Characterization of Nb 3 Sn Superconducting Strand Under Pure Bending by David L. Harris B.S. Mechanical Engineering (2003) Utah State University Submitted to the Department of Mechanical Engineering in Partial Fulfillment of the Requirements for the Degree of Master of Science in Mechanical Engineering at the Massachusetts Institute of Technology September 2005 0 2005 Massachusetts Institute of Technology All right reserved Signature of Author ..................................... Department of Mechanical Engineering August 10, 2005 Cr-tified bIy ..................... ... ..... .......... ... . .. . . Joseph V. Minervini Senior Research Engineer, MIT Plasma Science and Fusion Center Nuclear Science and Engineering Department Thesis Supervisor ..................... ivseph L. Smith, Jr. Samuel C. Collins Seniorjfpfessor of Mechanical Engineering Thesis Supervisor Certified by .................. Accepted by ............... ............ ...... ........... Lallit Anand Chairman, Department Committee on Graduate Students MASSACHUSETTS INSTITU E OF TECHNOLOGY NOV 0 7 2005 LIBRARIES BARKER 2 Characterization of Nb 3 Sn Superconducting Strand Under Pure Bending by David L. Harris Submitted to the Department of Mechanical Engineering on August 10, 2005 in Partial Fulfillment of the Requirements for the Degree of Master of Science in Mechanical Engineering ABSTRACT Characterizing the strain-dependent behavior of technological Nb 3Sn superconducting strand has been an important subject of research for the past 25 years. Most of the effort has focused on understanding the uniaxial tension and compression effects and applying this information to improve predictive scaling laws which are used for superconducting magnet design. However, the strain state of the strand in an actual magnet winding is often a complicated combination which includes uniaxial tension or compression, bending, and transverse compression. A bending mechanism was designed and used to characterize the bending strain behavior of two different types of Nb 3Sn superconducting strand at 4.2K in a magnetic field. Results showed that the critical current of the strand increased up to an applied bending strain between 0.2-0.3% and then decreased with continued applied strain. Thesis Supervisor: Joseph V. Minervini Title: Senior Research Engineer, MIT Plasma Science and Fusion Center 4 ACKNOWLEDGEMENTS I want to express my gratitude to all those who contributed both directly and indirectly to this thesis. Specifically, I want to thank my advisor, Dr. Joseph V. Minervini for his mentorship and guidance. He always made himself available when I had a question or concern. I am grateful for the many hours that Dr. Makoto Takayasu invested in helping me. I learned much from working with him. I am indebted to Professor Joseph L. Smith, Luisa Chiesa, Dave Tracey, Darlene Marble, and Fred Cote for all of their assistance. I am very grateful for my wife, Ellen, and her encouragement and support. And to my children who always make me smile. My work and schooling was supported by a National Defense Science and Engineering Graduate (NDSEG) Fellowship which was sponsored by the Department of Defense. A portion of this work was performed at the National High Magnetic Field Laboratory, which is supported by NSF Cooperative Agreement No. DMR-0084173, by the State of Florida, and by the DOE. 6 Table of Contents Title P ag e ...................................................................................................... 1 ABSTRACT .................................................................. 3 A cknowledgem ents ................................................................................ ... . .. 5 T able of Contents ........................................................................................ . .7 L ist of F igures ................................................................... . 11 17 L ist o f T ab les ................................................................................................ . . 19 Glossary of T erm s ...................................................................................... C h apter 1. Intro du ction .................................................................................... 23 1.1 History ...................................................................................... . . 23 25 1.2 Type II Superconductors ................................................................... 1.2.1 Theories of Superconductivity ................................................. 1.3 Superconductor Development ............................... 29 ....... 30 1.4 Production of Nb3Sn Strand ..................................... 35 1.5 Cable-in-Conduit Conductor (CICC) ........................................................ 40 1.6 Strain Behavior of Nb 3Sn ................................................................. 46 1.6.1 Uniaxial Strain .................................................................. . 47 1.6.2 Strain Scaling L aws ................................................................ 52 1.6.3 Compound Strain ............................................................... 54 1.7 Thesis Objective ........................................................................... Chapter 2. Analytical Development ................................................................... . 58 59 2.1 M echanics of M aterials ........................................................................ 59 2.2 Example Nb 3Sn Strand Bending .......................................................... 64 2.3 Differential Equation Approach to Large-Displacement Bending ................... 67 8 2.4 Geometric Verification of Pure Bending Relationship ................................ 75 2.5 Error Minim ization ............................................................................ 78 . 85 Chapter 3. Design ....................................................................................... 3.1 Operating Conditions and Requirements ............................... 85 3.2 B en ding O peration ............................................................................. 91 3.3 Test Sample Mounting System ........................................................... 95 96 3.3.1 Support Beam ........................................ 3.3 .2 C urrent Joints ...................................................................... 103 3.4 Strand H eat Treatm ent ....................................................................... 105 3.5 Mechanism Gear Design ... 109 .................................... 3 .6 P rob e Design .................................................................................. Chapter 4. Specifications and Test Results ............................................................ 1 14 119 4.1 M echanism Specifications ................................................................. 119 4.2 Support Beam Specifications ............................................................... 124 4 .3 S train Gag es ................................................................................... 12 7 4.4 Bending Mechanism Verification ................................. 129 4.4.1 Room Temperature Verification ............................................... 133 4.4.2 Liquid Helium Verification ............................... 135 4.5 NHMFL Facilities ........................................... 137 4.6 Sam ple Test Preparation ..................................................................... 140 4.7 Sam ple Characterization ..................................................................... 146 4.8 Critical Current Results .................................................................... 148 4.9 Bending Results .......................... ..................... 160 4 .10 S am p le Strain .................................................................... ........... 167 4.11 Conclusion ................................................................. 176 4.12 Recommendations ................................................ 177 9 APPENDIX A. Bending Error Estimates .............................................................. 181 APPENDIX B. Gear and Spline Calculations ......................................................... 189 A PPEN DIX C . Draw ings ................................................................................ 195 A PPEN DIX D . Photos ................................................................................... 22 1 APPENDIX E. Strand Heat Treatment ................................................................. 235 APPENDIX F. Critical Current Test Results .......................................................... 241 Referen ces ................................................................................................... 24 7 10 List of Figures Fig. 1.1. Critical superconductive surface ........................................................... 24 Fig. 1.2. Dissipative flux motion in a Type H superconductor .................................... 26 Fig. 1.3. (a) Flux penetration in a Type II superconductor, and (b) picture of actual flux lattice ............................................................. 27 Fig. 1.4. Flux pinning force comparison ............................................................. 28 Fig. 1.5. (a) Bronze billet pattern, and (b) Multifilament drawing process ......................... 36 Fig. 1.6. Picture of bronze process strand ........................................................... 37 Fig. 1.7. (a) Internal Tin billet, and (b) Picture of unreacted Internal Tin strand ............... 38 Fig. 1.8. External tin billet arrangem ent ............................................................. 38 Fig. 1.9. Twisting of superconducting strand .......................................... 39 Fig. 1.10. ITER Central Solenoid Model Coil Conductor ......................................... 41 Fig. 1.11. CICC cross-section view showing a series of internal magnification stages ........... 42 Fig. 1.12. Computer model of ITER (International Thermonuclear Experimental Reactor) ..... 44 Fig. 1.13. Strain dependent critical current in the 45T Hybrid magnet strand at 12T and 4.2K ........ ............................................... 47 Fig. 1.14. Reduced critical current vs. intrinsic strain for OST internal tin wire ............. 48 Fig. 1.15. U-spring strain device used at the University of Twente ................................. 49 Fig. 1.16. Pacman strain device used at the University of Twente ................................ 50 Fig. 1.17. The Walters Spring (WASP) device for measuring critical current as a function of strain ....................................................................... . 51 Fig. 1.18. Ekin transverse strain mechanism ........................................................ 55 Fig. 1.19. TARSIS periodical bending device .......................................................... 56 Fig. 1.20. Fixed bending strain behavior strand configuration ...................... 57 Fig. 2.1. B eam in pure bending ........................................................................ 60 Fig. 2.2. Deformation of a beam in pure bending: (a) side view of beam, (b) deformed beam ................... ......................... 61 Fig. 2.3. Scaled drawing of example strand at maximum strain state ............................ 66 12 Fig. 2.4. (a) Evolution of a beam through pure bending states, and (b) Pure bending is independent of symmetric vertical motion ............................ 68 Fig. 2.5. (a) Initially straight beam with rigid clamps, (b) Deformed beam, and (c) H alf beam with sym m etry .............................................................. 71 Fig. 2.6. Pure bending motion of beam ends for the example strand ................................ 75 Fig. 2.7. Beam deformed into a state of pure bending .............................................. 76 Fig. 2.8. (a) Side view of circular-type bending mechanism, and (b) top view of circular-type bending mechanism ....................................... 78 Fig. 2.9. Displacement at the beam end due to the lever arms ................................... 79 Fig. 2.10. Plot of nondimensional bending displacement error ...................... 83 Fig. 3.1. Drawing of the 195mm bore, 20T Bitter resistive magnet and cryostat at the National High Magnetic Field Laboratory (NHMFL) in Tallahassee, FL ................ 86 Fig. 3.2. Bending mechansim (a) complete mechanism, (b) with strand mounting system removed, and (c) inner gear train ................................... 92 Fig. 3.3. Bending Mechanism Operation (a) 00 rotation angle, (b) 200 rotation angle, (c) 400 rotation angle, and (d) 700 rotation angle for the Torque Arms .......... 94 Fig. 3.4. Strand Mounting System ............................................. 95 Fig. 3.5. Support Beam Layout (a) Front View and (b) Back View ...................... 97 Fig. 3.6. Stress-strain curves for Ti6A14V annealed 0.064 inch sheet at various temperatures ................................................................................... Fig. 3.7. Support Beam and test strand distances from neutral axis to outer surfaces ... .... . 99 100 Fig. 3.8. Current joint design with (a) All Components, and (b) Cut-Away View ............... 104 Fig. 3.9. Strand Heat Treatment Fixture, (a) Fixture and Cap, (b) Main Fixture ..... ..... 106 Fig. 3.10. Detail of heat treatm ent fixture end ......................................................... 108 Fig. 3.11. Bending Mechanism ............................................... 109 Fig. 3.12. Bending Mechanism Gear Train .................................. 111 Fig . 3 .13 . Prob e design ................................................................................... 115 Fig. 3.14. Drawings of (a) cryostat, and (b) probe. All dimensions are in inches ................ 116 Fig. 4.1. Bending mechanism (a) with removable Torque Arms and (b) gear train ......... 120 13 Fig. 4.2. Sample mounting assembly for OST (Eurpean) strand withf= 1.53 ................... 122 Fig. 4.3. (a) Current Joint mounting configuration, and (b) sample current-joint groove ...... 123 Fig. 4.4. Position of sample in Support Beam ......................................................... 125 Fig. 4.5. (a) Sample side of the Support Beam, and (b) end of Support Beam showing compensating grooves ............................................................... Fig. 4.6. Room temperature test of bending mechanism ............................................. 126 133 Fig. 4.7. Permanent deformation of Support Beam tested at room temperature .................. 134 Fig. 4.8. Probe and cryostat for the liquid helium bending mechanism verification test ........ 135 Fig. 4.9. Support Beam tested in liquid helium bath ................................................. 136 Fig. 4.10. Cell 4 at the National High Magnetic Field Laboratory ............ 137 .............. Fig. 4.11. Screen shot of testing control computer ................................................... 138 Fig. 4.12. B ending test probe ............................................................................ 140 Fig. 4.13. Bending Mechanism and Sample Assembly attached to probe ......................... 141 Fig. 4.14. Flexible current lead wires .................................................................. 142 Fig. 4.15. (a) Attachment points for current lead wires, and (b) attached current lead wires ... 143 Fig. 4.16. Probe mounted on magnet cryostat ......................................... 144 Fig. 4.17. Transferring liquid helium to the cryostat via the probe ................................. 145 Fig. 4.18. Voltage-current plots for IGC 157 Sample #1 (a) 0.2% strain, and (b ) 0 .1% strain ................................................................................. 150 Fig. 4.19. (a) Current data, and (b) n-values for IGC 157 Sample #1 .............................. 153 Fig. 4.20. (a) Current data, and (b) n-values for IGC 157 Sample #2 .............................. 154 Fig. 4.21. (a) Current data, and (b) n-values for IGC 157 Sample #3 .............................. 155 Fig. 4.22. (a) Current data, and (b) n-values for EU 153 Sample #1 ............................... 156 Fig. 4.23. (a) Current data, and (b) n-values for EU 153 Sample #2 ............................... 157 Fig. 4.24. (a) Current data, and (b) n-values for EU 153 Sample #3 ............................... 158 Fig. 4.25. Measured bending strain for (a) IGC 157, and (b) EU153 beams ....................... 162 Fig. 4.26. Bending strain error for (a) IGC157, and (b) EU153 beams ............................ 164 Fig. 4.27. Effect of Lorentz load on bending strain for (a) IGC 157, and (b) EU 53 b eams .............................................................................. 166 14 Fig. 4.28. EUl 53 test samples (a) before testing, and (b) after testing ............................. 168 Fig. 4.29. Offset between beam neutral axis and strand centerline 170 ................... Fig. 4.30. Conceptual method for adding tensile strains to bending strain ........................ 174 Fig. 4.31. Bearing surface of bending mechanism Input Shaft ...................................... 179 Fig. A. 1. (a) Beam with uniform load and fixed supports, and (b) moment distribution ........ 187 Fig. C.1. B ending m echanism model ................................................................... 195 Fig. C.2. Bending Mechanism Parts List ................................... 196 Fig. C.3. Bending Mechanism Bottom Plate, Part No. PBD-001-001 ................. 197 Fig. C.4. Bending Mechanism Top Plate, Part No. PBD-001-002 ................... 198 Fig. C.5. Torque Gear A, Part No. PBD-001-003 ..................................................... 199 Fig. C.6. Torque Gear B, Part No. PBD-001-004 .............................. 200 Fig. C.7. Drive Shaft, Part No. PBD-001-005 ......................................................... 201 Fig. C.8. Input Shaft, Part No. PBD-001 -006 ......................................................... 202 Fig. C.9. Torque Arm 153, Part No. PBD-001-007 ................................................... 203 Fig. C.10. Torque Arm 157, Part No. PBD-001-008 ................................................. 204 Fig. C. 11. Beam Clamp A, Part No. PBD-001-009 ................................................... 205 Fig. C.12. Beam Clamp B, Part No. PBD-001-010 ............................. 206 Fig. C. 13. Beam Clamp C, Part No. PBD-001-01I ................................................... 207 Fig. C. 14. Beam Clamp D, Part No. PBD-001-012 ................................................... 208 Fig. C.15. Thrust Bearing, Part No. PBD-001-013 .................................................. 209 Fig. C .16. Plate Spacer, PBD -001-014 ................................................................. 210 Fig. C.17. Shaft Coupler, Part No. PBD-001-015 .................................................... 211 Fig. C.18. Support Beam 153, Part No. PBD-001-016 .............................................. 212 Fig. C.19. Support Beam 157, Part No. PBD-001-017 .............................................. 213 Fig. C.20. Probe model ............................................... 214 F ig . C .2 1. Prob e p arts list ................................................................................ 2 15 Fig. C.22. Flange Plate, Part No. PBD-002-001 ..................................................... 216 Fig. C.23. Large Probe Plate, Part No. PBD-002-002 ................................................ 217 Fig. C.24. Upper Small Probe Plate, PBD-002-003 .................................................. 218 15 Fig. C.25. Lower Small Probe Plate, Part No. PBD-002-004 ........................ 219 Fig. D.1. Bending Mechanism .............................................. 221 Fig. D.2. Bending mechanism gear train .............................................................. 222 Fig. D.3. Bottom Plate, Part No. PBD-001-001 ...................................................... 223 Fig. D.4. Top Plate, Part No. PBD-001-002 ........................................................... 224 Fig. D.5. Torque Gear A & B, Part No. PBD-001-003 & PBD-001-004 .......................... 225 Fig. D.6. Drive Shaft, Part No. PBD-001-005 ......................................................... 226 Fig. D.7. Input Shaft, Part No. PBD-001 -006 ......................................................... 226 Fig. D.8. Torque Arm 153, Part No. PBD-001-007 .................................... 227 Fig. D.9. Front View, Support Beam 157, Part No. PBD-001-017 ................................ 227 Fig. D.10. Back View, Support Beam 157, Part No. PBD-001-017 ................................ 228 Fig. D.11. Machining Support Beam 157 ...................................... 228 Fig. D.12. Beam Clamp C, Part No. PBD-001-011 ................................................... 229 Fig. D.13. Beam Clamp D, Part No. PBD-001-012 ................................................... 229 Fig. D .14. Top portion of Probe ......................................................................... 230 Fig. D .15. Probe prepared for testing ................................................................... 231 Fig. D.16. Flange Plate, Part No. PBD-002-001 ...................................................... 232 Fig. D. 17. Flange Insulating Plate, Part No. PBD-002-005 ................... .................... 232 Fig. D.18. Large Probe Plate, Part No. PBD-002-002 ................................................ 233 Fig. D.19. Upper Small Probe Plate, Part No. PBD-002-003 ....................................... 233 Fig. D.20. Lower Small Probe Plate, Part No. PBD-002-004 .............. .................. 234 Fig. D.21. Bending Mechanism Insulating Plate, Part No. PBD-002-011 ........................ 234 Fig. E. 1. Furnace for heat treating IGC samples ...................................................... 237 Fig. E.2. Furnace for heat treating OST samples ...................................................... 237 Fig. E.3. Sample heat treatment fixture made from Ti6A14V ....................................... 238 Fig. E.4. Heat treatment fixture and cap coated with Graphokote to prevent sintering .......... 238 Fig. E.5. Grooves machined in sample heat treatment fixture ....................................... 238 Fig. E.6. Heat treatment fixture after removing from furnace ....................................... 239 Fig. E.7. Sam ples after heat treatm ent .................................................................. 239 16 Fig. E.8. Samples are one continuous strand .......................................................... 240 Fig. E.9. Removing samples from fixture .............................................................. 240 List of Tables Table 1.1 Timeline for Nb3Sn conductor development ............................................. 31 Table 2.1 Summary of the example strand specifications ......................................... 64 Table 3.1 Values for estimating Support Beam torque ............................................... 102 Table 4.1 Bending mechanism shaft rotation/strain state for [1.53 ............................... 132 Table 4.2 Bending mechanism shaft rotation/strain state forf-1 .57 ............................... 132 Table 4.3 Tensile strain in an offset strand with applied bending strain ........................... 172 Table 4.4 Bending strain in an offset strand ........................................................... 173 Table 4.5 Strain distribution in offset strand ........................... ............................ 175 Table A. 1 Estimate of actual bending strain at center of beam ..................................... 184 Table A.2 Derivative estimate of actual bending strain at center of beam ........................ 185 Table B. 1 Gear parameters for bending mechanism wormgears and worms ..................... 191 Table B.2 Spline parameters for bending mechanism components ................................. 193 Table F. 1 Test sample voltage tap separation distances (inches) ................................... 241 Table F.2 Test data for IGC 157, Sample #1 .......................................................... 242 Table F.3 Test data for IGC 157, Sample #2 .......................................................... 243 Table F.4 Test data for IGC 157, Sample #3 .......................................................... 243 Table F.5 Test data for EU 153, Sample #1 ............................................................ 244 Table F.6 Test data for EU 153, Sample #2 ............................................................ 