite gave an average of 793 ± 30 °C. Some migmatitic samples contain the assemblage garnet + sillimanite + plagioclase + quartz, which permits the use of the GASP thermobarometer. Figure 8 shows the results of GASP calculations for five samples of the Upper Nappe: two from the Tosen road cut, two from Upper Nappe rocks sampled along Tosenfjord, and one collected ~20 km to the north in Størborja (Fig. 1C). If it is assumed that the Ti-in-zircon temperatures determined for the ~480 Ma zircons are representative of the T of melting, then intersection of this temperature range with the GASP equilibrium curves should provide an estimate Ordovician and Silurian magmatism in the Upper Nappe, Uppermost Allochthon, Helgeland 133 NORWEGIAN JOURNAL OF GEOLOGY of the pressure of melting. A further constraint on pressure is the observation that cordierite is present in many of the migmatite samples from the Upper Nappe, which restricts melting conditions to be at P lower than the biotite-sillimanite-garnet-cordierite-liquid equilibrium (Fig. 8). We conclude that partial melting of the Upper Nappe migmatites occurred between 500 and 700 MPa and ~800°C. These conditions are appropriate for biotite-­ dehydration melting (e.g., Patiño Douce and Johnston, 1991; Vielzeuf and Montel, 1994; Montel and Vielzeuf, 1997). Younger intrusive rocks. Pressure-temperature estimates for intrusive rocks were made on the basis of Al-in-hornblende thermobaro­ metry (Anderson and Smith, 1995). All of the analyzed amphibole has calculated Fe3+/(Fe3+ + Fe2+) > 0.20, which Schmidt (1992) considered acceptable for use with hornblende barometry. Anderson and Smith (1995) suggested that amphibole outside the Fetot/(Fetot + Mg) range of 0.40-0.65 should not be used for hornblende baro­metry. Two samples (TF-73, TF-17) contain amphibole that meet these criteria and contain the equilibrium assemb­lage of plagioclase, K-feldspar, quartz, hornblende, biotite, and Fe-Ti oxide (Hammarstrom and Zen, 1986; Hollister et al., 1987). For these calculations, rim compositions of amphibole and plagioclase were used with the pressure calibration of Anderson and Smith (1995) and the edenite–richterite T calibration of Holland and Blundy (1994). Sample TF-17 is from the 447 Ma quartz dioritic pluton at the east end of the outcrop. Hornblende-plagioclase pairs yielded a P estimate of 329 ± 44 MPa and a T estimate of 712 ± 19°C. Monzonite sample TF-73 is thought to be a hybrid between the monzonitic host and enclaves of the net-veined dike dated at 437 Ma (dated sample N16.05; Fig. 4G). The estimated pressure was 365 ± 37 MPa and the T estimate was 723 ± 12°C. This temperature estimate is consistent with the Ti-in-zircon temperature calculated from magmatic zircons from sample N16.05 of 747 ± 77 C. The peach-colored box in Figure 8 indicates the most likely P and T conditions of hornblende, plagioclase, and zircon equilibrium among these younger intrusive rocks. Discussion and Conclusions Timing and conditions of magmatism Bt Grt As K 01 VF2 L 99A 0.9 As rd L Bt G rt xC rd L C Grt As L Crd Kfs b sA G 0.7 0.8 = Fe/(Fe + Mg) of garnet in assemblage: Grt+Bt+As Grt+Bt+Crd Grt+Crd+As L Cr rt Ab Ms V Kfs As 600 d Bt 0.6 il tS Gr rd lC Sp Kf 200 fs L tK Gr d Bt Cr 0.8 andalusite 500 rt G sillimanite 400 Bt Op kyanite Opx As Grt Crd 5 1 VF2 VF1 0.9 Opx As L 0.6 0.7 fs Grt K Bt As 800 600 Ti in zircon T Ab fs L As L 8 Ms 0. Ms Ab V leucosome T NaKFMASH V Bt Grt dV Opx Cr 700 T (oC) 800 Figure 8. 900 Al-in-hornblende P (A & S) P (MPa) 1000 A Figure 8. P-T estimates. P-T grid for fluid-absent partial melting of pelitic compositions, after Spear et al. (1999). Colored curves are equilibrium conditions for five Upper Nappe samples with the GASP (garnet-sillimanite-silicaplagioclase) assemblage calculated using TWQ (Berman, 1988, 1990). The gray box indicates estimated conditions of migmatization determined on the basis of Ti-in-zircon thermometry of ~480 Ma zircons and the results of GASP calculations. The pink-shaded box indicates the results of Al-in-hornblende barometry and hornblende-plagioclase thermometry on 448 and 437 Ma intrusive rocks. Phase abbreviations