Structure Physics Group

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Structure Physics Group
Structure Physics aims for fundamental insight into the
electronic and geometric structure of nanomaterials
Functional Energy Related
Materials in Oslo (FERMiO)
Members of the Structure Physics Group
PhD students
Permanent academic
Clas Person, Professor
Arne Olsen, Professor
Anette E. Gunnæs, Ass. Prof.
Øystein Prytz, Ass. Prof.
Adjunct academic staff
Sabrina Sartori, IFE
Bjørn Hauback, IFE
Martin Kirkengen, IFE
Vidar Hansen, UiS
Ole Martin Løvvik, SINTEF
Annett Thøgersen, SINTEF
Girma Gardew
Song Xin (Terje)
Per Harald Ninive, HiG
Wei Zhan
Asbjørn Skogstad
NN (THELMA)
2 x NN (FOXHOUND)
Master students
Andrey Kosinskiy
Kenneth Kjeverud Strand
Martin Normann
Raluca Tofan
Sindre Wiken Langfeldt
Knut Overskeid
Aidan Von Bonin
Mauro Povia
Technical
Ole Bjørn Karlsen, senior
Stefano Rubino, head
Researchers
Kjetil Valset
Espen Flage-Larsen, SINTEF
Dan Phoung Nguyen
Professor emeritus
Johan Taftø
Jon Gjønnes
Tore Amundsen
Permanent and adjunct sientific staff 2013
Experimental
Synthesis
Anette
Theory
Clas
Annett
SINTEF
Sabrina
IFE
Ole Martin
SINTEF
Stefano
Arne
Øystein
David
Ole Bjørn
Vidar UiS
Bjørn IFE
Permanent and adjunct sientific staff Jan. 2014
Experimental
Synthesis
Anette
Theory
Clas
Annett
SINTEF
Sabrina
IFE
Ole Martin
SINTEF
Stefano
Arne
Øystein
Ole Bjørn
Vidar UiS
Bjørn IFE
Permanent and adjunct sientific staff 2015
Experimental
Synthesis
Anette
Theory
Clas
Annett
SINTEF
Sabrina
IFE
Ole Martin
SINTEF
NN
NN
Øystein
NN
Ole Bjørn
Vidar UiS
Bjørn IFE
Halvleder
fysikk
FASE
SINTEF
Struktur
Katalyse
BATE
IFE
UiS
The Basic and Applied Thermo Electrics inititative
Industri
Internationale
samarbeids
partnere
NORTEM
The Norwegian Centre for Transmission Electron Microscopy
VISION OF NORTEM
A world-class TEM centre providing access to expertise and
state-of-the-art infrastructure for fundamental and applied
research within the physical sciences in Norway.
Miljøene bak NORTEM
TEM Gemini Centre
Trondheim
Department
of Physics
Department of Materials
Science and Engineering
SINTEF Synthesis
and Properties
Oslo
Physics
Department
SMN
NTNU
SINTEF
UiO
NORTEM
Instrumentation
Level 1: State-of-the-art instrument
Projects owned or planned by NORTEM research groups, include
competence and technique development.
External users will not generally operate these instruments.
Level 2: Advanced instrument
Operators with agreed needs get access after
sufficient training and skills. Formalized training
maintains quality and ensures effective use.
Level 3: Standardized and routine TEM
Many users require hands-on access to perform simple tasks, where
analysis is routine or TEM is a minor activity in a project.
Once a specific task is approved, users can be trained.
NORTEM
Instrumentation- level 1 and 2
Oslo-node
TITAN G2 60-300 kV
With probe corrector and
monochromator
JEM 2100F
UHR pole piece
New, latest generation GIF
NORAN detector
Holography
Trondheim-node
JEM ARM200F
Cold FEG and
double corrected
JEM 2100F
HR pole piece
Moving GIF, US CCD,
ASTAR, tomography and
Oxford EDS from 2010F
JEM 2100F
TITAN G2 60-300 kV
What is possible..
High energy resolution electron energy-loss experiments
(EELS)
What is possible ..
Better resolution in STEM;
Aberration
correction on the
probe forming lens
Cu-containing precipitates in Al-Mg-Si-Cu alloys (Calin Marioara, SINTEF,
right image taken at Titan Cs corrected microscope in CEN-DTU, Chris Boothroyd
What is possible..
Better resolution in STEM;
a
5 nm
Aberration
correction on the
probe forming lens
b
2 nm
HRSTEM of a GaAs nanorod with Sb insertion. HAADF images from a) 2010F (Trondheim) and b)
JEOL ARM200F probe corrected taken at JEOL research Centre, Tokyo, Japan Oct 09 by E.
Okunishi. Bottom part in both figures is the same crystal structure, but only probe corrected match
the structure simulation (insert in b)) Unpublished data. Courtesy, T. van Helvoort, NTNU.
What is possible..
Larger EDS detection
angle, often combined
with several detectors
and brighter sources
Atomic chemical mapping
(from FEI brochure)
Prøveholdere
•Vippe langs en og to akser
•Varmeholdere
•Kjøleholdere (Nitrogen)
•ETEM
ETEM
Gass in-situ ekperimenter
Catalysis
Hummingbird
Hummingbird's Atmospheric Gas Flow TEM Holder
allows in-situ observation of the interaction of
materials with a gaseous environment under relevant
conditions. The effect of gaseous overpressure on the
physical properties of a material can be observed in real
time during an experiment. High resolution imaging of
active catalystic nano-particles will provide a deeper
understanding of these materials.
Thin Film Research
Gold nano-particles in 1.1 atm of nitrogen gas, showing
atomic scale resolution.
From: FEI Titan at 300kV by Hummingbird Scientific.
A TiN thin film at 500°C in 1.1 atm
nitrogen.
From: 300 kV FEI corrected Titan in
BF mode.
ETEM
Væske in-situ ekperimenter
Hummingbird
Biomedical & Biological Imaging
Hummingbird Scientific's continuous-flow TEM fluid holder initiates new groundbreaking capabilities to interrogate and image
biological processes using TEM by enabling dynamic imaging of biological materials in their native liquid environments. This
includes fundamental sequence, structure and function studies, as well as single-cell targeting, micro/nanobubble studies, and
insight into in vitro constitution and protein recombination.
Fluidics
The combined usage of TEM and nanomarkers allows direct observation and particle
tracking inside fluid flows with resolutions up to 1 nm which will ultimately lead to
elucidation of questions concerning boundary layer studies and particle velocimetry.
Materials and Chemical Science
Imaging nanostructures in liquid environments enables an increased
understanding of nano-particle synthesis and assembly. Additionally,
corrosion processes and catalytic reactions can be studied.
Energy Conversion Processes
Hummingbird Scientific's liquid holder enables in-situ imaging of electrochemical
reactions in fuel cells and batteries as they are occurring.
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