245 Table F.7 Test data for EU 153, Sample #3 ............................................................ 246 18 Glossary of Terms a: minimum radius of superconductor filament A: cross-sectional area a: angle subtended by circular arc b: beam thickness B: magnetic field intensity C1 : constant of integration C2 : constant of integration C3 : constant of integration CICC: cable-in-conduit-conductor C,: specific heat of superconductor d: strand diameter db: beam thickness d,: strand diameter de: differential elongation dx: differential length de: differential angle 5: offset of strand from beam neutral axis E: elastic modulus E: critical electric field level c: bending strain CB: bending strain in strand when strand is offset from beam neutral axis Ebeam: 8 strand: bending strain in support beam bending strain of strand &t: strain in strand caused by thermal contraction ET: strain in strand caused by tensile load f nondimensional ratio between L, and L, F: force 20 G: shear modulus of elasticity GF: strain gage Gage Factor y,: mass density of superconductor h: beam height H,: critical magnetic field Hy: applied magnetic field HTS: high temperature superconductor I: current I: critical current I: moment of inertia ITER: International Thermonuclear Experimental Reactor J,: critical current density J0o: critical current density at operating magnetic field intensity ic: strain gage bridge constant f: length t : critical length twist pitch t,: twist pitch ld: deformed length of line L,: undeformed length of sample Lstrand: length of strand after deformation L,: distance between rotation axes in bending mechanism LTS: low temperature superconductor M: moment p,: magnetic permeability n: total gear ratio of bending mechanism N: normal internal force w: rotation from undeformed r: length of lever arm p: radius of curvature state 21 p,: electrical resistivity Pstrand: radius of curvature of strand T,: critical temperature T0 : operating temperature 0: angle of rotation of bending mechanism lever arms u: horizontal displacement Uerror: error in the beam end displacement from ideal Uideal: ideal displacement of beam ends for pure bending Umech: displacement of beam ends produced by bending mechanism v: vertical displacement V: internal shear VE: strain gage bridge excitation voltage bV: change in the strain gage measurement voltage : local axial coordinate y: distance from neutral axis 22 Chapter 1 Introduction The superconducting compound niobium-tin (Nb3 Sn) is an important technological material for building high field superconducting magnets. The superconductive state of Nb3Sn is sensitive to the strain conditions of the material. A considerable amount of research has been invested in trying to understand and predict this strain-dependent behavior so that more advanced magnet designs may be realized. This thesis describes the design and testing of a variable-strain bending mechanism which was used to measure the bending strain dependent critical-current of two different internal-tin Nb3 Sn strands, manufactured by Intermagnetics General Corporation (IGC) and Oxford Superconductor Technologies (OST). 1.1 History A material that is in a superconductive state has the two prominent characteristics of being able to conduct electrical current without resistance and, more importantly, expelling magnetic field from within the interior of the material. This second characteristic, known as the Meissner 24 effect, is the underlying means for conduction of electrical current without resistance in a superconductor. Superconductivity is a phenomenon that is common to many materials when placed under the appropriate conditions. Each material has specific critical values of temperature, T,, magnetic field, H,, and current density, J, which express the limits of the superconducting state. In addition, some materials, such as Nb3Sn, have a superconductive state that is particularly sensitive to the strain state, &.These values, representing the transition between the superconductive and normal resistive states, are often referred to as critical values. Thus the critical values establish a three-dimensional surface (or four-dimensional surface of properties if sensitive to strain), such as that shown in figure 1.1 which the material must be held within to remain superconducting. J Critical Surface Fig. 1.1. Critical superconductive surface. Kamerlingh Onnes discovered superconductivity in 1911 soon after he had successfully liquefied Helium in 1908. His original discovery came as he was testing the resistance of mercury with temperature. As he lowered the temperature below the 4.15 K critical temperature for mercury, the resistance suddenly dropped to zero. Onnes soon found several other materials that exhibited superconductivity at low temperatures, such as lead and indium. 25 After having established the critical temperatures for several materials, Onnes went on to find that there was also a critical magnetic field and critical current density. Realizing the potential of superconductivity, he built a solenoid magnet in 1913 using lead wire. This magnet could not remain superconducting beyond its own self-generated magnetic field of 0.08 T, establishing that there was both a critical magnetic field and critical current limit to the material. The materials that Kamerlingh Onnes and his contemporaries studied had very low critical values that appeared to diminish any potential of using them for large power applications. These substances, now known as Type I superconductors, were not able to transport any appreciable amount of electrical current in the presence of a low magnetic field. Type I materials only allow magnetic flux penetration within a thin layer at the surface of the material, as described by the London Theory which was introduced in 1935. It was the discovery of a lead-bismuth alloy Type II superconductor by de Haas and Voogd in 1930 that initiated the advancement of high power superconductor applications [1.1]. 1.2 Type II Superconductors Type II superconductors are a mixture of Type I superconducting material with a distribution of normal resistive regions. The local islands of resistive regions allow magnetic flux lines to penetrate through the mixture without destroying the overall superconductive state. If a transport current were applied to an ideal Type II superconductor in the presence of an external magnetic field, the resulting Lorentz force would cause the magnetic flux lines to move and redistribute across the material. This is illustrated by figure 1.2. The movement of the flux lines is dissipative and requires a voltage to sustain the transport current in the conductor, thus eliminating the superconductivity [1.2]. 26 VOLTA GE TRANSPORT CURRENT, Jit EXTERNAL FIELDHe Fig. 1.2. Dissipative flux motion in a Type II superconductor [1.2]. The flux lines may be pinned in place and prevented from moving by the presence of defects in the lattice structure of a non-ideal Type II superconductor. Vortices of magnetic flux penetrate through the normal regions and are surrounded by shielding currents. This establishes a pinning force that keeps the flux from moving and has the effect of raising the upper critical field level of the material. Each vortex contains one flux quantum which are arranged in a triangular lattice pattern throughout the material to minimize the energy state. This effect is illustrated in the drawing in figure 1.3a [1.3] and by an actual picture of the flux lattice in figure 1.3b [1.4]. Depending on the size and type of pinning site, there may be more than one flux quantum pinned. 27 Magnetic Flux Lines I Grair Bounda ries -- Pinned Vortex Current T - Transport Current (a) (b) Fig. 1.3. (a) Flux penetration in a Type II superconductor, and (b) picture of actual flux lattice [1.3,1.4]. The pinning sites of a Type II superconductor may be made up from several different types of imperfections in the bulk material including elemental inclusions, slip planes and other lattice defects, grain boundaries, and even voids from cold-working the material. The magnitude of the flux pinning force density depends on the type of pinning site and the superconducting material. Due to their differing pinning sites some Type II materials have higher flux pinning force density that others, as shown in figure 1.4 [1.5]. A higher flux pinning force density is desirable because it results in a higher critical field level for the material. 28 Bulk Pinning Force Comparison 10UMr T MC *mid t7u%Wr wih nd.% 'ipm ;2duwn Iftn.m*Wa1 dimO -kamuw et it fIWASq BEibbau..aliet ii. (UW-ASC) Mmmnd ibomn.s -lai: T --- NbSn YBCO -aW-U- b: Bat Heat Teated UW Manvflianmt. (Li and LaubalmsMe. IT) (2116)331 mno nedllsayer 15 45150 iNlcm. lbT:l-llb McCarmidp et t ie) pad Cu APC. MduW6WC. R. Zhou PWD lsi:sn --*+ Thesi ("n'"1 Sa Sn Pled CUAPC2OOru@630C. hou at aLfOST). - U - -e-- 4- 'I 4-~ -a-- - Ii. BM2 4a U - NbN!AfN - -flb 3 E: MlatbishTER MW hiwnal Sn lSa SnWand: Wih J, ermi Sn MW(Pen et al ASC~-M tachi.1M4M. Q4- l"/: Transfwnmd rod-40-be lb/i lb Slammed. APL.vol. 71(1). pp-122-124). 1357 IMANMtRayr B.Gray at aL (AL) I:N: 13nm-4M2nMi -- ePhysic C. 132' = mbrkd e.Ibab 73 K.Fokyn - n thwik nkmab -E- IWZVsO:lWR. Nb-Ti 191iamWttap* BNlip. bt -+- Hi2223: Roled 15 Fil Tpe(AwsC) B. UW6M --- .... -- -Okada et al PUlachi M Mg,'. -..-- y mn" 3. Eam et at(W) -a--Lf,: 10%wt SiC daped(Dou u e 2002 et al APL 2002.UW MgB 2 0 5 10 15 20 25 Applied Field (T) I *-fp.Mp.marLt d hkbVn! W MW-CMO byPibr Fig. 1.4. Flux pinning force comparison [1.5]. The concentration of pinning sites is just as important as the flux pinning force density in setting the critical field of a bulk Type II superconductor. Up to a point, increasing the number of flux pinning sites will allow more magnetic flux lines to penetrate the material and increase the critical field level. The magnetic field will penetrate through the normal regions until these sites are all filled, at which point the flux must go through the superconductive regions. This quickly causes a breakdown in the superconductive state and marks the critical field level. When more normal pinning sites are available, a higher intensity magnetic field can be applied to the bulk material before the flux lines must move to the superconducting region. However, as the amount 29 of resistive regions is increased it leave less available superconductive region for conduction of the transport current, thus reducing the current capacity of the bulk material. The concentration and type of pinning sites throughout the bulk superconductor are dictated by the material constituents and fabrication processes. The combination of cold-work on the material and special heat treatments can be used to control the quality and quantity of pinning sites, thus improving the critical field and current density limits of the bulk superconductor. Much research goes into developing these processes to create a conductor with the best possible final properties for the given design. 1.2.1 Theories of Superconductivity There are three significant theories of superconductivity that will be mentioned because of their importance to the subject, but will not be discussed in detail. These include the London Theory, the Bean and Anderson-Kim critical state models, and the BCS (Bardeen, Cooper, and Schrieffer) Theory. The London theory (1935) is a phenomenological theory that was a modification of Maxwell's electromagnetic theory to describe the Meissner effect (discovered in 1934). This theory establishes that the bulk superconductor is shielded from an external magnetic field by a supercurrent that flows in a thin layer at the surface of the superconductor and has a thickness equal to the London penetration depth, X. The Bean model (1962) and Anderson-Kim critical state model (1963) establish the balance between the flux pinning force and the Lorentz force. The Bean model assumes that the critical current of the superconductor, J,, is a constant while Kim proposed that J, is proportional to the inverse of the magnetic field intensity, 1/B. These theories provide ways to estimate the magnetic field and current profiles within a superconductor and predict the magnetization curve of the material. 30 The BCS theory (1957) is a quantum mechanical theory that successfully modeled Type I superconductivity properties. It is based upon the concept that electrons close to the Fermi level form into Cooper pairs caused by an attraction related to lattice vibrations at the appropriate temperature and mediated by phonon interaction. The electron pairs are bosons that can behave very different from single electrons that must obey the Pauli Exclusion Principle. These pairs have a slightly lower energy level and leave an energy band of around 0.001 eV. This energy gap allows the pairs to avoid the collision interactions that lead to resistivity. 1.3 Superconductor Development Applications of superconductors range from devices that simply exploit their behavior such as Josephson junctions to devices that place high demands on the superconductor, such as fusion reactor magnets. Of the thousands of superconducting materials that have been discovered there are only a few which are able to meet the demands of high field magnet applications. The environments in such magnets place the extremes of high field, high strain, high current, temperature instabilities, and sometimes radiation exposure on a superconductor. At present, there are only three superconductors that have been used successfully in such extreme applications and include the two Low Temperature Superconductors (LTS) Nb-Ti and Nb3 Sn and one High Temperature Superconductor (HTS) BSCC02223. There are four others that are under present development and which may be used in the future: Nb 3Al and MgB 2 as LTS and BSCCO2212 and YBCO for HTS [1.6]. Generally, it takes many years from the discovery of a superconducting material to its final development as a magnet-grade conductor. A timeline for Nb 3 Sn is given in table 1.1 and reveals that there was almost 30 years from the discovery of the superconducting properties of the material to the realization of a magnetic-grade conductor. Of, course as techniques become refined and the various problems worked out, the development process can be much faster for 31 subsequent materials. The development time to a magnet-grade Nb 3 Sn conductor was particularly long because of various problems related to stability and coupling losses which had to be solved. Table 1.1. Timeline for Nb 3Sn conductor development [1.7]. Event Period 1 Discovery Early 1950s 2 Improvement Jc Early 1960s 3 Co-processing with matrix metal Mid 1960s 4 Multifilament/twisting, Ic>100 A Early 1970s 5 Long length, typically -1 km Mid 1970s 6 Full specifications for magnets Late 1970s Stage The two most important problems that impeded early conductor development progress were flux jumping and coupling losses. The simple solutions turned out to be creating small multifilamentary strands with stability protection and twisting these filaments to minimize the area available for self-induced current. But it was only after much effort that these solutions were realized. Flux jumping is an event when the magnetic flux within a superconductor is suddenly rearranged. Under normal operating conditions the superconductor is in a stable state where the Lorentz force on the magnetic flux is just balanced by the pinning force. If some disturbance occurs to locally heat the superconductor then the critical current, J,, in that region will go down with the increase in temperature and flux motion will occur. Flux motion is dissipative and generates even more heat, which continues to locally raise the temperature. If the heating instabilities are not mediated by some means of protection then the positive feedback process 32 could quickly cause the material to transition into a normal conductive state and the subsequent Ohmic heating could permanently damage the conductor. Most low temperature superconductors (LTS) have critical temperatures below 20K. Since the specific heats of materials are very small at these temperatures, it only takes a minor disturbance to raise the temperature of the material by several degrees. Disturbances that might cause a local temperature rise include a mechanical motion that generates heat by friction or a transient magnetic field that causes an increase in current. Being faced with this stability problem, early conductor designs were unsuccessful because the sources of the problem were not well understood. But over time adiabatic and dynamic stabilization methods were developed which lead to practical conductors. Adiabatic stability is achieved when the energy generated by Joule heating is balanced by the heat capacity of the superconductor material. An analysis based on the Bean model, Faraday's law, and the thermodynamic heat capacity of the material produces equation 1.1, which gives the minimum radius of the superconductor, a, for adiabatic stability. This expression requires the specific heat of the superconductor, Cs, the mass density, y, the magnetic permeability, p,,,, the critical temperature, Tc, the critical current density, J,,, at the operating magnetic field level, and the operating temperature, T0 [1.8]. Ta T 'I p-j Jo Using example values of T, = 4.2K, Y,= 6.2 x IO3 kg/m3 , B = 5T, C, = 1J/kg-K, J00= 3 x10 9A/m 2, T= 7 K (C. 33 the minimum superconductor radius for adiabatic stability is a 68pm, or a diameter of d 140ptm. At low field levels J,, increases and J, is not a constant as assumed by the Bean model, but is a function of B. So, a conservative estimate of the superconductor filament diameter for complete adiabatic stability is d 70pm. Present designs of superconducting strands have filament diameters as small as 3pm. Dynamic stability is when the superconductive filaments are surrounded by a resistive material, such as copper, that has good thermal and electrical conductivity. Good thermal properties allow the heat generated in the superconductor to be quickly conducted away; good electrical conductivity provides a pathway for the current to flow when the superconductor transitions into its highly resistive normal state. This additional material stops the heating progression by providing an alternate path for the current to flow and allowing the superconductor to cool back to its operating state. Problems can occur within superconducting magnets that require active protection beyond stability methods. These problems include the breakdown of the insulation resulting in a short circuit between windings or large mechanical motions. Voltage sensors are placed at various points within the magnet to detect if a conductor begins to turn resistive, otherwise known as a quench. When this occurs the energy in the magnet can be quickly reduced by connecting a dump resistor across the magnet terminals or by switching on embedded heaters that heat the entire magnet above T,. The discussion on stability has shown that the superconductor should be formed into small filaments and surrounded by a conductive metal matrix. Small filaments are limited by their critical current density and are not capable of transporting any significant amount of current, besides being difficult to handle. So in order to increase the current-carrying capacity and practicality, modem designs combine many superconductive filaments within a copper matrix to create what is known as a multifilamentary strand. 34 A strand is composed of many superconductive filaments electrically connected by copper or some other resistive stabilizer. The electrical connections between the filaments provided by the matrix allow the strand to experience coupling losses. A strand in the superconductive state has a current and magnetic field distribution through its interior that can be described by the Bean and Anderson-Kim critical state models. This distribution means that coupling occurs between adjacent filaments when an external magnetic field is applied. Starting with a fully coupled scenario, analysis can show that the amount of coupling can be reduced by twisting the filaments. Introducing a twist in the strand shortens the distance between points where the filaments cross, thus reducing the projected continuous area within the external field. For the strand to not be fully coupled, it must have a twist pitch below a critical length, i C , that can be calculated with equation 1.2. This equation uses the same definitions as in equation 1.1 with the addition of p, for the electrical resistivity of the matrix material in the strand and, Hy, for the applied magnetic field [1.9]. C = 16Jjap (1.2) For a strand composed of superconducting filaments with a radius of a = 50Rm, a critical current density of J,=3x1O 9A/m 2, a copper resistivity of pc=3xO 10 9i-m, and p0 Hy = 0.01 T/s, the twist pitch should be under t =27cm. For higher rates of expected field change, the critical twist pitch should be correspondingly smaller. As a general rule the twist pitch, t ,, is usually designed to be less than 10 to 15 times the strand diameter. So, for a 1mm diameter strand, the twist pitch should be t P 10-15mm. It is important to note that although twisting is effective in uniform fields, it is only partially effective in non-uniform fields and completely ineffective with respect to self-fields. Self-field is the result of the transport current in the filaments and the filaments remain parallel to each 35 other regardless of any twist in the strand. This means that a large area is available for induced current to be generated by transients in the system. 1.4 Production of Nb 3 Sn Strand The design and manufacture of magnet-grade conductors faces the practical problem of how to produce many twisted small filaments distributed through a stabilizing matrix within a single strand. This discussion will be limited to a few of the methods for producing Nb 3Sn-based strand because they are the most relevant to this thesis. The Nb 3Sn compound is a brittle material that cannot be drawn into lengths of strand using standard wire forming techniques. Methods have been developed to manufacture Nb 3Sn strands by first combining together the necessary raw materials in a billet form and then passing the billet through a series of extrusion and annealing steps to achieve the desired strand diameter. The final step in forming the superconductor is a heat treatment that causes the constituents in the strand to react and form filaments of the Nb 3Sn superconducting compound. Handling of the strand after the Nb 3Sn has been formed must be done with extreme care because the brittle material can fracture easily. The ingredients combined in the raw billets include niobium and tin for the superconductor, copper for the matrix material, and a tantalum or niobium barrier to keep the tin from diffusing into the copper and forming lower-conductivity bronze during the heat treatment. These materials are combined using one of several different techniques and then drawn as a unit down to the final strand size. Each of the components has different material properties that make it difficult to extrude them together, so various annealing steps are often included to help the process. Copper is most often chosen as the matrix material because it is a highly ductile material that has excellent conductivity and combines well with the other materials. The ratio of copper-to- 36 superconductor in the strand is typically in the range of 1:1 or 2:1. This relationship has been shown to provide good stability while not occupying too much of the strand diameter available for current transport in the final product. Of course, different applications may use a strand with a slightly different amount of stabilizer. There are six contemporary manufacturing methods for creating Nb 3Sn strand: Bronze, Internal Tin, External Diffusion, Nb Tube and Sn Tube (Powder-in-Tube, PIT), Jelly Roll & Modified Jelly Roll, and Cable-in-Tube (CIT). Only the first three methods will be covered because they are the most relevant. Bronze process starts with a bronze billet that is drilled with a pattern of holes which are filled with niobium as shown in figure 1.5a. Several of these billets are extruded into hexagonal shapes and then stacked into a copper can with an interior tantalum barrier. The can is sealed and evacuated and then extruded followed by drawning into the final strand diameter as illustrated by the process outline in figure 1.5b [1.10]. This extrusion process is similar for many of the multifilament strand techniques. Stack & Extrude into Hexagonal Shape Cu-Sn Nb 00 Extrude FCold [~Draw Seal & Evacuate 0 00 0 0 0 Fig. 1.5. (a) Bronze billet pattern, and (b) Multifilament drawing process [1.10]. Preheat & Extrude 37 A picture of a Bronze process strand cross section is shown in figure 1.6. The view of the entire cross-section reveals the light outer copper surface with the darker tantalum barrier surrounding the filament pattern. The magnified view shows the individual filaments and the hexagonal pattern. Fig. 1.6. Picture of bronze process strand [1.11]. Internal Tin process begins with a pure copper billet that is drilled and filled with niobium and tin in a pattern similar to figure 1.7a. These billets are combined and drawn together to form a single strand. The extrusion and annealing steps are different than with the Bronze process because the constituents have different material properties. The barrier is usually co-extruded with the surrounding copper stabilizer. The Nb-Cu-Sn subelements are then restacked inside the barrier tube and drawn to final wire size. The picture of the internal tin strand cross-section in figure 1.7b shows that the tin core occupies a significant portion of the area. The tin must diffuse through the copper surrounding the niobium filaments and combine to form the Nb3 Sn compound during the heat treatment. This ends up creating a bronze matrix because tin has a greater affinity for copper than niobium. The outer copper shell and the tantalum barrier that keeps the tin from diffusing to the surface are clearly visible in the picture. The Internal Tin design typically results in a higher J, than an equivalent Bronze process. 