are: Ms, muscovite; ab, albite; As, aluminosilicate; Kfs, K-feldspar; Bt, biotite; Grt, garnet; Opx, orthopyroxene; Crd, cordierite; Spl, spinel; Sil, sillimanite; L, silicate melt; V, aqueous fluid. We interpret the U-Pb data for the migmatites to indicate that partial melting of the Upper Nappe occurred at ~480 Ma. Melting occurred at ca. 500–700 MPa pressure (ca. 20–28 km depths) and ~800°C (Fig. 8), conditions consistent with biotite-dehydration melting (e.g., Vielzeuf & Holloway, 1988; Patino Douce & Johnston, 1991; Vielzeuf & Montel, 1994; Montel & Vielzeuf, 1997). Under these conditions, enough melt was produced to allow for mobilization of melt-rich parts of the migmatite to form cross-cutting diatexites. It is noteworthy that the diatexitic rocks are chemically more refractory than the stromatic migmatites (i.e., diatexites have lower SiO2 and higher TiO2, CaO, total Fe). This chemical difference indicates that although the diatexites may have initi­ ally had larger proportions of melt than the stromatic migma­tites, melt was lost during or after emplacement. There is no field or geochemical evidence that migmati­ zation was accompanied by mafic magmatism, at least at the level of exposure. This leaves the source of heat for ca. 480 Ma crustal melting in the Upper Nappe, and elsewhere in the HNC, an unanswered question. The next magmatic event recorded in the study area was emplacement of the small quartz dioritic pluton at 448 Ma. The age of this pluton is identical to larger plutons that intrude the underlying nappes of the HNC, specifically the Velfjord plutons ~10 km to the west and northwest (Fig. 1B, C; Barnes et al., 1992, 2004). The quartz diorite is distinct from these plutons in having signifi­ cantly higher initial 87Sr/86Sr values (Fig. 7) and also in its calc-alkalic (versus alkali-calcic to alkalic) compositions at comparable SiO2 contents. These distinctions 134 C. G. Barnes et al. NORWEGIAN JOURNAL OF GEOLOGY suggest that the quartz dioritic magma either had a distinct source or underwent significant crustal contamination compared to the Velfjord plutons. et al., 2007). Evidently, middle Ordovician metamorphism and local crustal melting occurred throughout the HNC in response to nappe amalgamation (Barnes et al., 2007). The various dikes with ages from 437–432 Ma are noteworthy because of the wide range of bulk compositions, from gabbroic to granitic. The abundance of mingled dikes among the 437–432 Ma dikes shows that mafic and felsic magmas coexisted in this time range. Overall, these rocks are metaluminous to weakly peraluminous and have low initial 87Sr/86Sr compared to the migmatites and 448 Ma quartz diorite (Figs. 5, 7). There is no correlation between the chemical composition (e.g., SiO2 content) and isotope ratios and among the rocks with SiO2 >71 wt %, i.e. rock types that range from tonalite to granite (2.5 to 7.0 wt % K2O), with no correlation of SiO2 with K2O. Nevertheless, most samples have small negative Eu anomalies (Fig. 6) and mafic–intermediate rocks have high (>1000 ppm) Sr contents (Fig. 5). These observations suggest that the various 437–432 Ma dikes are not related by differentiation of a single, evolving magma, but instead arise from a deep-seated source region in which isotopic compositions vary within a narrow range but major element concentrations can vary significantly. Specifically the combination of low initial 87Sr/86Sr, high Sr contents and lack of correlation between Sr and differentiation among intermediate and mafic rocks, small, uniform Eu anomalies, and low alumina saturation index is suggestive of magma generation or differentiation under conditions where plagioclase fractionation was minor, consistent with lower crustal conditions. Although anatexis in the Upper Nappe occurred at ~700 MPa pressure, by the 448 Ma emplacement of the quartz dioritic pluton the Upper Nappe rocks were at a pressure of ~300 MPa. Similar amounts of exhumation have been documented in the Velfjord region (Barnes and Prestvik, 2000) and at Vega (Marko et al., 2007; Oalmann, 2010). In Velfjord, exhumation was interpreted to occur during and after emplacement