Structure Physics Group Structure Physics aims for fundamental insight into the electronic and geometric structure of nanomaterials Functional Energy Related Materials in Oslo (FERMiO) Members of the Structure Physics Group PhD students Permanent academic Clas Person, Professor Arne Olsen, Professor Anette E. Gunnæs, Ass. Prof. Øystein Prytz, Ass. Prof. Adjunct academic staff Sabrina Sartori, IFE Bjørn Hauback, IFE Martin Kirkengen, IFE Vidar Hansen, UiS Ole Martin Løvvik, SINTEF Annett Thøgersen, SINTEF Girma Gardew Song Xin (Terje) Per Harald Ninive, HiG Wei Zhan Asbjørn Skogstad NN (THELMA) 2 x NN (FOXHOUND) Master students Andrey Kosinskiy Kenneth Kjeverud Strand Martin Normann Raluca Tofan Sindre Wiken Langfeldt Knut Overskeid Aidan Von Bonin Mauro Povia Technical Ole Bjørn Karlsen, senior Stefano Rubino, head Researchers Kjetil Valset Espen Flage-Larsen, SINTEF Dan Phoung Nguyen Professor emeritus Johan Taftø Jon Gjønnes Tore Amundsen Permanent and adjunct sientific staff 2013 Experimental Synthesis Anette Theory Clas Annett SINTEF Sabrina IFE Ole Martin SINTEF Stefano Arne Øystein David Ole Bjørn Vidar UiS Bjørn IFE Permanent and adjunct sientific staff Jan. 2014 Experimental Synthesis Anette Theory Clas Annett SINTEF Sabrina IFE Ole Martin SINTEF Stefano Arne Øystein Ole Bjørn Vidar UiS Bjørn IFE Permanent and adjunct sientific staff 2015 Experimental Synthesis Anette Theory Clas Annett SINTEF Sabrina IFE Ole Martin SINTEF NN NN Øystein NN Ole Bjørn Vidar UiS Bjørn IFE Halvleder fysikk FASE SINTEF Struktur Katalyse BATE IFE UiS The Basic and Applied Thermo Electrics inititative Industri Internationale samarbeids partnere NORTEM The Norwegian Centre for Transmission Electron Microscopy VISION OF NORTEM A world-class TEM centre providing access to expertise and state-of-the-art infrastructure for fundamental and applied research within the physical sciences in Norway. Miljøene bak NORTEM TEM Gemini Centre Trondheim Department of Physics Department of Materials Science and Engineering SINTEF Synthesis and Properties Oslo Physics Department SMN NTNU SINTEF UiO NORTEM Instrumentation Level 1: State-of-the-art instrument Projects owned or planned by NORTEM research groups, include competence and technique development. External users will not generally operate these instruments. Level 2: Advanced instrument Operators with agreed needs get access after sufficient training and skills. Formalized training maintains quality and ensures effective use. Level 3: Standardized and routine TEM Many users require hands-on access to perform simple tasks, where analysis is routine or TEM is a minor activity in a project. Once a specific task is approved, users can be trained. NORTEM Instrumentation- level 1 and 2 Oslo-node TITAN G2 60-300 kV With probe corrector and monochromator JEM 2100F UHR pole piece New, latest generation GIF NORAN detector Holography Trondheim-node JEM ARM200F Cold FEG and double corrected JEM 2100F HR pole piece Moving GIF, US CCD, ASTAR, tomography and Oxford EDS from 2010F JEM 2100F TITAN G2 60-300 kV What is possible.. High energy resolution electron energy-loss experiments (EELS) What is possible .. Better resolution in STEM; Aberration correction on the probe forming lens Cu-containing precipitates in Al-Mg-Si-Cu alloys (Calin Marioara, SINTEF, right image taken at Titan Cs corrected microscope in CEN-DTU, Chris Boothroyd What is possible.. Better resolution in STEM; a 5 nm Aberration correction on the probe forming lens b 2 nm HRSTEM of a GaAs nanorod with Sb insertion. HAADF images from a) 2010F (Trondheim) and b) JEOL ARM200F probe corrected taken at JEOL research Centre, Tokyo, Japan Oct 09 by E. Okunishi. Bottom part in both figures is the same crystal structure, but only probe corrected match the structure simulation (insert in b)) Unpublished data. Courtesy, T. van Helvoort, NTNU. What is possible.. Larger EDS detection angle, often combined with several detectors and brighter sources Atomic chemical mapping (from FEI brochure) Prøveholdere •Vippe langs en og to akser •Varmeholdere •Kjøleholdere (Nitrogen) •ETEM ETEM Gass in-situ ekperimenter Catalysis Hummingbird Hummingbird's Atmospheric Gas Flow TEM Holder allows in-situ observation of the interaction of materials with a gaseous environment under relevant conditions. The effect of gaseous overpressure on the physical properties of a material can be observed in real time during an experiment. High resolution imaging of active catalystic nano-particles will provide a deeper understanding of these materials. Thin Film Research Gold nano-particles in 1.1 atm of nitrogen gas, showing atomic scale resolution. From: FEI Titan at 300kV by Hummingbird Scientific. A TiN thin film at 500°C in 1.1 atm nitrogen. From: 300 kV FEI corrected Titan in BF mode. ETEM Væske in-situ ekperimenter Hummingbird Biomedical & Biological Imaging Hummingbird Scientific's continuous-flow TEM fluid holder initiates new groundbreaking capabilities to interrogate and image biological processes using TEM by enabling dynamic imaging of biological materials in their native liquid environments. This includes fundamental sequence, structure and function studies, as well as single-cell targeting, micro/nanobubble studies, and insight into in vitro constitution and protein recombination. Fluidics The combined usage of TEM and nanomarkers allows direct observation and particle tracking inside fluid flows with resolutions up to 1 nm which will ultimately lead to elucidation of questions concerning boundary layer studies and particle velocimetry. Materials and Chemical Science Imaging nanostructures in liquid environments enables an increased understanding of nano-particle synthesis and assembly. Additionally, corrosion processes and catalytic reactions can be studied. Energy Conversion Processes Hummingbird Scientific's liquid holder enables in-situ imaging of electrochemical reactions in fuel cells and batteries as they are occurring.