38 - Cu - Nb PO q~~Sn (b) (a) Fig. 1.7. (a) Internal Tin billet, and (b) Picture of unreacted Internal Tin strand [1.12]. External Tin process is similar to Internal Tin in that it relies on the transport of tin through the copper to react with the niobium during heat treatment. However, the tin is added to the surface after the copper billet has been filled with niobium rods and extruded. The extrusion is plated with tin and then combined with similar extrusions which are drawn together to form the strand. Figure 1.8 shows the general layout of the external diffusion billet after it has been plated with tin. This process is not often used because it either requires too fine subelements or results in too small of a wire diameter. Nb Cu A Fig. 1.8. External tin billet arrangement [1.13]. I S 39 Other strand processes are based upon the same concept of bringing the materials together and forming a strand that is later heat treated to produce the Nb 3Sn compound. The primary differences are in the configuration and steps used to create the strand. Some of the processes result in a strand with a higher J,, while others produce an advantage with respect to AC losses. The cold working and annealing steps are carefully adjusted for each process so that either the J, is maximized or the AC losses are minimized after the final heat treatment. During heat treatment, the niobium and tin can diffuse and create bridges connecting filaments together. This is detrimental to the strand performance because the coalescence of the filaments creates a much larger effective diameter which, as was shown earlier, increases the likelihood of flux jumping as well as higher magnetization losses. TvistAnneal Spool Fig. 1.9. Twisting of superconducting strand [1.14]. Test Plating (optional) 40 After the strand has been drawn to its final size it is twisted to a specified twist pitch in order to reduce coupling losses. The general twisting steps are similar for the different strand designs and are shown in figure 1.9. The strand may be plated with chrome to give it a protective surface which eliminates strand-to-strand diffusion bonding during heat treatment. This is used when the strands are cabled together to form a large conductor. 1.5 Cable-in-Conduit Conductor (CICC) After the strand has been produced it is assembled into a conductor configuration for use in the windings of the magnet. Different types of magnets use different conductors based on the design requirements. Depending on the conductor design, the superconducting strand is maintained below its critical temperature using either conduction or the flow of a cryogen fluid. The magnet windings may be in a bath of cryogen as in MRI and NMR machines or have a cryogen flow forced through the conductor as in fusion magnets and high-energy physics dipoles and quadrupoles. Liquid-free conduction-cooled magnets are emerging in a wide variety of applications mostly because of improvements to cryocooler performance. Superconducting magnet conductors are generally composed of the superconductor, an electrically conductive material for stability (Cu, Al, or Ag), the cooling system, and a highstrength metal for structural support [1. 15]. A magnet conductor design should be able to transport the maximum current density while providing electrical insulation, cooling, stability, and mechanical integrity all at the lowest possible cost. The cable-in-conduit conductor (CICC) is composed of a cabled superconductor in a metal conduit cooled by forced-flow supercritical helium. Its current carrying capacity combined with its stability protection and inherent mechanical strength make it suitable for applications that use high field, large volume magnets, such as in ITER (International Thermonuclear Experimental 41 Reactor) [1.16]. CICC was originally conceived circa 1975 and has subsequently received much development attention. [1.17]. A picture of a disassembled length of CICC designed for use in the ITER CSMC (Central Solenoid Model Coil) is shown in figure 1.10 [1.18]. This conductor is made up of a combination of Nb 3 Sn internal tin superconducting strands and copper wires used for quench protection which are twisted together in several stages to create the final cable. The twist pattern for this cable can be seen in the figure and shows that groups of three strands are first twisted together and then combined in subsequent twist stages to form the cable structure. Each stage has a specified twist pitch and the overall pattem can be described by a series that represent the number of groups twisted together at each stage; for this CICC it is 3-3-4-5-6 = 1080. Fig. 1.10. ITER Central Solenoid Model Coil Conductor [1.18]. 42 A cross-sectional view of a CICC in figure 1.11 shows some of the additional features of the conductor [1.19]. The six final petals of the cabling are oriented around a stainless steel spring that maintains a central cooling channel for the single phase supercritical helium flow. The helium fills the void space and conducts away excess heat as it is forced through the magnet windings. Long lengths of cable are inserted into welded extrusions of a nickel-steel superalloy conduit of Incoloy Alloy 908 which is compacted around the cable to the final dimension. Fig. 1.11. CICC cross-section view showing a series of internal magnification stages [1.19]. 43 A series of magnifications of the conductor in figure 1.11 show the cross-section of a single strand followed by a small group of the over 1100 filaments in the internal tin configuration and concludes with a micrograph of one of the 3pm diameter Nb 3Sn filaments. After assembling the CICC it must be heat treated to form the Nb3Sn superconducting compound. The reaction may occur either before or after the conductor assembly has been formed into the magnet windings, depending on the design procedure. In the case of ITER, the conductors are formed into the magnet windings before the reaction heat treatment to form the Nb 3 Sn phase. One of the primary applications for the cable-in-conduit conductor is in large fusion reactor magnets such as those intended for ITER. Figure 1.12 is a picture of a computer model of the ITER design showing the relative scale along with the various magnets and systems [1.20]. The six central solenoids that are used to heat the plasma are at the core of the reactor and the toroidal field coils used to contain the plasma can be identified by their characteristic D-shape. Poloidal field coils surrounding the containment chamber at different elevations are used to shape the plasma. 44 [1.20]. Fig. 1.12. Computer model of ITER (International Thermonuclear Experimental Reactor) ITER is an experimental reactor that is a step between contemporary fusion reactors used to study plasma and future reactors that will be capable of generating electricity. It is an international project involving The People's Republic of China, the European Union and and Switzerland (represented by Euratom), Japan, the Republic of Korea, the Russian Federation, 45 the United States of Amenica. It is planned to be built in Cadarache, near Aix-en-Provence, France and is technically ready for construction to begin. The first plasma operation is expected to take place in 2016 [1.20]. Within fusion magnets, such as those found in ITER, large electromagnetic Lorentz forces are generated which place tremendous loads on the components. In particular, the brittle Nb3Sn strands which make up the conductor experience a complicated combination of mechanical stresses. It is important to understand the effect of these loads on the strain-sensitive strand in order to design reliable magnets that will operate at their expected levels. As described before, the strands are twisted in several stages into cables and then compressed into the structural jacket. This combination of cabling and compression means that the pathway of a single strand through the conductor is complicated and irregular. The strand may be positioned next to the jacket wall at one point and then migrate to the inner channel at a different axial distance along the conductor; it can run parallel to neighboring strands or cross over them causing a potential pinch point. When the conductor is carrying current in a large magnetic field the pathway followed by the strands leads to a complicated evolution of tension, compression, bending, and pinching strains as the Lorentz forces are applied. The effect of the Lorentz force accumulates within the conductor because, in addition to having their own electromagnetic forces, the strands closer to the magnet axis push against those strands further from the axis. These resulting strains can significantly degrade the ability of the Nb 3Sn superconductor to transport current. Much work has gone into trying to understand the strain-related behavior of Nb 3Sn not just for fusion magnets but for any application that places a strain-sensitive superconductor under a load. 46 1.6 Strain Behavior of Nb 3 Sn The strain-related behavior of Nb 3 Sn was studied by Buehler and Levinstein approximately a decade after its identification as a superconductor [1.21] and it was almost 20 years later that Ekin presented a strain scaling law that could be used for the design of practical superconductors [1.22]. This early work was primarily concerned with the uniaxial tensile and compressive effects on the current capacity of Nb 3Sn with some thought given to bending strain effects [1.23]. The research showed that the application of tensile strain first increased the critical current capacity of Nb 3Sn strand up to point before it began to decrease. This was explained by a precompression on the Nb 3 Sn that was applied by the surrounding matrix materials due to the different coefficients of thermal expansion as the strand was cooled from the reaction temperature to the operating temperature. Since those pioneering studies, substantial work has gone into better understanding the strain behavior of Nb 3Sn strand and developing improved strain scaling laws that are used for magnet design. A general overview will be given of the various efforts that have been undertaken to understand the strain behavior of Nb 3Sn. Rather than focusing on a single type of strain research, this overview will present a variety of studies that will serve to illustrate the numerous issues that surround the problem. The amount of effort that has gone into understanding the strain behavior of Nb 3Sn and other superconducting materials is an indication of the importance of this problem to superconductor applications. This effort has been driven by the need for better design tools as the boundaries of experience are pushed by new and more demanding magnet requirements. 47 1.6.1 Uniaxial Strain The material surrounding the Nb 3Sn filaments in a strand places an intrinsic compressive strain on the superconductor upon cool-down. The exact value of this compressive strain depends on the particular arrangement and quantities of the several materials in a given strand design, but typically is around -0.3% strain. Application of an external tensile axial strain to a strand relieves this compression and increases the critical current. If the applied strain goes beyond this amount, then the critical current begins to degrade. Appling a compressive strain on a Nb 3Sn sample will just serve to degrade the critical current level from the intrinsic cool-down state. Figure 1.13 shows a plot of the critical current in a Nb 3 Sn strand as a function of an applied tensile strain. The strand characterized in the plot was produced by Teledyne (TWC) and used in the 45T Hybrid magnet at the National High Magnetic Field Laboratory (NHMFL) [1.24]. The figure reveals the increase and subsequent degradation in the critical current of the strand as the applied strain goes to +0.3% and beyond. The open points are I measurements during loading and the closed points are measurements after unloading. The unloading began at the point marked "A" and measurements were done at 4.2K in a background field of 12T perpendicular to the sample. 0 40 S0- o 0.2 0.4 0.6 0,8 1 1.2 1.4 Strain, % Fig. 1.13. Strain dependent critical current in the 45T Hybrid magnet strand at 12T and 4.2K [1.24]. 48 A common practice when reporting strand strain behavior measurements is to move the data so that it is in terms of the intrinsic strain on the filaments. This consists of normalizing the critical current to the maximum value and shifting the data so that the new zero-strain point corresponds to this peak current. Figure 1.14 shows such a plot for an internal tin 00.8mm Nb 3Sn strand manufactured by Oxford Superconductor Technology (OST). An adjusted intrinsic strain of 0.0% results in the maximum measured current for the sample at external field levels of 17T, 19T, and 20T. The critical current value was defined for an electric field of 0.1 pV/cm, which will be explained in detail in chapter 4. The dashed lines represent fitting of the data to the strain scaling model developed by Ekin for predicting strain dependent behavior. Strain was applied to the sample using a popular device known as a Walters Spring (WASP) [1.25]. 1. 00 0. 9. 0. 0. o 0. 0. WI 63 -_20 _ _ 0. 0. 321T 0.2 0. -0.4 Nb n -I rnal In - - ......1 . . . . ...-.. . 0.0 -0.1 -0.2 -0.3 -. - 0.1 - 0.2 0.3 intr. strain (%) Fig. 1.14. Reduced critical current vs. intrinsic strain for OST internal tin wire [1.25]. 49 Uniaxial strain tests of Nb 3Sn are often performed with mechanisms that are capable of loading the sample through a large range of tension and compression in order to get a more complete understanding of the strand behavior. The mechanisms are designed to be used in the bore of a magnet that can produce a field intense enough to measure the critical current of the sample over a useful range. Requiring the test to take place in a magnet bore severely limits the length of the sample, which is unfortunate because longer samples give more sensitive measurement results. There are three devices that are prominent in studying the strain-behavior of technological superconductors: a U-spring holder, a device known as "Pacman", and the Walters Spring. The U-spring device has been used in various forms over the years to apply strain to superconducting samples. An example of one used at the University of Twente is shown in figure 1.15 [1.26]. The sample is mounted across a bridge that is either stretched or compressed by movement of the device's legs. It is a versatile and reliable system for characterizing the strain behavior of technical superconductors, but it has limitations with respect to the length of the sample that can be measured. Consequently, other devices intended to lengthen the sample have been developed. Strain dpsk -- - - - - -- 45n Tbermoseter --- _ S a p lh eo l e r .---smupe----- -Tape - 5 nun Tape -- 0 Strain p.p e----- 0 Struin pop L < Strain adjustmunI - HM--- Cnue%-uetloon (top) Fig. 1.15. U-spring strain device used at the University of Twente [1.26]. 50 The Pacman device shown in figure 1.16 was developed at the University of Twente. This mechanism lengthens the sample from the -45mm of the U-spring to -104mm. Of course, the effective test measurement distance is shorter than this, but it has resulted in a factor of 10 increase in length. The sample is affixed to the outside diameter of the holder and when a pure torque is applied to the ends of the circular beam section the beam diameter changes. This results in either a tension or compression in the test sample. Aside from the end effects, analysis shows that the strain in the test section is fairly uniform and introduces little bending [1.26,1.27]. I 2 3 e36 -7 3 2.53 000 3.7 5 Fig. 1.16. Pacman strain device used at the University of Twente [1.26,1.27]. The Walters Spring (WASP) is an ingenious mechanism presented in 1986 that significantly increases the sample length for strain measurements [1.28]. The Walters Spring has been adopted and modified for use by several researchers to study the strain behavior of both Low Temperature (LTS) and High Temperature Superconductors (HTS) [1.29,1.30]. Figure 1.17 shows the device used by Institute of Applied Physics at the University of Geneve, Switzerland [1.25,1.31,1.32]. 51 This WASP device can hold a sample length of 80cm and the Ti6Al4V spring alloy allows linear and reversible strains up to 1.4% to be applied at 4.2K. The sample is wrapped around the outer surface of the spring and either lies in a groove or is fixed by soldering. The mechanism operates by applying opposing torques at each end of the spring. It has benefited from many years of refinement and is one of the more common devices used for characterizing the strainbehavior of Nb 3Sn strand. mnt contaot stram gauge Ti alloy spring Nb 3Sn wire Fig. 1.17. The Walters Spring (WASP) device for measuring critical current as a function of strain [1.31]. The critical current information collected from the various strain methods is intended to improve understanding of the behavior of strain-sensitive superconductors. This data is then used to develop and improve universal strain scaling laws for use in magnet design. Being able to accurately predict the performance of the superconductor within a magnet allows designs to be created that optimize the use of the expensive superconducting materials. 52 1.6.2 Strain Scaling Laws Scaling laws have been developed to predict the behavior of technological superconductors in a practical design. Those superconductors with little or no strain sensitivity have relationships that express the behavior of the material in the three-dimensional space of current density, temperature, and magnetic field. But those superconductors with strain-sensitivity, such as Nb 3Sn, have a slightly more complicated description that includes additional parameters to account for the strain effects. Superconducting magnet designs have often avoided the added cost and uncertainty associated with using a strain-sensitive superconductor by using less strain dependent materials, such as NbTi. This limited the potential capability of those magnets because the strain-sensitive superconductors, such as Nb 3Sn, have inherent critical properties that allow them to produce higher magnetic field levels. The maturation of strain scaling laws provided a means for more accurate designs to be created using these materials as the need for magnet performance intensified. In 1980, Ekin presented a universal strain scaling law for practical superconductors [1.22]. This law and its refinements have been particularly successful for Nb 3Sn conductors and has allowed many magnets to achieve their design parameters. The Ekin scaling law was expanded to include temperature dependence and the effects of nuclear radiation by Summers in 1991 [1.33]. Work on the development and refinement of universal scaling laws continues to be done in an effort to extend the range and accuracy of these predictive tools [1.34,1.35,1.36]. The Summers-Ekin scaling law for Nb 3Sn is presently the most common method for designing magnets. Expressions for this scaling are given by equations 1.3 to 1.11. This scaling law consists of a few simple expressions for the critical current density, J", and the critical temperature, T,, which are modified by additional expressions that compensate for the strain 53 state and magnetic field conditions. Constant parameters are selected from a table of values depending on the strand configuration and its use [1.37]. J (Bmax,op, tot) Bmax' op' tot 1+ JO(Top Jc(BmaxTop,tot T (Bma,,x 76=o C TCO 6toJ- I-r (1.3) (1.4) BCM c2, M where Jci (Bmx , To,,I-o ) = Bc2 (T, ,., )= b= BO( Bmax "" BcTcoetot (Bc2 (Top Bc20 (v,,, XI_-t2 Jc (Top,)= J b= CO - 6 1_ - (t22 )112 ) (1 - 2 ) 2 b-1 /2(1 -b) 2 (1.5) (1.6) (1.7) (1.8) ) (1.9) TCO (6=To -e (1.10) 54 Bc2 (,t ) = B20M - a-tot (1.11) 1.7) For binary Nb 3Sn, oa=900 for s&0 t<O and u=1250 for stot>O; with ternary Nb 3Sn, c=1400 for stot<O and a=1800 for &tot>O. Some example material constant values are given below: For binary Nb 3Sn: Bc2 M =24T, Tom =16K, and Co=2.22x10 0 AT 2m2 For high performance ternary Nb 3Sn: B.2 , =2 8 T, Tom=18 K, C0 =1.16x10'0AT1 2m2, and J0 =3.3554x1O 10 A/m 2 For low performance ternary Nb 3Sn: Bc2.M=28T, Tcom=18K, C0 =0.9064x10 AT 2m2 , and J0 =3.3554x10 10A/m 2 1.6.3 Compound Strain Much of the research focus for improving the strain scaling laws has been in the areas of tension and compression. But, as was stated earlier, the true strain state of the strands within a magnet conductor, such as a CICC, is very complicated and not clearly understood. In addition to uniaxial tension and compression, a technical strand in a magnet conductor may also have a combination of transverse compression (pinching), bending, and possible twisting loads. These loads occur in different combinations along the same strand as it passes along its path through the windings. Other experiments have been designed and performed in an effort to capture some of the more complicated loading conditions that the strand may experience. These have been done both to test the application of the scaling laws in more complicated strain conditions and to gather empirical data that compensates for the knowledge gap between the predicted performance of a strand and its actual performance within a magnet conductor. 