of ca. 448–445 Ma plutons (Barnes and Prestvik, 2000; Yoshinobu et al., 2002), whereas exhumation preceded the 448 Ma magmatism at Tosenfjord. The age of exhumation at Vega is uncertain, but may have been as old as 475 Ma (Marko et al. 2007). Evidently, although high-grade metamorphism was coeval across the HNC, exhumation was diachronous. In contrast, the young 424 Ma granitic dike has much higher initial 87Sr/86Sr and lower εNd than the 437–432 Ma dikes, suggesting a distinct source for this youngest magma batch. The low HREE of this granite (Fig. 6D) indicates residual garnet in the source, which is in contrast to nearly all of the older dikes. It is noteworthy that although the 424 Ma granite displays a garnet REE signature, it is only slightly peraluminous, which rules out an origin by partial melting of typical metapelitic rocks in the HNC (e.g., Nordgulen and Sundvoll, 1992; Barnes et al.2002). Several of the ca. 437–432 Ma dikes are foliated, including mingled dikes in which mafic enclaves underwent sub-solidus deformation (Appendix 1), and the ~437 Ma net-veined rocks are cut by a shear zone with reversesense (top-to-west) displacement. In contrast, the 424 Ma granitic dikes show no evidence of sub-solidus deformation. Evidently, magma emplacement at ca. 435 Ma was accompanied by local penetrative deformation, at least some of which was contractional. Relationship to regional geology The age of migmatization of the Upper Nappe at~ 480 Ma is essentially identical to that of migmatization in the Horta and Lower Nappes (Yoshinobu et al., 2002; Barnes The work of Nordgulen and colleagues (Nordgulen, 1993; Nordgulen et al., 1993; Yoshinobu et al., 2002; Barnes et al., 2007) have shown that the earliest plutons in the Bindal Batholith (478–475 Ma) are restricted to the western HNC and that plutons from 467–444 Ma crop out primarily in the central and western parts of the nappe complex. In contrast, plutonic rocks in the 440– 430 Ma age range crop out across the HNC, from the westernmost exposures (e.g., Sklinna pluton; Barnes et al., 2007) to the easternmost ones (Nissen et al., 2006). This change from early, relatively focused magmatic activity to later, widespread magmatism in the HNC may be related to changes in tectonic environment (contraction versus extension), dip of a subducting slab (older steep dip to younger shallow dip), or to the development of a slab window in early Silurian time and initiation of the Scandian collision. The possibilities can only be resolved with further detailed petrological and geochronological study of the HNC. Acknowledgments. - We thank Øystein Nordgulen for bringing this exceptional exposure to our attention and for his geologic insights on HNC geology. S. Swapp provided able assistance with the microprobe analyses. We also thank H. Schiellerup and R. Larsen for their thoughtful reviews. This research was supported by NSF grant EAR9814280 and by the Norwegian Geological Survey. Electronic Appendix Tables Table 1. U-Pb age data determined by LA-ICP-MS Table 2. U-Pb age data determined by SHRIMP-RG. Table 3. Representative major and trace element analyses Table 4. Nd and Sr isotope data. Table 5. Representative garnet analyses. Table 6. Representative hornblende analyses. Table 7. Representative biotite analyses. Table 8. Representative plagioclase analyses. Table 9. Clinopyroxene analyses. NORWEGIAN JOURNAL OF GEOLOGY Ordovician and Silurian magmatism in the Upper Nappe, Uppermost Allochthon, Helgeland 135 References Cited Anderson, H.S., Yoshinobu, A.S., Chamberlain, K., Nordgulen, Ø. & Barnes, C.G. 2008: Magma Emplacement and the Development of Ghost Stratigraphy in the Andalshatten Pluton, Central Norway. Geological Society of America Abstracts with Programs, 40, # 6, 251 Anderson, J. L. & Smith, D. R. 1995: The effects of temperature and fO2 on the Al-in-hornblende barometer. American Mineralogist 80, 549–559. Barnes, C. G. & Prestvik, T. 2000: Conditions of pluton emplacement and anatexis in the Caledonian Bindal Batholith, north-central Norway. 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Geology 30, 883–886. NORWEGIAN JOURNAL OF GEOLOGY