55 An early test for the transverse strain behavior of a superconductor was done by Ekin [1.38]. This device used two anvil heads to compress a sample placed between them in a background magnetic field, as shown in figure 1.18. The sample was heat treated, or reacted, in a U-shape to create legs for the current contacts. Measurements showed that the degradation in the strand with transverse strain was more severe than for a condition of uniaxial strain. F Rounded Edges Voltage Taps B B Sample Reacted to Shape Solder Copper Current Contact Pivoting Anvil Head F Fixed Anvil Head Fig. 1.18. Ekin transverse strain mechanism [1.38]. A novel strain device was created after analysis of the ITER Central Solenoid Model Coil (CSMC) and Insert coils revealed that the performance of the cables was below the prediction based on single strand characteristics. The device, known as the "Test Arrangement for Strain Influence on Strands" (TARSIS), was intended to load a single strand in a state that was similar to the conditions in the magnet cable-in-conduit conductor [1.39]. The mechanism is shown in figure 1.19. It consists of a lower drum and an upper cap with a periodic circular arrangement of fingers and pins, respectively. The sample is placed between these fingers and pins on the circumference of the drum. It is constructed from Ti6Al4V alloy so 56 that the sample can be heat treated directly on the device to avoid handling issues and have a low thermal induced strain on cool-down since the titanium alloy has a thermal coefficient of expansion near than of Nb3 Sn strand. Operation consists of closing the cap on the drum so that the fingers interlace with the pins, thus placing the strand in a periodic bending-tension-shearingpinching state. The alignment and movement is carefully controlled and measured by an extensometer and load cell. Fig. 1.19. TARSIS periodical bending device [1.39]. Tests with TARSIS were done cyclically to observe the degradation with repeated load application, as occurs in a magnet that is turned on and off. Results showed a reduction in strand performance that was a combination of permanent degradation from plastic deformation and reversible degradation with loading. TARSIS was a new step in strand testing, but at this point it has been determined to be more of a quantitative device rather than qualitative. Other tests have been performed that attempt to isolate the bending strain behavior of Nb 3 Sn strand. Senkowicz, Takayasu, and Lee have been involved in a series of static bend tests where 57 the sample is clamped in a fixture with a constant radius of curvature [1.40]. The Nb3Sn strand is heat treated in a straight configuration and then mounted in a groove between two curved Ti6Al4V clamps at room temperature. The device is then placed in a background magnetic field and the critical current is measured. A series of clamps are used that incrementally proceed from a baseline of 0.0% strain to 1.4% strain. A picture of the strand mounted between two clamps with a given radius of curvature is shown in figure 1.20. Fig. 1.20. Fixed bending strain behavior strand configuration [1.41]. Results showed that the critical current first increased up to a bending state near 0.4% and then degraded, much like tension tests. After a lowering of the critical current, there was a curious increase around 0.6% that quickly went down with additional bending strain. Because of the nature of the device, an individual strand can only be tested at its fixed bending strain state. It does not provide a way for the same strand to be loaded at multiple strain states. Therefore, it is not clear if the increase or degradation in critical current is solely from bending strain or a combination of bending strain and handling damage. 58 1.7 Thesis Objective Many tests have shown that there is a continued need for additional information about the strain behavior of Nb 3 Sn strand. Gathering this information leads to improvements in strain scaling laws and the ability to design more capable and optimized superconducting magnets. The objective of this thesis is to design, construct, and test a mechanism for characterizing the variable-strain bending behavior of technological Nb 3Sn superconducting strand. The strand will be placed on a support beam that will be bent through an evolution of pure bending states. This will allow a single strand to be characterized over a large range of bending strains which is similar to previous work done with high temperature superconductors [1.42]. Any degradation in the critical current of the strand during testing should be solely a result of the loading state. It is intended that such a device will take the next logical step beyond uniaxial strain to extend the understanding of strain behavior in a technological superconducting strand. The pure bending device will be designed for characterizing the strand in a 4.2K liquid helium bath with a background magnetic field. The magnet chosen for the design is the 190mm bore 20T resistive Bitter magnet at the National High Magnetic Field Laboratory in Tallahassee, Florida [1.43]. This magnet was selected because it has a large bore which allows a longer test sample length at relatively high magnetic field. This thesis discussion will proceed in Chapter 2 with an analytical development of the equations necessary for designing a pure bending device. Chapter 3 will continue with the important design requirements and complications that had to be satisfied by the design. And the conceptual design will be described along with the solutions to the problems. Chapter 4 will present the testing that was performed and conclude with a discussion of the results and recommendations for future work. Chapter 2 Analytical Development The previous chapter discussed the motivation for performing a pure bending experiment on Nb3Sn superconducting strand that experiences strain degradation. This chapter will develop the analytical equations for designing a large-displacement pure bending experiment. 2.1 Mechanics of Materials Bending refers to the flexure of a beam into some curvature. Pure bending occurs when the beam has a constant curvature along its length, as if it were bent into an arc of a circle. The beam has a constant bending moment throughout and there are no shear forces. In contrast, a beam experiencing nonuniform bending has internal shear forces and the curvature changes along its length. As shown in figure 2.1, a beam in a state of pure bending has compressive stresses on the inner face and tensile stresses on the outer face. Somewhere between these two surfaces is the neutral axis defined as the location where the stresses are zero. For a linearly elastic homogeneous beam, the neutral axis lies at the centroid of the cross-sectional area when there is no axial force 60 acting on the cross-section. The radius of curvature defines the amount of flexure in the beam and can be used to determine the bending state. A beam can be loaded in pure bending by applying two moment couples having the same magnitude but acting in opposite directions. Similarly, a beam can be bent around an object with a constant curvature, such as a cylinder, to create a pure bending state. In both cases the forces must be applied so that shear stresses are not generated. The motion required to create pure bending consists of moving two points of the beam closer together as they are rotated in opposite directions relative to one another. This movement preserves the original length of the beam and assists the natural tendency to curve into an arc. The relationship between the displacement and rotation motion is critical for achieving pure bending and is the ultimate focus of this chapter. Radius of Curvature, P Inside Face (compression) M M Neutral Axis Outside Face (tension) Fig. 2.1. Beam in pure bending. A brief development of the relevant mechanics equations will now be presented. This will make the assumptions and consequent limitations of these equations more clear. Further treatment of linear elastic mechanics may be found in a textbook on the subject [2.1]. 61 Figure 2.2a shows a length of a homogeneous beam prior to being deformed. The dashed line represents the neutral axis of the beam. Lengths along the neutral axis are assumed not to change when the beam is placed in pure bending. The line dx lies on the neutral axis while the line cd is a distance y above the neutral axis. Examining the normal strains in these locations when a positive moment couple is applied to the beam provides the means for deriving the pure bending relationships. a b ,d c ----------------------------- -------- - ---- M dx e M f (a) dd bM a M dx e f (b) Fig. 2.2. Deformation of a beam in pure bending: (a) side view of beam, (b) deformed beam. 62 The lines ae and bf represent initially parallel cross-sections of the beam that have been rotated in the deformed beam of figure 2.2b. The resulting angle between these lines is dO and, if extended, they would intersect at a distance p from the neutral axis. The initial distance between the two lines at the neutral axis, dx, remains unchanged after the beam is deformed and can be expressed in equation 2.1 using the radius of curvature, p, and differential angle, do. dx = pod (2.1) All of the other lines connecting lines ae and bf either lengthen or shorten depending on their location relative to the neutral axis, thus creating normal strains, F. To evaluate these normal strains, the deformation of line cd will be considered. This line remains the same distance y from the neutral axis when the beam is deflected, but changes in length. The deformed length of line cd can be found from the geometry. Realizing that the radius of curvature for this line is p-y, the deformed length is lcd. lcd =(p - yWJ9 (2.2) Equations 2.1 and 2.2 can be combined to eliminate dO, yielding equation 2.3. lcd = dx -dxj) (2.3) Originally the two lines ae and bf were parallel and separated by a distance dx. It then follows that the elongation of line cd due to bending, dl, is given by equation 2.4. dl = lcd -dx = -dx (2.4) 63 Strain is defined as the amount of elongation divided by the original length, which can be expressed by rearranging equation 2.4: C dl dx y p (2.5) Equation 2.5 verifies that there is negative strain, or compression, above the neutral axis and positive strain, or tension, below the neutral axis when the beam is in a state of pure bending. The magnitude of the strain within the beam depends on the location relative to the neutral axis and is directly proportional to the y distance. The strain is at maximum compression on the inner surface of the beam (positive y) and varies linearly to a maximum tensile strain at the outer surface (negative y). A useful expression that relates the applied moment, M, to the radius of curvature of a beam in a state of pure bending is presented without proof in equation 2.6. The elastic modulus, E, and moment of inertia, I, are material and geometric properties of the beam, respectively. M = EI (2.6) p Equations 2.5 and 2.6 are the basis for determining the forces and rotations that result when a beam is placed in a specified pure bending strain state. Although it was not explicitly given for equation 2.6, both equations were derived using two basic assumptions. First, there exists a neutral axis within the beam that does not change length when the beam is bent. Second, a more subtle assumption is that cross-sections that are plane before bending remain plane after bending. Both of these assumptions are related to the requirement that the material which makes up the beam is homogeneous and linearly elastic. If a beam is distorted beyond its elastic limit and begins to plastically deform, then these assumptions diverge from reality and the accuracy of equations 2.5 and 2.6 are increasingly reduced. It is important to remember these restrictions 64 when applying them to the pure bending of Nb 3 Sn superconducting strand; the beam must remain within its elastic limit in order for a pure bending state to exist. 2.2 Example Nb 3Sn Strand Bending Now that the mechanics equations have been presented, an estimate can be made for the amount of rotation that is required to bend an example Nb 3Sn superconducting strand. Testing of the strand will take place in the 195mm bore 20T magnet at the National High Magnetic Field Laboratory. A reasonable assumption for the bendable test length, L,, is 4.5 inches (114mm), based on previous strand experiments in this same facility. The ITER spec strand has a circular cross-section with a diameter, d, of 0.81mm (0.0319 inches). Critical current tensile tests show that the Nb 3Sn strand current carrying capacity begins to degrade at axial strains of 0.3%. This happens when the strand as a whole is under the same uniform strain. But in pure bending, part of the strand is in compression while the rest is in tension. So to capture the transition point, it is probably necessary to go to a higher bending strain at the strand surface such as 0.7%. A bending strain of 0.7% means that there would be a compressive strain of 0.7% on one surface of the strand that would vary linearly to a 0.7% tensile strain at the opposite surface. Table 2.1 summarizes all the specifications for the example strand. Table 2.1. Summary of the example strand specifications. Ls d 4.5 inch (114 mm) 0.0319 inch (0.81 mm) Cma 0.007 (0.7 %) 65 The design range of the bending mechanism is determined by the total angle that the strand must be rotated through. Equation 2.7 is the standard geometric relationship used previously to relate the arc length to the radius of curvature, but in this case the arc length is the original test length of the strand and the variable a is the angle subtended by the arc. L, = pc (2.7) Combining equations 2.5 and 2.7 allows the radius of curvature to be eliminated and the angle to be expressed in terms of the defined parameters in equation 2.8. Recall that y in equation 2.5 is the distance from the neutral axis to the position in the beam of interest. In symmetric beams, such as the circular cross-section of the strand, the neutral axis is located at the center of the beam. The maximum strain has been defined for the outer surface of the strand as a whole, so that y is equal to half of the diameter. a= L (2.8) d 21 Substituting the example values outlined above reveals that the strand must be bent into an arc that spans 1.975 radians (113.2 deg) to achieve the maximum strain state. To provide some sense of the geometry, figure 2.3 shows a scaled drawing of a 4.5 inch (114mm) strand bent into an arc of 113 deg. Even though these results are based on an estimate of the strand test length, the actual strand length will not be significantly different. 66 L, = 4.5 inch smx=0.007 p =2.278 inch 1130 Fig. 2.3. Scaled drawing of example strand at maximum strain state. It is evident from the large rotation of the example strand that it must be bent using a largedisplacement test method. If the strand length were shorter, then only small rotations would be required in order to achieve the maximum strain state. A simple method, such as the standard four-point bend test, could then be used to characterize the superconductor. However, for reasons that are discussed in section 3.1, the strand should be as long as possible in order to achieve an accurate measurement of the critical current of the sample. Therefore, an apparatus capable of large-displacement pure bending motion must be designed. Inspiration for a large-displacement bending apparatus can be found in the field of composite materials research. Bend tests are commonly used to determine the strength of composite materials because tensile tests can damage the sample in the region were it is held. This is particularly important for brittle samples such as ceramics or materials that lack sufficient internal cohesion like asphalt. Most often the four-point bend test is the preferred method, but in cases where the rotations are significant a large-displacement method must be used. Such a large-displacement technique has been developed and was validated with glass-epoxy samples [2.2]. Using an apparatus with a similar layout would not be practical for testing the Nb3 Sn 67 samples because of the space limitations imposed by the magnet bore. Consequently, an alternative device must be created that uses the available space more effectively. 2.3 Differential Equation Approach to Large-Displacement Bending The design and optimization of a large-displacement bending mechanism depends on the relationship between the translations and rotations required to produce a pure bending strain state in the beam. In this section, the governing relationship between translation and rotation will be derived. Conceptually, the pure bending of a beam is an evolution through a series of intermediate circular arcs. At each state the beam must have a constant radius of curvature, which means that it truly forms a portion of a circle. This transformation process is illustrated in figure 2.4a where an initially straight beam is bent through a series of pure bending states. It is apparent from the figure that the ends of the beam must move closer together as they are rotated [2.3]. But figure 2.4b reveals that pure bending has no dependency on the vertical motion of the ends so long as all movement is symmetric about the beam's centerline. 68 I / I I N 1~ / 011 (a) (b) Fig. 2.4. (a) Evolution of a beam through pure bending states, and (b) Pure bending is independent of symmetric vertical motion. The coupling between the rotation of the ends of the beam and the horizontal movement can be found by solving a set of generalized constitutive beam equations originally presented by Simo 69 [2.2]. These governing expressions, given by equations 2.9-2.11, relate the displacement of a beam to the internal normal force, N, the shear, V, and the moment distribution, M, while allowing for large transformations. The limiting assumptions for these equations require that the beam be homogeneous and that planes remain plane throughout deformation. As a reminder, these same assumptions were used in deriving equations 2.5 and 2.6, which assures that the expressions used to design the pure-bending device remain consistent. N (EA 1+ d jfd\ V =(GA cos+-v sin V d dv cos / dg M = (EI)dl / +- d) 1 sin V/] j (Normal force) (2.9) (Shearing force) (2.10) (Moment Distribution) (2.11) d In these equations, E is the modulus of elasticity, G is the shear modulus of elasticity, I is the moment of inertia about the bending plane, and A is the cross-sectional area of the beam. The terms (EA) and (GA) represent the tensile and shearing stiffness while (EI) is the bending stiffness of the cross-section. The equations are essentially one-dimensional because they are given only in terms of the LOCAL axial coordinate of the beam, . The variables u, v, and M' respectively give the horizontal displacement, vertical displacement, and rotation of a local section of the beam relative to its original undeformed position. Pure bending requires that the normal and shearing forces of the beam are zero and that the internal moment is constant. Applying these requirements to equations 2.9-211 results in the following modifications: 70 LC du dv. 1+ dv cos /+--sin/-1 ( du cos V - =0 (2.12) 1 sin l=0 (2.13) M = (EI)d/ dg (2.14) Only three boundary conditions are required to find the relationship between the horizontal translation and rotation at the ends of the beam. In figure 2.5a an initially straight beam of length L, is shown with rigid clamps attached to the ends. The clamps are not allowed to deform when they are used to apply a moment couple, M, to the beam. As the beam clamps are rotated an angle 0 from their original orientation, the length of the beam, L., remains constant as shown in figure 2.5b. Due to the beam's bending stiffness, the applied moment must be increased as the clamp rotation angle increases. It is important to realize that the applied moment is only a function of the beam clamp rotation as emphasized by the term M(6) in the figure. Because the beam clamps are rigid, the rotation of the beam at the local coordinate of = 0 in figure 2.5c is equal to 0. This is given by the first boundary condition in equation 2.15. V/( = 0)= 0 (2.15) The second and third boundary conditions come from the symmetry of the beam. Both the horizontal translation and rotation of the beam at the symmetry line must be zero for a pure bending state. U =L' =0 2) (2.16) 71 (2.17) U0 Rigid LS L PLXC lamp III (a) Ls M(O) M6 (b) Ls/2 + -~ -V X +N -- M(O) Symmetry Line (c) Fig. 2.5. (a) Initially straight beam with rigid clamps, (b) Deformed beam, and (c) Half beam with symmetry. 72 Finding the desired solution from the generalized constitutive equations begins by solving equation 2.12 for dv/d , yielding equation 2.18. Substituting this expression into equation 2.13, then simplifying and solving for du/d produces equation 2.19. dv d = 1 {~ I 1sin V/ I du = cos d 1du 1+ d Cos/ d y/ 1 (2.18) -1 (2.19) From the definition of pure bending, the internal moment distribution along the length of the beam is constant and does not depend on the location, . Rather, the internal moment is only a function of 0 as described previously. Equation 2.14 can be restated as equation 2.20, which highlights that the right-hand side consists of only constant terms as far as the variable is concerned. dy _M(O) d EI (2.20) Instead of solving for ' in the typical manner, a solution can be found that extracts out the dependency on 0. Integrating equation 2.20 and expressing it in the most general format results in equation 2.21. Applying boundary conditions 2.15 and 2.17 gives a solution to the constants C1 and C2 , which are substituted to arrive at equation 2.24. V/ = C1 + C2 (2.21) C] (2.22) = 0( 73 9 C2 =2 (2.23) L, 0 - 5+1 (2.24) The relationship between the internal translation and rotation distribution along a beam in pure bending can be found by first substituting equation 2.24 into 2.19 to get 2.25 and then integrating to arrive at the general solution given by equation 2.26. SCOS 0 u -LS L +1] -1 sin 0 20 2 2 -L +1 (2.25) - (2.26) +C3 Boundary condition equation 2.16 is used to find the value for C 3, which is then substituted and combined with the fact that sine is an odd function to get the relationship for u, 0, and in equation 2.28. C3 (2.27) L2 2 1 1iFS+n 2- 2 0 LS u= -L -j 1 - (2.28) A practical bending mechanism will only apply translation and rotation at the ends of the beam using rigid clamps instead of forcing a particular distribution along the beam's entire length. To 74 produce pure bending, the required motion of the clamps can be found by substituting the coordinates of the beam at the clamp-beam interface into equation 2.28, namely =0 and =L,. Because of symmetry, the motions at the clamp locations are mirror images and given by equations 2.29 and 2.30. These equations are the governing translation-rotation relationship for placing a beam in a state of pure bending. u = IL,1- si()] for =0 (2.29) u = I-LS[ for = L, (2.30) 2 0 -1 Plots of equations 2.29 and 2.30 showing the horizontal translation as a function of rotation for the two beam ends are given in figure 2.6. These curves were created using the parameters from the example beam in section 2.2. The length of the beam was L, = 4.5 inch (114 mm) and bent through an arc of 113 degrees at maximum strain. To generate this arc each end of the beam is rotated through approximately half of the total angle, or 57 degrees, which is the maximum rotation in figure 2.6. 75 Beam Motion at Ends, Ls=4.5 inch 0.4 -- 0.3 - -- - - - - -- ------- ---- -- - ------- -- - - - - - ------ ----- ----- --- - - - ----- ----------- 0.0 0 X: -- ( -0.1 - ---------- - ---- - - - - =O 10 20- 30 40 -------- 50 - 60 =Ls -0.2I -0.3 - -0.4 Rotation (degree) Fig. 2.6. Pure bending motion of beam ends for the example strand. 2.4 Geometric Verification of Pure Bending Relationship It is important to find an independent check to verify the derived pure bending relationship between the horizontal translation and rotation at the ends of a beam given by equations 2.29 and 2.30. This will be done using a simple geometric argument. Figure 2.6 shows a beam of length L, that was originally straight and subsequently loaded into an assumed state of pure bending. Rigid clamps attached to the ends of the beam were rotated through an angle 0 and translated a distance u to bend the beam into a constant arc with a radius of curvature p and angle a. It can be shown that a is related to 0 by equation 2.31 for all rotations, provided that the beam remains in a pure bending condition. 76 Ls/2 u - P Fig. 2.7. Beam deformed into a state of pure bending. a = 20 (2.31) Using symmetry, the horizontal displacement of the rigid clamp, u, is the difference between the undeformed and deformed distance from the beam centerline to the clamp. The undeformed distance is L,/2 and the deformed distance can be found from the right triangle that has the radius of curvature as the hypotenuse. The expression for u is given by equation 2.32 after incorporating equation 2.31. u =-L, - psin(0) 2 (2.32) Since Ls remains constant throughout the bending progression, the radius of curvature can be expressed as a function of 0 by combining equation 2.7 with 2.31 to produce equation 2.33. 77 P = LS 20 (2.33) Substituting equation 2.33 into 2.32 results in equation 2.34, which is identical to the pure bending relationship 2.29. A similar development can be used to verify equation 2.30. u =I L 1- si L O 2 (2.34) Pure bending derivations based on both geometry and the constitutive equations for the internal forces in a beam produced the same relationship between the horizontal displacement and rotation. This nonlinear relationship of motion must be incorporated into some sort of mechanism if it is able to load a beam in pure bending. There are many configurations that could be devised to create the pure bending motion. However, a mechanical device that could produce the precise translation-rotation nonlinear motion would be relatively complex. Such a mechanism would be larger, more complicated, and less reliable than a simpler system that would, instead, reasonably approximate the pure bending relationship. It turns out that the movement required to trace the circumference of a circle is very similar, although not ideal, to that required by equations 2.29 and 2.30 and would produce a good approximation to pure bending motion. Circular motion can be easily achieved using standard mechanical components. But this type of movement introduces horizontal displacement errors when compared to the ideal pure bending relationship. Fortunately, these errors can be minimized to acceptable levels by optimizing the mechanism geometry. 78 2.5 ErrorMinimization Of the various bending mechanism configurations considered, the basic layout shown in figure 2.8 proved to be the most robust and versatile. The components consist of two rigid beam clamps attached at the ends of the beam. These clamps are connected to lever arms that rotate about a fixed axis. The distance between the two axes of rotation is represented by L, and the free length of the beam is L,. The lever arm length, r, can be chosen to minimize the amount of pure bending error. Although the lever arm length is fixed during operation of the mechanism, it can be designed ahead of time to produce minimal error over a specific range of bending. The length of the beam, L,, does not change as it is bent. The rigid lever arms are simply rotated so that the two ends of the beam move closer together and it is forced to assume the shape of a circular arc. A detail worth mentioning is that the beam is not required to intersect the axes of rotation as the bending motion progresses. In addition to moving the two ends of the beam closer together, the rotations of the lever arms translate the entire beam in a direction perpendicular to the page in figure 2.8a. Referring back to figure 2.4, this has no effect on pure bending motion as long as the translation remains symmetric about the beam's centerline. Beam Lever Arm Axis of Rotation (a) 79 Ls ] rw4] Ik I r r (b) Fig. 2.8. (a) Side view of circular-type bending mechanism, and (b) top view of circular-type bending mechanism. Optimizing the mechanism to create quasi pure bending in the beam consists of comparing the motion created by the lever arms to that required by the pure bending relationship. Since the motion is antisymmetric for both cases, it is sufficient to do the optimization using equation 2.29 and an expression for the displacement-rotation caused by the lever arm. - u U LP r r Fig. 2.9. Displacement at the beam end due to the lever arms. 80 The amount of displacement at the beam ends caused by the rotation of the lever arms can be derived from the geometry in figure 2.9. The distance from the pivot axis to the free portion of the beam is equal to r in the undeformed configuration. As the lever arms are rotated an angle 0 from the initial position, the horizontal distance from the pivot axis to the beginning of the rigid clamp changes. This distance can be found from the right triangle. The net horizontal displacement of the beam ends, umech , is the difference between these two values as expressed by equation 2.35. = r - r cos6 U,,,ch (2.35) Equation 2.29 specifies that the amount of horizontal displacement required for pure bending depends on the beam length, L. To perform a generalized optimization, this dependency should be eliminated by nondimensionalizing the length terms in the relevant equations with Ls. Dividing equation 2.29 by L, produces the nondimensional form for pure bending horizontal displacement, iis,,, in equation 2.36. UWd = 1[I- (2.36) Nondimensionalizing equation 2.35 will be done after r has been expressed in terms of L. The dimensions L, and L, are more important for the design of the bending mechanism than r because gears will be used to rotate the lever arms in the actual device. With this in mind, r can be expressed from the geometry of figure 2.8b as equation 2.37. r = IL, - L) 2 (2.37) 81 A constant of proportionalityf will be introduced to express L, in terms of L, in equation 2.38 because Lp is simply a fractional length of L. L =-L, (2.38) f Substituting equations 2.37 and 2.38 into equation 2.35 and then dividing by L, produces equation 2.39, which is the nondimensional expression for the horizontal displacement in the quasi pure bending mechanism. imech = (I- Cos) 1 (2.39) An expression for the error between the ideal bending relationship and the approximate bending mechanism can now be defined. There are only two variables for producing pure bending in a beam: horizontal translation and rotation. Since the approximate bending mechanism is based on the rotation of a lever arm, the error of the mechanism comes from the horizontal translation component. And the error expression used to optimize the mechanism will be defined as the difference in the horizontal displacement from an ideal pure bending device, as stated in equation 2.40. Uero, =Ui (2.40) U- mech Including the details of equations 2.36 and 2.39 in 2.40 gives the particular error expression in equation 2.41. Wrror =- Icos 2 - sin-- + 0 f (1Cos (2.41) 82 Curves of equation 2.41 could be plotted for many different values of the proportionality constantf to find the optimum geometry of the bending mechanism over a specified range of lever arm rotations, but a little math will help to quickly narrow down the possibilities. This is done by requiring the horizontal displacements to be equal at some angle of rotation and solving forf Setting the nondimensional equation 2.39 equal to 2.36 and solving forf results in equation 2.42. Note that care must be taken not to improperly divide out the 9 during the solution process because it is allowed to have a zero value. f cos9 - 1 cos 0 - sin 6 6 (2.42) Taking the limit of equation 2.42 as 0 goes to zero reveals that the best value off for the start of the bending process is 1.50. This value off translates into a value for r that is one sixth the length of the beam, L, using equations 2.37 and 2.38. At a value of 9 equal to 80 degrees, the best proportionality constant,f is 1.55. These results forf provide a good starting point for the mechanism optimization, but they can be misleading because the values are only best at a single rotation angle. In reality, the mechanism must be able to provide minimum bending error over a wide range of lever arm rotations. For that, equation 2.41 must be plotted as a function of 0 for various values off Applying the insight gained from equation 2.42 the plots should begin with anfvalue of 1.50. Figure 2.10 show curves of equation 2.41 for values off ranging from 1.50 to 1.57 over angles of zero to 90 degrees. A maximum angle of 90 degrees is the applicable limit to equation 2.41 because the mechanism displacement given by equation 2.35 was derived using the lever arm pivot axis as the reference point. This expression becomes invalid when the lever arm rotates beyond the reference point which occurs for angles exceeding 90 degrees. If larger rotations are needed for the error minimization then a new expression for mechanism displacement would 83 need to be derived. Ultimately this is not an issue because the maximum strains that the bending mechanism will be designed to achieve will occur at lever arm rotation angles near 56 degrees, as was shown by the example strand problem presented in section 2.2. Nondimensional Error Minimization 0.0200 w 0 0.015 - --------------- ---- --------- --- f= f= -a-f = -- f = -x--- f= 0.010 - --------------------------------- - - - . -- - 0.005 0 Z ----- - ---- - - -- ---- - - -- -- 0.000 1 -------------------- -0.005- -- - - -- - -- - - __- - -- --------------- 1.50 1.52 1.53 1.55 1.57 -0.010 0 20 40 60 80 100 Rotation Angle (deg) Fig. 2.10. Plot of nondimensional bending displacement error. Over the full range of angular rotation up to 90 degrees the valuef= 1.55 has the least average error. But up to a maximum rotation of 56 degrees the valuef= 1.53 has the least overall error. Consequently, this value off will be used as the basis for designing the bending mechanism. In the figure, all but the first curve cross the zero-error axis at some point. These locations represent the solution to equation 2.42 for that particular value off A beam loaded by a bending mechanism under these conditions would actually be in a state of pure bending provided that it was not experiencing plastic deformation at its outer surface. 84 The error analysis does not provide a sense of how close to pure bending the nondimensional geometry would create in an actual application. It may be that all of the curves plotted are too inaccurate over the range of interest. Or it is likewise possible that even the curve plotted with the worst average error, namelyf= 1.50, would produce sufficiently accurate bending results. The analysis is only a way to compare one quasi-bending geometry to another and to show which configuration is potentially the best. The error analysis could be repeated using the dimensional equations and the example beam length of L, = 4.5 inches to find the amount of displacement deviation from the ideal case of pure bending. But that still would not provide a sense of the bending distribution within the beam. There are four possible ways to estimate how closely the beam comes to pure bending: first, a finite element program could be used to model the motion of the ends of the beam and solve for the stress distribution. Second, the governing constitutive equations, 2.9-2.11, could be numerically solved with the appropriate boundary conditions to find the internal moment distribution. Third, estimates can be made on the internal stress distribution using smalldisplacement beam mechanics. Fourth, an upper bound on the bending state at the center of the beam can be approximated by comparing the change in bending strain to the change in displacement. This last method was used because the other methods either required large time investment or resulted in questionable accuracy. The procedure for the bounding estimate is described in Appendix A. It shows that even for the non-optimized case off=1 .57 the bending state at the center of the beam remains within 1% of the ideal bending state. Chapter 3 Design The previous chapter developed the analytical relationships for large-displacement pure bending motion. It was shown that there was a relationship between the rotation and displacement at the ends of a beam in order to produce pure bending. Due to the nonlinear nature, the displacementrotation relationship changes with increased applied bending. This motion is difficult to create using simple machine components and so an approximate approach is justified based on circular motion. The geometry of the conceptual bending mechanism requires optimization to minimize the displacement errors introduced by the circular movement. This chapter extends the analytical development to create a practical mechanism for loading Nb 3Sn strand in a bending state for critical current testing. Operating requirements for the mechanism will first be discussed followed by the design and construction considerations that went into the principal components. 3.1 Operating Conditions and Requirements Pure bending critical current tests of the Nb 3 Sn superconducting strand were done in the 0195mm (7.68 inch) bore, 20T, Bitter resistive 20MW DC magnet at the National High Magnetic Field Laboratory (NHMFL) in Tallahassee, Florida. Figure 3.1 shows an illustration of 86 the magnet and the accompanying cryostat insert [3.1]. The cryostat provides an environment suitable for performing low-temperature tests such as superconductor critical current measurements. The cryostat has an outer chamber which is filled with liquid nitrogen to reduce the radiation heat loss and an inner chamber that uses liquid helium to maintain a 4.2K test temperature. The cryostat reduces the available magnet diameter from a warm-bore size of 195mm (7.68 inch) to a cold-bore size of 170mm (6.70 inch). Kc ~_ ~ - Outer chamber filled witlh liquid nitrogen Testing region filled with liquid helium Fig. 3.1. Drawing of the 195mm bore, 20T Bitter resistive magnet and cryostat at the National High Magnetic Field Laboratory (NHMFL) in Tallahassee, FL [3.1]. 87 Since the field center of the magnet is 74.13 inches (1883mm) from the top flange of the cryostat, the bending mechanism has to be attached to the end of a probe which positions it at the correct location. The probe serves the multiple purposes of resisting the forces generated during testing, allowing remote access for adjusting the bending load on the test samples, and providing a framework for the wiring and instrumentation. Two Nb 3 Sn strands were selected for the bending tests: an Intermagnetics General Corporation (IGC) strand used in the ITER Central Solenoid Model Coil and a recently developed Oxford Superconductor Technologies (OST), type 1, billet number 7567 strand. Both strands have a diameter of 0.81mm and are internal tin designs. There are many important environmental conditions and requirements that must be endured by the testing equipment. Each one has important consequences that affect the overall design. They can be divided into the categories of Operating Conditions and Specifications which are outlined below: Operating Conditions 1. Portions of the probe and the entire bending mechanism with the test samples will be submerged in a liquid helium bath. This bath keeps the samples at a constant 4.2K, which is the boiling temperature of liquid helium at atmospheric pressure. Low temperature is necessary so that the Nb3Sn samples will remain below their critical temperature. The liquid helium bath establishes a stable operating temperature that remains constant throughout the tests. The various materials should perform their functions under these conditions without damage. Particular consideration should go into the interactions of materials with differing Coefficients of Thermal Expansion (CTE) as the components are cooled from room temperature to 4.2K. Wires that move during testing should be electrically insulated with a material that can flex without damage. 88 Parts that require lubrication cannot be lubricated with grease because grease would freeze and not provide any benefit at 4.2K. A dry lubrication such as graphite or molybdenum disulfide should be used instead. 2. Magnetic field intensities for the testing will range from 12T to 15T, therefore ferromagnetic materials should not be used in the mechanism or probe. Magnetic materials would generate large forces that could damage the probe, mechanism, cryostat, or even the magnet. In addition, a sufficient presence of magnetic material would distort the magnetic field in the region of the test sample. The forces on a current-bearing sample in a high magnetic field can be significant. The critical current of a recently tested sample of the OST strand at 4.2K was approximately 300A at 12T and 220A at 14T [3.2]. The Lorentz load on an 11.4cm (4.5 inch) long sample at a magnetic field strength of 12T would be 410 N (92 lbf). This load is calculated using equation 3.1, where I is the current, B is the magnetic field strength, and f is the length of the sample. F = (I xB) (3.1) A distributed force of this amount would obviously distort an unsupported test strand that has a diameter of 0.81mm (0.032 inches) and the strength properties of annealed copper. This distortion would mean that a pure bending test would not be possible unless the strand was supported by some sort of structure that allowed it to be placed in pure bending while keeping it from being distorted by the Lorentz force. To support the strand, the test strand is placed on a support beam with sufficient stiffness to significantly reduce the amount of distortion caused by the Lorentz force. The pure bending motion is then applied by the bending mechanism to the support beam and the 89 Lorentz load forces the strand to conform to the radius of curvature of the beam. Thus, the support beam serves as a template for the pure bending of the test strand. The additional bending stiffness of the support beam is necessary to support the test strand but it also increases the amount of force that must be provided by the bending mechanism. Details of this support beam are given in the design section. Requirements 3. The mechanism should load the strand in a strain state that is as close to pure bending as possible over its designed operating range. An error analysis is used to optimize the configuration over the limits specified. 4. Costs to develop and build the bending mechanism should be kept as low as possible. Use of standard materials and practices will help to reduce costs. Tolerances should be generous enough so that expensive procedures are not necessary, but small enough so that dimensional inconsistencies will not create significant errors in the bending distribution. 5. The strand test length should be as long as possible because the characterization of superconducting strand is more accurate with longer samples. The test for the critical current of a superconductor consists of measuring the voltage drop across a sample length as the current is increased. The voltage drop is more difficult to measure in short samples than long ones because voltage is the line integral of electric field, which means that the voltage drop is greater for a longer sample. A higher voltage drop is preferable because it is easier for equipment to detect. In addition, noise from the environment is less likely to obscure larger voltage drop measurements. 90 Strand geometry is another reason why the test length should be as long as practical. As discussed in chapter 1, the strand is composed of twisted superconducting filaments that are rotated at a specific pitch within a copper matrix. The intent of the bending test is to characterize the properties of the bulk strand as a single entity. Therefore, it is important to have a long enough sample to accurately represent the average properties of the strand. Because the strand filaments are twisted, the minimum strand length should be at least several twist pitches long in order to capture the strain changes that the filaments experience as they rotate through the regions of compressive and tensile strain produced by the bending test. 6. The mechanism should be capable of loading the sample to a maximum bending strain of 0.7%, or possibly 0.9%, at the outer surface of the strand. Strain levels of these magnitudes have several implications on the design. First, for the given strand diameter and design test lengths this amount of strain requires the strand to be bent into an arc of more than 114 degrees for the case of 0.7% strain and 151 degrees for a strain of 0.9%. Second, the bending moment in the support beam is significantly greater at the higher strains than at the lower strains, produces large forces in the loading mechanism. The design of the mechanism and the materials must be able to withstand these forces while simultaneously meeting the other constraints. 7. The test sample must remain perpendicular to the magnetic field throughout the entire bending procedure. This orientation requirement is standard procedure for critical current measurements and more closely resembles the conditions that a Nb 3Sn strand would experience in a fusion magnet. 91 In strain-based critical current tests of short samples it may be possible to ignore the change in the orientation of the sample relative to the magnetic field as the sample is distorted. However, as reported above, the sample in the large-displacement bend test would be bent into a circular arc of 151 degrees. This would have a significant effect on the perpendicular component of the magnetic field that of each portion of the strand would experience if the bending plane were in the wrong orientation. Consequently, the mechanism must operate in the magnet so that the bending plane remains perpendicular to the magnetic field. For the same reasons this orientation is a requirement for the Lorentz force to consistently load the strand against the support beam. 8. The mechanism should be capable of cyclic testing where the bending load on the strand can be fully reversed. The loads on fusion magnets, such as the ITER central solenoid, are cycled. This cycling may cause fatigue degradation in the superconducting strand. A bending mechanism that is capable of fully reversible cyclic testing would be beneficial to studying this effect. 3.2 Bending Operation The mechanism design shown in figure 3.2 is the realization of the conceptual method for producing quasi-pure bending as introduced in section 2.5 (figure 2.8). This particular arrangement proved to be the most robust and versatile of all the configurations considered. It consists of a series of gears that translate the bending motion to the Support Beam holding the test sample. 92 Test Samples Support Beam Beam Clamp Input Shaft Coupler Torque Top Plate 4C3 CO (b) (a) Input Shaft i Thrust Bearing Plate Spacer Torque Gear Bottom Plate* 0 Drive Shaft (c) Fig. 3.2. Bending mechansim (a) complete mechanism, (b) with strand mounting system removed, and (c) inner gear train. 93 An 82 inch (208 cm) long shaft with an attached Hand Crank is connected to the mechanism via the Input Shaft Coupler. Rotating this shaft provides the torque to operate the bending mechanism. When the shaft is rotated, a worm on the end of the Input Shaft translates the input torque 90 degrees to the Drive Shaft wormgear. This wormgear motion causes the two Torque Gears that are connected directly to the Torque Arms to rotate in opposite directions. The Beam Clamps are connected to the Torque Arms which load the ends of the Support Beam when rotated. The relationship between the translation and rotation produce by the mechanism is chosen to produce quasi-pure-bending in the Support Beam over a large range of motion. This bending evolution is shown in figure 3.3 beginning with the initial, undeformed condition. The figure continues with Torque Arm angular rotations of 20, 40, and 70 degrees. This severe amount of rotation was not selected simply for the illustration but actually represents the deformed condition of the Support Beam at a strain state just below the maximum limit of 0.9% bending. 94 .1*. . K (a) 6 0. b) 9 (b) I. 0h (c) (d) Fig. 3.3. Bending Mechanism Operation (a) 0* rotation angle, (b) 200 rotation angle, (c) 400 rotation angle, and (d) 70* rotation angle for the Torque Arms. 95 3.3 Sample Mounting Assembly The sample mounting system consists of the Support Beam, the Beam Clamps, and Current Joints, as shown in figure 3.4. Three superconducting test samples are mounted in grooves that are machined into the Support Beam. Each of the three sample strands will be subjected to the same testing conditions and should produce similar bending characterization. But it is possible that one of the strands may be damaged before testing, resulting in a lower characterization. If only two strands were tested there would be no way to know if a lower characterization was simply because one strand had been damaged or whether the other strand was an exceptional sample. Therefore, a minimum of three strands were chosen to help with the comparison by providing an additional sample. Of course, more samples would be better but this is not practical due to the sizing restrictions on the mechanism and the amount of time that would be required to characterize more strands in the limited time slot scheduled for testing at the NHEMFL. Support Beam Beam Clamp Joint Block Test Sample Joint Wire Fig. 3.4. Strand Mounting System. 96 3.3.1 Support Beam The Support Beam is the backbone of the test samples. It has the dual purpose of supporting the strands against the Lorentz force while simultaneously serving as a template that uses this force to compel the strands into a bending state. The bending mechanism deforms the Support Beam to produce the desired radius of curvature rather than directly applying force to the fragile superconducting strands. The test strands are placed in grooves in the Support Beam so that they are adequately supported against the Lorentz forces through the full range of bending motion. The samples are not affixed to these grooves so that there is no shear coupling between the two components. Instead, the strand floats in the groove and relies on a combination of bending motion and the Lorentz force to keep the strand in the groove. The strand is held at the ends by a soldered joint underneath the Beam Clamps. The strand support grooves are machined to be at least as deep as the diameter of the strand so that the strand is not crushed and damaged by the Beam Clamps. This requires the Support Beam to be thicker than the strand diameter and thick enough so that additional material remains for moderate stress flow continuity. Machining grooves into a rectangular cross-section Support Beam has the effect of moving the neutral axis away from the initial position half way between the two outside surfaces. Moving the neutral axis means that when the beam is loaded in pure bending one surface will experience a higher magnitude stress state than the opposite face. Under these conditions a beam with the machined grooves will reach its elastic limit before an equivalent beam that was not machined. Additional machining of the Support Beam could be done to adjust the position of the neutral axis so that it coincides with the center of the sample. Any machining of the Support beam must be symmetric above and below the beam centerline so that a twisting moment is not introduced with the bending deformation. 97 Figure 3.5 shows the layout of the Support Beam. On one side (fig. 3.5a) of the beam, small grooves for the test samples run the length of the beam and connect to larger grooves at the ends. These larger grooves are for the transition joint between the superconducting samples and the copper current leads that provide the input power. The holes near the ends are for bolts that are used to fasten and align the Support Beam. These holes do not need to be symmetrical about the beam centerline because they are positioned within the region that is supported by the Beam Clamps. The opposite side of the beam (fig. 3.5b) has a series of grooves that move the geometric neutral axis of the beam to the center of the test samples. These adjustment grooves were designed to be a larger diameter and a shallower depth than the test sample grooves, which was done to reduce the potential stress concentrations and preserve the integrity of the Support Beam. Using shallower grooves required that six had to be machined to adjust the neutral axis rather than just three. K (a) Fig. 3.5. Support Beam Layout (a) Front View and (b) Back View. (b) 98 In addition to providing strand support, the Support Beam must have enough bending stiffness to render the effects of the Lorentz force on the bending distribution insignificant. The Lorentz force is a distributed load on the beam and creates an internal shear which modifies the bending distribution and introduces error to the bending state. To reduce this error, the Support Beam should be thick enough so that the internal moment distribution is almost entirely made up from the applied torque, thus reducing the significance of the Lorentz component. An analysis for estimating the effect of the Lorentz force on the bending distribution is presented in Appendix A. Unfortunately, the thickness requirements for the Support Beam have negative implications for both the strength of the bending mechanism and the elastic limit of the beam material. A greater bending stiffness means that the mechanism components must be able to withstand the larger forces. A thicker beam has surfaces at larger distances from the beam neutral axis, which means that the beam material must have an elastic limit high enough to sustain elastic behavior up to the maximum desired bending state. After an extended search of possible materials it was decided that the titanium alloy Ti6A14V had the best combination of properties for the Support Beam. Measured data for 0.064 inch (1.626 mm) thick Ti6A14V sheet in the annealed condition shows that the elastic strain limit increases from 0.73% at room temperature to approximately 1.4% at 4.2K, as indicated by figure 3.6 [3.3,3.4]. This high magnitude elastic strain limit is required for the Support Beam material because its additional thickness means that it experiences a larger strain state than the test sample. 99 20 Ti-6AI-4V 0, 064 IN SHEET ANN 240 42F -425F TO FT, L(4) To )OWF (3) RT 320 160 }RT ____ 120 20F 400F 80 TNOF 00F _______ IWXOF 40 'TENSION 0 0 0.004 G.008 0.012 STRAIN - IN PER 0.0It, IN Fig. 3.6. Stress-strain curves for Ti6Al4V annealed 0.064 inch sheet at various temperatures. The general expression for the strain in a beam as function of radius of curvature was derived in Section 2.1 and summarized by equation 2.5. It is restated here as equation 3.2 for convenience, recalling that the strain, s, is a function of the distance from the neutral axis, y, and the radius of curvature, p. = (3.2) This equation applies to both the test strand and the Support Beam which experience the same radius of curvature. However, the distance from the neutral axis of each of these components to their respective outer surfaces results in two different values for y. Applying equation 3.2 to the Support Beam and test strand and setting the radius of curvatures equal produces a relationship 100 between the strains in the two components, given by equation 3.3. This relationship is valid in general and can be applied to relate the strains at any position within the two components, but its use here will be limited to relate the maximum strains at the outer surfaces of the Support Beam and test sample. 6 beoam = Estrand Ybea (3.3) strand The geometry referred to by equation 3.3 is clarified by figure 3.7 where the distance from the strand's neutral axis to its outermost surface is given by ystrd. The parameter ybea is similarly the distance from the Support Beam's neutral axis to its surface. For the case of pure bending, the neutral axes of the Support Beam and test sample should be coincident to avoid axial strain in the strand. Neutral Axis Ybeam- Fig. 3.7. Support Beam and test strand distances from neutral axis to outer surfaces 101 Sheets of Ti6A14V alloy are rolled to standard commercial thicknesses and include 0.03125 inch (0.794 mm), 0.0625 inch (1.588 mm), 0.125 inch (3.175 mm), etc. The Support Beam cannot be made from the 0.03 125 inch (0.794 mm) sheet because it is too thin to fully contain the 0.81 mm (0.03189 inch) diameter strand. And the 0.125 inch (3.175 mm) sheet is too thick because it will result in surface strains beyond the elastic limit of the alloy when bent to the maximum strain state. For the Nb 3Sn strand to be tested to a maximum bending strain of 0.7% a sheet thickness of 0.0625 inch (1.588 mm) was selected. Inserting the values of ybeam= 0.03125 inch (0.794 mm), ysfrand= 0.01594 inch (0.405 mm), and Faad= 0.7% into equation 3.3 reveals that the strains at the outer surfaces of the Support Beam will reach a magnitude of 1.37%, which is just below the elastic strain limit of the chosen Ti6Al4V alloy at 4.2K. In addition, a Support Beam made from the 0.0625 inch (1.588 mm) sheet will have enough thickness for machining the strand grooves and sufficient bending stiffness to reduce the effects of the Lorentz load on the bending distribution. As part of the iterative design process, it was found that a Support Beam height of 2 inches (50.8 mm) would produce good bending stiffness while providing enough space to have adequate current joints for the three test samples. With the thickness and height of the Support Beam known, an estimate can be made of the amount of torque required to deform the beam to the maximum bending state. The internal moment, M, of a beam made from a material with an elastic modulus, E, and a moment of inertia, I, bent into a radius of curvature, p, was originally presented in Section 2.1. This expression is restated as equation 3.4. M = (3.4) p 102 The moment of inertia for a rectangular cross section beam is given by equation 3.5, where h is the beam thickness and b is the height. This equation provides an upper bound for the moment of inertia of the Support Beam because the actual beam will have machined grooves which reduce this value. I 12 bh' (3.5) Substituting equation 3.5 into equation 3.4 and combining the expression for the strain of the strand as a function of curvature (equation 3.2) yields the magnitude of the internal moment of the beam in terms of more convenient parameters, equation 3.6. In creating this equation, the term ystrand was replaced with half of the strand diameter, d/2. 1 Ebh 3 M = I-b 6 d (3.6) Esra Table 3.1. Values for estimating Support Beam torque. E (4.2K) b h d &strand 18.9 2.0 0.0625 0.03189 0.007 Mpsi inch inch inch in/in 130 0.0508 0.00159 0.00081 0.007 GPa m m m m/m An estimate for the torque required to deform the Support Beam can be found by substituting geometry and material properties into equation 3.6. These values for the Support Beam are outlined in table 3.1 and result in a required applied torque of 337 inch-lbf (38 N-m). This torque estimate was used to determine the gear strength requirements in the design of the bending mechanism. 103 3.3.2 Current Joints Electrical joints are used to transfer current coming from the power supply to the superconducting test sample. The current leads should have a rigid section that will support the strand against the Lorentz force and a flexible region that will allow for the movement of the bending mechanism. In addition, the joints should occupy as little space as possible in the magnet bore so that the test sample length can be longer. Combining all of the requirements for the current joints resulted in the design illustrated in figure 3.8. The small diameter test strand comes across the face of the Support Beam and makes a 90 degree bend at the end where it meets with the larger diameter copper Joint Wire. The strand is heat treated in this configuration to avoid the damage that would occur with trying to bend a straight section. The strand is soldered into a continuous machined groove in the Joint Wire so that it remains below the surface. A larger groove is machined in the Support Beam to accept the Joint Wire. The Joint Wire fits into a hole in the Joint Block where it is soldered. A bolt runs through the Joint Block, Support Beam and Beam Clamps to hold all of these components in position. A flexible cable, not shown in the figure, is soldered to the remaining hole in the Joint Block at one end and connected to a solid copper current lead at the other. This solid current lead runs through the probe to the outside room environment where it receives current from the power supply. This same style joint is used on all of the connections and provides a way to independently provide current to each of the samples. 104 WhIm (a) (b) Fig. 3.8. Current joint design with (a) All Components, and (b) Cut-Away View It is clear from figure 3.8 that there is no insulation between the Joint Blocks and the clamps. There is little concern for a short circuit across the Beam Clamps or Support Beam because of the large relative resistance of these components compared to the superconducting sample. The characterization of the sample will be completed before it fully transitions to a normal resistive state where current sharing would be an issue. Mounting a superconducting sample to a metal support system has been used in a majority of the strain-behavior critical current experiments. It was important from a current transfer standpoint to increase the length of the joints to be as long as possible. By including the 90 degree bends at the ends of the test samples, the total current joint length is greater than 1.0 inch (25.4mm) long. This increased length provides the additional distance needed to transfer the current between the copper wires and the test strand. 105 This particular design of the current joints was chosen so that the overall length of the test sample would be as long as possible in the magnet bore. Otherwise the 90 degree bends would have been avoided, because they greatly complicate both the heat treatment and mounting procedure for the strand. The voltage taps used for sample characterization measurements are placed so that they are not too close to the current joints. After the current passes into the strand at the current joint, it redistributes throughout the cross section of the sample for some distance. If the voltage taps were placed in this redistribution region, they would measure an apparent resistive component in the sample. This also reduces the measurement sensitivity. So it is important that the voltage taps be placed sufficiently far away from the current joints. To ensure enough space for current redistribution, a value of 1.0 cm (0.394 inches) was used for the distance between the end of the current joint and the position of the voltage taps [3.5]. 3.4 Strand Heat Treatment As described in section 1.4, the strand must be heat treated so that the niobium and tin will react to form Nb 3Sn superconducting filaments. Before heat treatment the strand is ductile and can be readily handled. But after heat treatment extreme care must be used in handling the strand so that the brittle Nb 3Sn filaments will not be damaged. The strands must be rigidly supported during the heat treatment process. A common technique for holding samples during a heat treatment is to use quartz glass tubing. However, the current joint design outlined in Section 3.3.2 requires a 90 degree bend and quartz glass tubing would not work because the samples could not be safely removed. A heat treatment fixture was designed for the test samples. It is shown in figure 3.9 and consists of a main fixture that has machined grooves for supporting and shaping the strand and a fixture cap that holds the strand in place during the heat treatment. 106 (a) (b) Fig. 3.9. Strand Heat Treatment Fixture, (a) Fixture and Cap, (b) Main Fixture The fixture is made from the titanium alloy Ti6Al4V. This material was selected because it has a lower thermal coefficient of expansion (CTE) than the strand, which means that as the fixture does not expand as much as the strand when heated. With the aid of the fixture cap, this expansion differential keeps the strand tight in the machined grooves throughout the entire heat treatment temperature range. This tight fit is essential to producing a strand with very straight regions and 90 degree bends. 107 The heat treatment fixture had to be made so that there was a precise fit with the fixture cap. Wire EDM (Electrical Discharge Machining) was used to make the parts to very accurate dimensions. The EDM process is independent from the mechanical properties of the material and, instead, depends on the thermal and electrical conduction. Wire EDM uses a thin brass wire as the electrode which continuously moves past the material being machined. The surface of the wire gets eroded away by the electrical discharge and so new wire is fed at a sufficient rate to keep the wire from eroding all the way through. Titanium does not have particularly good thermal or electrical conduction properties and can take a considerable amount of time to machine with EDM. The fixtures and caps took a total of 7 hours and 25 minutes of actual machining time on a Charmilles model ROBOFIL 240cc machine and consumed 2.217 miles (3568 meters) of 0.010 inch (0.254mm) diameter half-hard brass wire. The bend in the heat treatment fixture was designed with a radius of 0.125 inch (3.175 mm), which was considered the minimum acceptable bend radius for the superconducting strand. Bending the strand into too small of a radius would cause internal damage in the unreacted sample and significantly affect the performance after heat treatment. Before being heat treated, the internal tin design strand has regions of pure tin. This tin would melt and flow out of the strand during the heat treatment process if special precautions were not employed. When mounting the strand in the heat treatment fixture, a single continuous length is woven into the grooves and the two ends are extended beyond the fixture approximately 30 inches (76 cm) and crimped. Using a single piece of strand leaves only the two ends as possible routes for tin leakage. If tin does leak it will come from the extra length of strand which is discarded after the heat treatment. Figure 3.10 is an end detail of the heat treatment fixture that reveals how the strand is supported as it is wrapped in the grooves. The strand is placed in a groove and then wrapped around a tab on the fixture to reverse direction and continue onto the adjacent groove. These tabs also hold the strand tight in the grooves so that the fixture cap can be applied or removed without 108 disturbing the strand. The figure of the heat treatment fixture shows that it will hold six samples. This leaves three extra samples in case one or more are damaged during mounting. Fig. 3.10. Detail of heat treatment fixture end. As discussed in section 1.4, different strand designs require different heat treatment processes. Heat treating causes the component materials within the strand to react and form the Nb 3 Sn superconducting compound. Since there are various design geometries and techniques for making the strand, each one requires a tailored heat treatment schedule to create the best conditions for the reactions to take place. There are balances between heating the strand up incorrectly and causing internal voids, heat treating at too low a temperature and not allowing the tin and niobium to completely react, or heat treating at too high a temperature and forming undesired compounds such as excess bronze. A strand manufacturer relies on past experience and trial-and-error to develop the best heat treatment process that will result in the greatest current capacity or optimum AC loss behavior for the given strand design. Since the IGC and OST strands are slightly different designs, they must heat treated separately. A total of three different heat treatment fixtures were made to heat treat the various test samples: two fixtures of different test lengths for the IGC strand and one for the OST strand. The heat treatment schedules for these two strands and pictures of the actual fixtures are presented in Appendix E. 109 3.5 Mechanism Gear Design The entire bending mechanism, including the sample mounting system, is shown in figure 3.11. This design was the result after satisfying the numerous operational requirements. The bore size of the test magnet was the most important factor in the final geometry. Other factors such as achieving the longest test sample length, having three test samples, and including a strand Support Beam dictated the remaining parts of the quasi-pure bending mechanism. The final mechanism design emerged after an iterative process of adjusting the secondary components to satisfy the primary factors. The gear elements were the most significant secondary influence and governed the design of much of the mechanism. Ef Fig. 3.11. Bending Mechanism. 110 All of the components of the bending mechanism, except for the test strand and the Support Beam, are constructed from the same material. Using a single material eliminates the geometry relationship changes that would occur during cooling if the mechanism were made from materials with different thermal coefficients of expansion (CTE). Preserving the distance relationships is important for a machine that relies on geometry to create bending motion. Also, the accuracy and strength of the gears used in the mechanism depend on the separation distances between gear centers. By having a uniform material for the gears and gear housing, the changes in the gear center distances perfectly compensates for any changes in the gear dimensions. Austenitic 316 stainless steel was chosen as the material for the bending mechanism based on magnetic and strength properties. Although 316 stainless steel has a relative magnetic permeability of 1.008 its strength characteristics were superior to the other two material candidates, brass and aluminum. Using the higher strength material meant that the mechanism components could be made smaller, thus allowing for a longer test sample in the limited space magnet bore. The specific austenitic stainless steel choice of type 316 was due to its characteristics in a 4.2 K environment. Type 316 is often used in cryogenic applications because of its superior fracture toughness. It has high creep strength, a relatively low thermal conductivity, and better corrosion resistance than types 302 or 304. Many cryogenic applications use type 316L because the lower carbon content results in better welds. Welding is not necessary for the construction of the bending mechanism and regular 316 was selected because it is less expensive and more readily available. Applied torque from the Input Shaft has to be leveraged and directed to the sample Support Beam by the gear train. One of the requirements of the gear train is that it must rotate and translate the ends of the Support Beam in order to produce the bending motion. There are various gear systems that could have been used to create a mechanical advantage while producing rotations in opposite directions from a single rotation source, but none were as robust, 111 simple, and space conserving as the worm and wormgear. Originally a spur gear system was considered, but this required a much more complex arrangement with several stages of gears to have the strength and purpose of the simpler design shown in figure 3.12. With this design, the single worm on the Drive Shaft is able to simultaneously step down the gear ratio and rotate the Torque Gears in opposite directions. Input Shaft Drive Shaft Torque Gear Fig. 3.12. Bending Mechanism Gear Train. 112 The bending mechanism was designed to be as flexible as possible so that it could be used with various types of samples. This required the strong and interchangeable connections provided by the involute splines used on the Input Shaft and Torque Gears. Three different Sample Mounting Assemblies were prepared for testing on the bending mechanism. During the tests, the module design of the bending mechanism will allow the test samples to be quickly changed. The input torque for the bending mechanism is provided by hand rotation. Thus, the gear train does not need to be designed to operate at high speeds or for a large number of cycles. This reduces the effects of wear and fatigue on the gears and leaves only strength requirements. The tooth sizes for the bending mechanism were chosen based on the magnitudes of the loads throughout the gear train resulting from friction and applied torque. The tooth size chosen for the Torque Gears and the corresponding worm on the Drive Shaft determined the range of available diameters for these components. Sizing of the various gear components came after selecting the gear tooth sizes. There are several gear design practices that also contributed to the geometry. The most significant of these is that there should be at least 26 teeth on a wormgear to avoid undercutting of the teeth which reduces their strength [3.6]. This minimum number of recommended gear teeth sets a minimum diameter for the wormgear and worm for a given tooth size. Originally, the gear train was designed based on the ANSI (B6.9-1977) standard for singleenveloping fine pitch worm gears [3.7]. After contacting several gear manufacturers it became clear that custom tooling would need to be purchased to produce the gears that had been optimized to satisfy the bending mechanism requirements. In order to lower production costs, the bending mechanism was redesigned based on using helical gears in place of the singleenveloping wormgears. 113 Helical gears are not as strong as similar wormgears because they only have a single point contact with the worm as opposed to a line contact that distributes the load over a greater area of the tooth. Consequently, the finished gears were assembled and lapped with compound to create a wear pattern that helped to spread out the load. The gear train design had the greatest influence on the overall geometry of the bending mechanism. Determining the final geometry was an iterative process that was balanced by the other mechanism requirements. The equations that were used for the sizing and strength of the gear components are outlined in Appendix B. Gears made from stainless steel can be a problem from a friction standpoint: stainless steel is well-known for galling and cold-welding to itself under stress. Since shaft bearings and other materials could not be used to mediate the stainless steel interactions in the mechanism, there was concern that the thrust surfaces and gear teeth would be damaged and potentially fail if operated without lubrication. Standard lubricating methods could not be used in the cryogenic environment. Grease would not work at 4.2K because it would freeze and flake off of the surfaces. Brass bushings as the bearing surfaces would introduce an additional level of complication to the mechanism design because of the different thermal coefficient of expansion from the 316 stainless steel. A dry film lubricant was determined to be the best solution to the friction issues. Of the various dry film lubricants available, Molybdenum Disulfide was determined to be the best for the conditions. It is often used in cryogenic applications requiring motion and has a lower coefficient of friction at 4.2K than either graphite or Tungsten Disulfide [3.8,3.9]. 114 The bearing surfaces on the Upper and Lower Support Plates and the Thrust Plates were electroplated with silver to provide a good foundation that would reduce the coefficient of friction by introducing a dissimilar material from the stainless steel. Since silver cannot be directly applied to stainless steel, the surfaces were first coated with copper. After silver plating, powdered Molybdenum Disulfide was mixed with ethyl alcohol and sprayed on the gear components. It was then worked into the components by hand. The dry lubricant adhered to the silver coated surface far better than the stainless steel surfaces. 3.6 Probe Design The probe provides the support structure for the bending mechanism and instrumentation. It extends the mechanism into the liquid helium bath and positions the test samples at the field center of the magnet. The probe must have enough strength to resist the Lorentz forces and keep the various components aligned during testing and transportation. It should also be designed to minimize the amount of heat energy that is conducted to the liquid helium bath. Too much heat transfer will cause the helium to boil off quickly. The probe design for the bending mechanism is shown in figure 3.13. The bending mechanism is attached to the bottom and is positioned so that the center of the magnetic field coincides with the test samples. A helium fill tube is provided to transport the liquid helium from the helium Dewar to the bottom of the cryostat. Filling the cryostat from the bottom is much more stable and allows the helium vapor to cool the probe as it rises to the top and escapes to the atmosphere. 115 O M:ftfh_ G-10 Plates Flange Plate Helium Fill Tube Bending 41 1mechanism Flange Ie Insulation Plate Current Lead Tubes Hand Crank Fig. 3.13. Probe design. A hand crank is attached to a stainless steel shaft that connects to the bending mechanism Input Shaft. This provides the means for applying the torque to operate the bending of the samples. A series of stainless steel threaded rods connected by glass-epoxy Gi0 plates provide the probe structure. The GlO plates are excellent thermal and electrical insulators and remain stable in the cryogenic environment. The Flange Plate is where the probe attaches to the cryostat. The various shafts and tubes are electrically insulated from the cryostat by the GlO Flange Insulation Plate. Copper Current Lead Tubes are used to vent the helium vapor. They support the current lead wires and ensure that these wires remain as cold as possible to maintain a low electrical resistance. 116 -Cryostat Flange 41.50 -dQ ci I~FDI 9.75 7 74.13 Magnet Center 75.93 Mechanism Top Plate 06.650 74.13 88.00 Hel ium Fill Tube -FieId Center 89.75 (a) (b) Fig. 3.14. Drawings of (a) cryostat, and (b) probe. All dimensions are in inches. 117 The inside dimension of the magnet cryostat are shown in figure 3.14a. These dimensions were measured directly from the existing cryostat and are smaller then the drawings published on the NHMFL website. The important dimensions of the probe are given in figure 3.14b and show the distance from the probe Flange Plate to the bending mechanism Top Plate. This measurement was used to adjust the position of the samples in the actual probe. Probe instrumentation includes two liquid helium level sensors and a hall sensor. The liquid helium sensors are both 35 inches long. One is placed with its end at the bottom of the cryostat so that it will immediately register when the helium level begins to rise. This sensor also extends above the samples to show when they are immersed in the helium bath. The second sensor overlaps the first sensor in the region of the test samples and continues further up the probe. Including two sensors in the test region provides a backup in case a problem occurs with one of the sensors. Liquid helium sensors use NbTi superconducting wire to determine the helium level. Provided that the magnetic field intensity is low enough, the wire below the helium level is in a superconducting state and the portion of the wire above the helium level is held in a normal resistive state. The helium level can be measured from the resistance of the wire since only the normal portion is resistive. As the helium level rises, the resistance of the sensor linearly goes down. When the sensor is completely submerged it has zero resistance. Knowing the original length and normal resistance of the sensor allows the helium level to be determined. There are two types of helium level sensors. The four-wire sensors have a heater which keeps the portion of the superconductor above the liquid helium level in a normal state. The two-wire sensors use a significant amount of current (100 mA) to keep the upper portion normal. Instrumentation wires used in liquid helium must be insulated with PTFE (Teflon) in order to remain flexible. Other types of plastic insulation increase the risk of cracking and exposing the wires at the 4.2K temperature. 118 A Hall sensor is mounted in the probe to confirm the direction of the magnetic field relative to the test samples. It is important to make sure that the Lorentz force is in the correct direction so that the test samples are supported by the Support Beam. Following convention, the magnetic field should be directed from the floor to the ceiling. This is used to choose the direction of the current through the sample. This chapter has been focused on the most important design issues surrounding the bending mechanism, test samples, and probe. Consequently, all of the components have been presented as computer models in their designed form. The actual parts were fabricated from these models. Drawings showing the particular dimensions of the components are included in Appendix C. Pictures of the completed parts for the bending mechanism, test samples, and probe are presented in Appendix D. Chapter 4 Specifications and Test Results The previous chapter discussed many of the important design issues that had to be considered for the successful realization of a practical bending mechanism capable of performing strainbehavior characterization of Nb3Sn superconducting strand. This chapter presents specifics about the design and operation of the actual mechanism. Issues concerning the measurement and testing procedures are also covered. The testing results are discussed and followed by recommendations for further work. 4.1 Mechanism Specifications Recall that the accuracy of the bending mechanism depends on the ratio between the initial, undeformed, length of the sample, L8, and the distance separating the rotation axes, L,, as defined in figure 2.8 of section 2.5. This ratio has been designated by the nondimensional parameterf For ideal pure bending, the lever arms should change length with rotation to produce the appropriate displacement. But the practical bending mechanism uses a fixed lever arm length with a constant value off chosen to minimize the amount of error over the range of operation. 120 The bending mechanism was designed so that the lever arms (Torque Arms) and samples could be easily exchanged. This also gives the device the flexibility for use in a variety of different tests. Figure 4.1 a is a picture of the bending mechanism showing the removable Torque Arms mounted on splines extending from the Torque Gears below. The completed gear train is revealed in figure 4. lb when the Upper Plate is removed. Input Shaft Torque Arm 1V (a) 121 Torque Gear jF, Drive Shaft (b) Fig. 4.1. Bending mechanism (a) with removable Torque Arms and (b) gear train. For the characterization of the Nb3Sn strand, two different values off were chosen: 1.53 and 1.57. The valuef= 1.53 was selected because it was shown by the analysis in section 2.5 to have the smallest bending error over the operating range. The corresponding Torque Arms are stamped with "153" and are used for one set of the IGC samples and the OST (European) strand. The value off= 1.57 is used with a second set of IGC samples and Torque Arms marked with 122 "157." This value was chosen for two reasons: first, it is the same ratio that was used in a bending mechanism by previous researchers for characterizing high temperature superconductor [4.1]. Second, the error analysis for this particular ratio showed that it had the largest average bending error for lever arm rotations from zero to 900, but that at 90* the error suddenly drops to zero. It was important to include a test with a controlled bending error because it provided a way to quantify the effect that the displacement error had on the quality of the overall bending distribution through the sample. Using two Torque Arm lengths requires different samples and Support Beams. Detailed drawings are provided in Appendix C. The distance between the Torque Gear pivot axes, Lp, is a constant 2.9757 inches (75.58mm). Therefore, the free unclamped length of the Support Beam and test samples, L., is 4.5528 inches (115.64mm) forf=1.53 and 4.6719 inches (118.67mm) for f=1.57. Figure 4.2 shows an entire sample mounting assembly including the Support Beam, Beam Clamps, Current Joints and leads, and samples for the OST (European) strand withf=1.53. Fig. 4.2. Sample mounting assembly for OST (Eurpean) strand withf= 1.53. 123 The Beam Clamps on each end of the Support Beams are 0.700 inches (17.8mm) wide with bolt holes drilled through the centers. Consequently, the alignment holes for the Support Beam are spaced 5.258 inches (133.4mm) apart forf=1.53 and 5.372 inches (136.4mm) forf=1.57. The test samples make a 900 bend (with a 0.125 inch radius of curvature) around the outside of the Beam Clamps to achieve the longest possible Current Joint length. The portions of the strand underneath and to the sides of the Beam Clamps are soldered into a groove on the copper Current Joints. Figure 4.3 shows the configuration of the Current Joints on the Beam Clamp and the mounting groove for the sample. The outer surface of the mounted sample is coincident with the sides of the Beam Clamps, giving an overall outside strand dimension of 5.953 inches (151.2mm) forf=1.53 and 6.072 inches (154.2mm) forf=1.57. (b) Fig. 4.3. (a) Current Joint mounting configuration, and (b) sample current-joint groove. 124 These dimensions for the bending mechanism components were driven by a combination of all of the operating requirements. The primary design objective to achieve the longest sample length possible in the limited magnet bore was followed closely by the strength requirements of the gear train. The sample mounting assembly forf=1 .57 represents the longest configuration that can be used in the mechanism without colliding with the Input Shaft or cryostat. There are marks on some of the bending mechanism components to show the required orientation for producing symmetric bending. These marks are used during assembly to ensure that the parts are aligned correctly. The letter "A" is stamped on one Torque Arm and one Torque Gear. This means that those components go on the "Actuator" side of the mechanism, which is the side with the Input Shaft. The symbol "0" is stamped on the Torque Gears at the base of a single gear tooth. This means that those teeth should be pointing towards each other in the same worm thread on the Drive Shaft when the gear train is assembled. There are slashes, near the splines of the Torque Gears and Torque Arms. The Torque Arms should be positioned on the Torque Gears so that these slashes are aligned. 4.2 Support Beam Specifications The groove for holding the sample in the Support Beam was not machined deep enough to place the center of the sample coincident with the centerline of the beam. A groove 0.048 inches (1.23mm) deep would have to be machined in the 0.065 inch (1.588mm) thick Support Beam to have the center of the 0.03 2 inch (0.81mm) diameter strand lie at the centerline of the beam, leaving only 0.017 inches (0.35mm) of wall material. This would have resulted in high stress concentrations at that location, causing the Support Beam to fail. Recall from section 3.3.1, that this size of Support Beam was the thickest that could be used in the bending mechanism based on the maximum strain limit of the Ti6Al4V alloy. 125 The actual sample groove was machined to a depth of 0.036 inches (0.91mm), placing the center of the 0.032 inch (0.81mm) diameter strand 0.012 inches (0.3mm) from the centerline of the Support Beam. To compensate for the offset of the sample centerline, grooves on the opposite side of the Support Beam were machined so that the geometrical neutral axis of the beam was coincident with the sample center. The relative position of the strand centerline to the Support Beam is illustrated in figure 4.4. A machined Support Beam showing the sample grooves, current joint grooves, bolt holes, and compensating grooves is shown in figure 4.5. Geometrical Neutral Axis IamleSupport Sample Beam cross-section Half-way between Beam Surfaces Fig. 4.4. Position of sample in Support Beam. 126 (a) (b) Fig. 4.5. (a) Sample side of the Support Beam, and (b) end of Support Beam showing compensating grooves. 127 4.3 Strain Gages Strain gages were placed along the length of the Support Beam to measure the bending distribution. Each side of the Support Beam had gages mounted at the centerline and at the ends near the Beam Clamps. The end gages were positioned a distance of 1.75 inches (44mm) from the center of the Support Beam for thef=1.53 samples and 1.81 inches (46mm) for thef=1.57 samples. Because of the position of the strand and compensating grooves, the gages on the sample side were at a different elevation than the corresponding gages on the opposite side. This did not significantly affect the measurements because the bending deviations occurred along the length of the beam, and not in the vertical direction. The strain gages served as an independent check on the bending distribution in the beam. They were not critical components because the rotations of the input shaft were the primary method for setting the strain state of the mechanism. Instead, the strain gages were used to measure the deviations from pure bending. Each of the gages should, ideally, measure the same amount of strain if the beam is in pure bending. When simply checking for a pure bending distribution, it is only important that the gages are within an expected tolerance of each other. However, to compare the quality of the bending distribution relative to the expected distribution from the rotations of the Input Shaft, the strain gages needed to provide accurate values. This was a significant issue in the 4.2K liquid helium bath with a 12T magnetic field. The strain gages selected were series WK-13-125AD-350 from Vishay Micro-Measurements Group. These gages have a nominal resistance of 3502 and an active gage length of 0.125 inches (3.18mm). The grid material is a nickel-chromium alloy used for more extreme test environments with a uniaxial grid pattem. The gage backing material is a glass-fiber-reinforced epoxy-phenolic that encapsulates the grid alloy. 128 It is important to control the amount of heat transfer from the strain gage to the liquid helium in order to have a constant environment that will give consistent measurements. If there is too much heat transfer, the helium can go into a nucleate boiling regime and affect the resistance of the gage giving erroneous results. The WK series gage was selected because the epoxy encapsulation over the grid material acts as an insulation barrier that helps to diffuse the electrical heat generated before it reaches the helium on the surface. The 350 ohm rating of the gage was chosen to limit the amount of power generation while still providing enough sensitivity. It is also important that the excitation voltage for the gages be kept low enough to not heat up the gages significantly. Micro-Measurements supplies gages with a self-temperature-compensating property. The gages can be chosen to have an approximate thermal coefficient of expansion that matches the test material at the testing temperature. This self-temperature-compensation (STC) property changes in a nonlinear fashion with temperature and so a material match at one temperature may not apply at another temperature. The gages selected for measuring the Support Beam bending distribution have an STC property that correlates to aluminum alloys near room temperature, but changes to a value that closely matches the titanium alloy used for the beam at the 4.2K testing temperature. The Gage Factor (GF) of the strain gage changes with temperature. At room temperature the purchased matched set of gages had a GF of 2.06. The included literature showed that the GF changed linearly with temperature according to a temperature coefficient of GF equal to 1.0%/100'C. Dropping from room temperature at 24' C to the -269' C testing environment meant that the appropriate GF for the strain gages was 2.93% greater, or equal to 2.12. The adhesive selected to install the gages was Micro-Measurements M-Bond 610. This is a twocomponent epoxy-phenolic adhesive that must be cured at an elevated temperature. The operating range of the adhesive allows it to be used reliably at 4.2K. At this temperature it has an elongation limit of 1% which is lower than the intended 1.4% strain that the Support Beam 129 experiences. However, the gage itself has a recommended strain limit of 1.0% at -195' C (-320'F) so the governing restriction was not the adhesive. After appropriately cleaning the beam surfaces, the strain gages were applied using the M-Bond 610 adhesive which was then cured at a temperature of 1770 C (350' F) for 1 hour. An instrumentation box was designed and built to use for the strain gage measurements. This box was capable of measuring up to 4 strain gage circuits simultaneously using parallel Wheatstone bridge configurations. It had provisions for the bridge balancing and voltage outputs for the data acquisition system. The strain gages could be connected in a double-bridge circuit or a single-bridge by including a dummy resistor. The double-bridge was set up so that any noise or temperature effects would be canceled out. This circuit utilized strain gages mounted on opposite sides of the Support Beam with one in tension and the other in compression. This resulted in an output with double the strain magnitude which eliminated the ability to observe the strain levels on the individual faces of the beam. 4.4 Bending Mechanism Verification It was important to test the operation of the bending mechanism before performing the characterization tests on the Nb 3 Sn samples. The quality of the bending distribution in the Support Beam was checked both at room temperature and in a liquid helium bath. These tests showed that the mechanism would develop a bending distribution throughout the beam that remained within 15% of the intended bending state. The bending state for this experiment is defined as the maximum strain magnitude that occurs on the outer surface of the test strand. It is not the strain state of the Support Beam. The IGC and OST (European) Nb 3Sn internal-tin test samples have an outer copper stabilizer sheath surrounding the inner portion with the superconducting filaments. Consequently, the defined bending state refers to the strain at the surface of this copper layer rather than the bending state in 130 the filaments. This definition is consistent with other strain behavior characterizations because it treats the technological strand as a single unit instead of trying to separate out the strain states of the filaments. In reality, the strain state of the individual filaments is very complicated even in uniaxial testing because of the different materials present and the twisting of the filaments. For the bending tests, the defined strain state of the mechanism was controlled by the number of rotations of the Input Shaft. The relationship between the strain state of the sample and the Input Shaft rotations is derived as follows: The magnitude of the desired strain state, c, is related to the test sample diameter, d, and the radius of curvature, p, by a modification to equation 2.5, which is given by equation 4.1. 6 =- s 2p (4.1) The geometric relationship between the arc length of the sample, Ls, the radius of curvature, and the subtended angle, a, was expressed as equation 2.7 and is restated as equation 4.2 for convenience. L, = po (4.2) For the bending mechanism, the angle of rotation for one of the Torque Arms, 0, is equal to twice the angle of the bending arc, a, as described in section 2.4. Using this fact and combining equations 4.1 and 4.2 yields equation 4.3, which shows the amount of rotation for the Torque Arms to achieve the desired strain state in the strand. 0= C d, (4.3) 131 The rotation of the Torque Arms is controlled by the 36-tooth Torque Gears which are connected to a 1-tooth worm. This worm is fixed to a 27-tooth wormgear on the Driveshaft which is fed by the 1-tooth worm on the Input Shaft, making for a total gear ratio of 972 to 1 or n=972. Equation 4.4 gives the number of rotations of the bending mechanism Input Shaft that are required to place the test strand in a desired bending strain state, where 27C is included to convert the angle to rotations. Of course, the length dimensions must be in the same units. Rotations of Input Shaft = n C 27d, (4.4) The maximum strain magnitude on the outer surface of the Support Beam is related to the strain level of the test sample by equation 3.3, which has been modified in terms of the diameter of the strand, ds, and the thickness of the beam, db, to produce equation 4.5. Ebeam = Estrand (4.5) Tables 4.1 and 4.2 were generated with equations 4. lthrough 4.5 to show the number of Input Shaft rotations for a range of strain states, along with other parameters, for the two different length test samples corresponding to values off=1.53 andf-1.57, respectively. These tables were used to set the strain states for all of the bending tests. 132 Table 4.1. Bending mechanism shaft rotation/strain state forf=-1.53. Ratio,f 1.53 Sample Length (in) 4.55282 Strand Diameter (in) 0.03189 0.065 Radius of Curvature (inches) 00 Beam Thickness (in) Strand Strain Beam Strain (%) 0 0.10 0.20 0.30 (in/in) 0.40 0.50 0.60 0.70 0.80 0.90 0 0.002038 0.004077 0.006115 0.008153 0.010191 0.012230 0.014268 0.016306 0.018344 15.95 7.97 5.32 3.99 3.19 2.66 2.28 1.99 1.77 Torque Arm Angle (deg) 0 8.18 16.36 24.54 32.72 40.90 49.08 57.26 65.44 73.62 Rotations of Input Shaft 0 22.09 44.17 66.26 88.34 110.43 132.51 154.60 176.69 198.77 Table 4.2. Bending mechanism shaft rotation/strain state forf=1 .57. Ratio,f Sample Length (in) Strand Diameter (in) Beam Thickness (in) Strand Strain (%) Beam Strain (in/in) 0 0.10 0.20 0.002038 0.30 0.40 0.50 0.60 0.70 0.80 0.90 0 0.004077 0.006115 0.008153 0.010191 0.012230 0.014268 0.016306 0.018344 1.57 4.67185 0.03189 0.065 Radius of Torque Rotations Curvature (inches) 00 Arm Angle of Input (deg) 0 Shaft 0 15.95 7.97 5.32 3.99 3.19 2.66 2.28 1.99 1.77 8.39 16.79 25.18 33.58 41.97 50.36 58.76 67.15 75.54 22.66 45.33 67.99 90.65 113.32 135.98 158.64 181.31 203.97 133 4.4.1 Room Temperature Verification The room temperature bending verification test was done to visually check the operation of the mechanism before attempting an enclosed liquid helium test. The bending mechanism was attached to the end of the test probe and actuated using the hand crank. The test incrementally went from the initial zero strain state to a maximum state of 0.8% bending strain. It was known beforehand that this magnitude of strain state would result in plastic deformation of the Support Beam due to the lower elastic strain limit of the titanium alloy at room temperature. So a beam with a minimal amount of investment in machining was used for the testing. Figure 4.6 shows the bending mechanism with the trial Support Beam at a sample strain state of 0.7%. This corresponds to an arc-angle of 114.5 degrees with a surface strain on the beam of 1.43%, which is greater than the 0.73% elastic strain limit at room temperature. Fig. 4.6. Room temperature test of bending mechanism. 134 As the Input Shaft was rotated, the curvature of the trial Support Beam was periodically checked with curved templates that had been previously machined. These showed the bending distribution to be very close to the strain setting along the entire length of the beam. As the bending continued to be applied, this quality of distribution degraded due to the inherent errors of the bending mechanism and the fact the Support Beam was beyond its elastic limit and was being plastically deforming. This plastic deformation served to relieve the strain in the center of the Support Beam and reduced the overall curvature. This effect was significant as can be seen by the permanent deformation of the beam shown in figure 4.7. Fig. 4.7. Permanent deformation of Support Beam tested at room temperature. At a sample strain state of 0.8%, the amount of torque required to adjust the bending mechanism was measured. A torque of 2.5 ft-lb (3.39 N-m) was needed to apply any additional bending via the Input Shaft, which was well within the design strength limits of the mechanism. 135 4.4.2 Liquid Helium Verification The gears of the bending mechanism were coated with a Molybdenum Disulfide dry-film lubricant before testing in the liquid helium bath. This replaced the grease that had been used for the room temperature test. A new Support Beam with all of the required machining was used for this test. It was important to have both the sample grooves and adjustment grooves to check if the stress concentrations would cause a beam failure. Strain gages were applied to the beam to measure the strain distribution and test the probe wiring and data acquisition system. Fig. 4.8. Probe and cryostat for the liquid helium bending mechanism verification test. 136 The test proceeded in a similar manner to the room temperature test with the Input Shaft being successively rotated to the desired sample strain level. Two liquid helium level sensors in the probe ensured that the Support Beam was immersed in a helium bath before proceeding with the test. Figure 4.8 shows the probe in the cryostat with helium gas escaping and condensing the atmospheric vapor. Fig. 4.9. Support Beam tested in liquid helium bath. As expected, the Support Beam was not plastically deformed when bent to the maximum strain state as revealed by figure 4.9. However, several of the strain gages either broke, causing an open circuit, or delarminated from the beam surface. The liquid helium testing was very useful because it exposed several issues that needed to be improved. Most important, the mounting of the strain gages was modified so that they would be more likely to provide reliable data at the higher strain levels. The changes included mounting and curing the strain gages on one side before applying the gages to the other side. This two-step procedure was preferable to mounting all of the gages simultaneously because it allowed the clamps holding the strain gages to be placed more securely. Other changes included adding strain reliefs to the gages so that there would be less tension on the wiring during testing. 137 4.5 NHMFL Facilities The various magnets at the National High Magnetic Field Laboratory for use by visiting researchers are placed in separate rooms, or cells. The magnets are at the rear of their respective cells and are surrounded by an elevated fiberglass deck that provides access to the magnet bore. The front portion of the cell, in the low-field region near the entrance, is open for testing equipment and instrumentation to be set up. Figure 4.10 shows a picture of Cell 4, which holds the 20T 190mm bore magnet. Fig. 4.10. Cell 4 at the National High Magnetic Field Laboratory. 138 The NHMFL also provides users with tools, instrumentation, and data acquisition systems upon request. For the bending strain characterization tests, this included 8 Keithley model 2182A digital voltmeters, a 1500A current power supply, and a computer running a NHMFL customprogrammed LabVIEW application with up to 20 channels of data sampling. Fig. 4.11. Screen shot of testing control computer. Figure 4.11 is a screen shot of the computer used to control the magnet and collect the measurement data. The data acquisition program in this picture shows a plot of the voltage vs. current measurement for one of the bending test samples. The window with "Cell 4" contains the controls for the magnet. From this window the user can specify the magnetic field level and has the ability to fully reverse the magnetic field direction. It also provides control for ramping the magnet between two field levels at a specified rate. 139 There are limits to the magnets which are set by the physical characteristics of the magnet and the power supplies. Each magnet has a maximum field level and ramp rate. To produce a 12T field the 20MW 20T 190mm bore magnet requires 23.5kA, 11.74kA for 6T, and 0.097kA for 0.05T. At 12T the three coils in the magnet have voltages of 91.33V, 127.92V, and 56.16V. A fault control system keeps the magnets from being damaged. This system measures key parameters in the magnet including the coil currents, coil voltages, coil temperature. It also monitors the water used to cool the resistive Bitter magnet by keeping track of the inlet temperature and pressure and the outlet temperature and pressure. Anything that causes these parameters to go outside of their tolerance limits will trip the system. When the fault system is tripped control is automatically transferred from the user to the control room. The control room then runs some tests to check the condition of the magnet before retuming control to the user. The fault control system is particularly sensitive to fluctuations in the coil voltages. The user tests must be insulated from the magnet so that a stray current from an extemal power supply does not trip the system. A small amount of noise in the magnet power supply may also trip the fault system. Because the magnet power supplies are designed to provide constant current over a large range, they have difficulty at the zero field setting. If left to dwell at this level for a small amount of time, the power supplies will fluctuate enough to trip the fault control system. As a safety precaution, the user must bring down the magnetic field intensity before making adjustments to the test sample. To avoid tripping the system, the magnet can be set to a field level where it is low enough for the user to make adjustments but high enough so that the power supply has low voltage noise. For the 20T 190mm bore magnet this setting was a field intensity of 0.05T. 140 4.6 Sample Testing Preparation The support system for the bending test is the probe. Figure 4.12 shows the completed probe set up with the bending mechanism and ready for being placed in the magnet cryostat. Foam pieces have been installed near the top Flange Plate to reduce the amount of heat transfer caused by the convective flow of the helium gas. Fig. 4.12. Bending test probe. 141 Before a test, the Sample Assembly is mounted to the bending mechanism on the end of the probe. All of the necessary current leads and instrumentation wiring are then connected. The Sample Assembly consists of the Support Beam, Beam Clamps, Current Joints with leads, and 3 separate bending samples. After attaching the Sample Assembly and bending mechanism to the probe, all of the electrical connections were checked and then insulated with mylar tape. Figure 4.13 shows the Sample Assembly and bending mechanism attached to the end of the probe and ready for being inserted into the magnet cryostat. The GI 0 plate attached to the bottom of the bending mechanism has a slightly larger diameter and was used to electrically insulate the mechanism from the wall of the cryostat. One of the liquid helium level sensors can be seen in the figure as the tube with the series of holes. Fig. 4.13. Bending Mechanism and Sample Assembly attached to probe. 142 Figure 4.14 shows the routing path of the current lead wires. A portion of the current lead wires had to be flexible to allow for the bending motion of the samples. An 8 AWG copper cable made from 30 AWG strands was chosen for the lead wires to provide the most flexibility while transporting the current. The original insulation for these wires was stripped off and replaced with PTFE (Teflon) tubing. The lead wires were approximately 18 inches (45cm) long and were bolted to solid copper blocks mounted on a GI0 plate. Fig. 4.14. Flexible current lead wires. Figure 4.15a shows the copper blocks on the probe that are used to attach the current lead wires. Each block was drilled and soldered to a high purity copper insulated Westinghouse magnet wire that passes through the GI0 plate and continued through a tube, extending outside of the probe. These wires were used to supply current to the samples. Figure 4.15b shows these connection points with the flexible current lead wires attached. 143 (a) (b) Fig. 4.15. (a) Attachment points for current lead wires, and (b) attached current lead wires. 144 After all of the testing preparations on the probe were completed, it was lifted by an overhead crane and carefully lowered into the magnet cryostat. The current lead wires were then bolted to 2-gage welding cables. These cables extended to the sample power supply and provided a way to select which sample was being tested without having to shut down the magnet. The other instrumentation wires for the helium level sensors, Hall sensor, sample voltage taps, and strain gages were then routed to the instrumentation table and connected to the data acquisition system. jj:iikt Fig. 4.16. Probe mounted on magnet cryostat. 145 Figure 4.16 shows the probe mounted on the magnet cryostat along with the hand crank used to adjust the strain level of the samples. Because of the position of the hand crank in a region of relatively high magnetic field, the magnet had to be shut down before the strain could be adjusted. Figure 4.17 is a picture of the magnet cryostat being filled with liquid helium through the probe. The outer shell of the magnet cryostat had been filled with liquid nitrogen well in advance to lower the temperature as much as possible before filling with liquid helium. The picture shows the helium transfer line and the two 250 liter Dewars that were used to maintain the helium level for the duration of the testing. Fig. 4.17. Transferring liquid helium to the cryostat via the probe. 146 4.7 Sample Characterization The bending mechanism and probe were created to measure the change in the critical current of Nb3Sn strands with an applied bending strain. Critical current testing of superconducting strand is done to determine the current value where the strand transitions from a superconductor back to a normal resistive state under a specific set of conditions. The transition does not occur instantaneously, but happens over a range of currents. Consequently, the critical current is determined using a selected critical value electric field, Ec. The current that corresponds to this amount of electric field in the test sample is the critical current, I. A critical current test consists of measuring the voltage across two points of the sample as an applied current is slowly increased. For the majority of the test, the current through the strand is increased with no apparent increase in the measurement voltage. But as the current levels approach the transition region of the superconductor, the voltage begins to increase. Depending on the behavior of the test sample this voltage can appear suddenly and increase rapidly or it may be a slow increase drawn out over a larger range of applied current. This behavior is a function of the design of the test sample and the conditions that it is under. It is also related to the distribution of the many superconducting filaments within the resistive bronze matrix that makes up a technological Nb 3Sn strand. The measured voltage is related back to the electric field criterion, E0 , by the test distance between the sample voltage taps. The electric field is equal to the voltage divided by the distance between the voltage taps. Therefore, a longer sample produces a larger voltage than a short one for the same electric field level. This is important when significant noise may be present in the measurement and E, is relatively low. The ITER criterion for critical current testing is E,=O.1 V/cm. This is a level that is appropriate for test samples that are 0.5 to 1.0 meters long. The standard ITER J barrel test uses a test 147 sample length of 0.5m. When testing shorter samples that are on the order of centimeters or millimeters, it may be necessary to use a larger field criterion such as 1 .O V/cm or 2.0pV/cm. Because of the relatively short length of the bending strain samples, an electric field criterion of Ec=2.OpV/cm was used for determining the critical current. This value was chosen because it has been used by other researchers, including Ekin, for strain characterization tests. The distance between the voltage taps on the bending test samples are approximately 4.30 inches (11cm), meaning that the critical current will be measured near a voltage of 22gV (2.20x104 V). In addition to determining the I,, the characterization test can be used to derive the n-value of the sample. The n-value is an exponential parameter relating the changing electric field, E, in the sample to the changing current density, J. This relationship is shown by equation 4.6. This expression could also be stated using voltage in place of electric field and current in place of current density because they differ only by the constants of length and area, respectively. -= - J (4.6) The n-value describes the exponential transition of the strand from the superconducting state to the normal state. A large n-value means that the transition occurred very quickly; the electric field increased rapidly over a short current range. A small n-value signifies a slower transition over a longer range of current. Generally, a large n-value also means that the strand has a higher critical current. When determining the n-value from a characterization test, the critical values are used for E (or V,) and J, (or Ic). A second point is then chosen at an E (or V) and its corresponding J (or I) either above or below the critical point. These values are combined to calculate the n-value from equation 4.6. 148 Both the critical current, I, and the n-value of the test sample should change as the applied bending strain varies. With uniaxial tension tests these values both increase up to an approximate applied strain of about 0.3% before they decrease. These values tend to become lower with subsequently applied strain cycles. It is anticipated that the bending test will exhibit a similar behavior where the L and n-value increase up to some applied strain value and then decrease. 4.8 Critical Current Results Three separate test runs were scheduled for the bending strain characterization tests over a period of three days. After preparing the probe with one of the three Sample Assemblies and filling the cryostat with helium, the testing window for the magnet power supplies was approximately 7 hours. In that time the three strands in the Sample Assembly were tested over the entire bending strain range. The probe was then removed from the cryostat and allowed to warm up to room temperature before the Sample Assembly was exchanged the next day in preparation for the evening tests. The first samples to be tested were the IGC samples withf=1 .53 (IGC153). These were followed by the IGC samples withf=1.57 (IGC 157) and then the OST (European) samples withf=1.53 (EU153). The testing on the first day was limited due to several problems that occurred. There were problems with the liquid helium sensors in the probe and the power to the magnet was shut down for extended periods. The tests were also limited by a combination of high sample noise and the voltage taps on the samples breaking loose. Consequently, a consistent range of data was not collected from any of the samples from the first day of testing. For the subsequent tests, the voltage taps were reattached with allowances made for strain relief using 30 gage magnet wire instead of the previous 22 gage wire. 149 The unexpected behavior of the samples at the lower strain levels on the first day helped with the anticipation of this effect on the second day. At the lower strain levels, the samples either quenched or transitioned at lower than expected current levels. It was possible that this was caused by the loose mounting of the samples in the Support Beam grooves. The samples had been carefully mounted so that they would not be damaged by handling. But this left them unsupported and probably allowed them to shift as the Lorentz force increased during the characterization testing. This low-current phenomenon occurred with all of the samples, including those that appeared to be mounted securely in their support grooves previous to testing. This low critical current behavior continued with the additional application of bending strain. At the higher bending strains the test samples were able to settle into the Support Beam grooves. But this did not change the low current trend in the measurements. However, as expected, the critical current increased up to a point before it began to decrease. Some of the sample measurements had large amounts of noise, which limited the useful data that was collected. When this occurred, the sample was retested in an attempt to collect better data. In some of the cases, the noise in subsequent tests was low enough to provide acceptable measurements, but in most cases the noise remained. The most extreme noise appeared in the measurements around the same time each evening and remained until the magnet time was over. Unfortunately, this time consistently corresponded to the lower strain measurements where the strand had first been loaded and then unloaded. To provide a sense of the amount of noise encountered, figure 4.18 shows voltage-current measurement plots for IGC 157, Samplel. Figure 4.18a is for a strain state of 0.2% after being unloaded from the maximum strain. In this plot, the transition region is clearly visible before the sample quenches. Figure 4.18b is the same sample measured 15 minutes later at a strain state of 0.1%. It is clear from the figure that the noise is too significant to provide any useful information. Much effort went into trying to determine the source of the noise with no success. 150 1GC157 Sample #1, 0.2% Strain 1.OE-04 8.OE-05 6.OE-05 4.OE-05 2.OE-05 0 - , w% nA 0.OE+00 -2.0E-05 -4.OE-05 -6.OE-05 -8.OE-05 -1.OE-04 i 0 2 20 4 40 -T 60 - 8r 1 12 80 100 120 140 - 140 Current (A) (a) IGC 157 Sample #1, 0.1% Strain 1.OE-04 8.OE-05 6.OE-05 4.OE-05 2.OE-05 - 0.OE+00 0 > -2.OE-05 -4.OE-05 -6.OE-05 -8.OE-05 -1.OE-04 0 20 40 60 80 100 120 140 Current (A) (b) Fig. 4.18. Voltage-current plots for IGC157 Sample #1 (a) 0.2% strain, and (b) 0.1% strain. 151 The voltage-current plots for the three IGC 157 samples were measured initially with no bending strain applied. The bending strain was then increased to a sample strain of 0.1% and voltagecurrent data was again collected for the three samples. This continued in 0.1% strain increments up to a maximum strain of 0.7% at which point, the strain was released in the same incremental steps with measurements being taken at each step. The testing of the EU 153 samples occurred in a similar pattern with the strain increasing in 0.1% incremental steps up to 0.7% before it was reduced. At the initial zero bending strain level, each of the EU 153 samples quenched before transitioning to the critical electric field criterion of E,=2.0[tV/cm. This quenching continued for each of the samples up to an applied bending strain of 0.4%. After this point the samples did not quench as early and critical current data was able to be collected. Figures 4.19 through 4.24 are plots of the critical current data and n-values for the IGC 157 and EUl 53 samples tested. The samples were numbered according to their positions on the Support Beam: Sample #1 was positioned at the top with #2 in the middle and #3 at the bottom. Any gaps in the plots are because the data was not available. IGC 157 Sample #3 has a limited set of data because a voltage tap broke off when it was loaded to a bending strain of 0.3%. The data points are connected by lines to clarify successive data points and there are separate lines which designate loading or unloading of the sample. Loading refers to the applied strain being increased from an initial strain value of 0%. Unloading is the release of the strain from the maximum value of 0.7% and returning to the zero state. All of the testing was performed at the liquid helium temperature of 4.2K. The IGC157 samples were measured in a background magnetic field of 12T, while the EUl 53 samples had an applied field of 13T. The larger magnetic field for the EU153 samples was selected to reduce the amount of current in the lead wires. The lead wires had been designed to sustain a maximum 152 current of 200A and it was possible that the EU strand would have a critical current above this value at the lower field 12T field. At the initial low strains, the EU 153 samples quenched before reaching the critical electric field criterion. Thus, the data is presented as the quench values. These same samples did show a transition at the lower strain levels when the sample was unloaded. The n-value data is presented in terms of two different definitions shown as nI and n2. Both nI and n2 data was calculated using equation 4.6 with the critical electric field criterion of Ec=2.OgV/cm and the corresponding critical current, I. The lines designated by n1 were calculated using equation 4.6 and a second electric field value of E=3.5[tV/cm with its corresponding current. The lines designated by n2 used a second electric field value of E=7.1 IV/cm. The reason for presenting two separate n-values is because many of the samples would quench soon after they had reached the critical electric field criterion and measurement data was not available for the preferred n2 points. Consequently, the n1 points were calculated using a lower secondary electric field point that was available for most of the test samples. But even some of samples quenched before reaching the lower electric field level of ni, leaving gaps in the data plots. It is interesting that the values of ni and n2 are very similar for most of the strain states in a given sample. These plots are a brief summary of the data that was collected. More of the test data information is presented in the tables included in Appendix F. As a reference, critical current measurements have been made for the IGC and OST strands using the standard ITER Jc barrel test. For the condition of zero applied strain and a 12T magnetic field, the critical current of the IGC strand has been measured at I = 144A, with an n-value of n = 33 [3.10]. The critical current of the OST (EU) strand was recently measured at Ic = 247A under a zero applied strain and a 13T magnetic field [3.2]. The critical electric field for these measurements used the ITER standard of Ec = 0.1pV/cm. 153 Ic, IGC157 Sample #1 ------- --- --- -- 140- -- 120 - ---------- ----------- ----- -----100 --- 8- - -L-- z .2 80 - ------60 - - 6 ------ ---------------- s ------------- ------- ---- -a-Unloading ----------------------------- 40 U---- Loading ----------------------- 20 0 0. 0 0.2 0.4 0.6 0.8 Appied Strain (%) (a) n-values, IGC157 Sample #1 ---------- ----- ---------------16.0------ ----- ------------- ----- G) C 14.0 --- -12.0 -1-------0-----------------------6 ----10.0 ------- -- -----------8.0 ------- - -----------6.0 - -4.0- ----------------------------- ----------- ------- ---------2.0 0.0 0.8 0. 0 0.6 0.4 0.2 Applied Strain (%) (b) Fig. 4.19. (a) Current data, and (b) n-values for IC 157 Sample #1. a-e-n1 n Loading -w--n2 Loading -x n1 Unloading n2 Unloading 154 Ic, IGC157 Sample #2 140 - 120 - -- - - - ------------------------- -- ----- - -------- ---- - - --80 - - ------------------ -------60 - ---- - - - ---------- - -- - ---------------- -----40 - -- 100 - - ---- -------- 20 -0 - -- --- iaUnloading d-g --- -- --- _e-Loading 0 0.0 0.2 0.4 0.6 0.8 Applied Strain (%) (a) n-values, IGC157 Sample #2 0 20.0 18.0 16.0 14.0 12.0 10.0 8.0 6.0 4.0 2.0 0.0 - -- - - - - - ----- - - - - ---------- - - - --------------- - - ------------------------ ----------- - - - - - - -------- - -- -------------------------- ---- -- --- - -- -- - - --- - --- - -----~~------ -- - -------- ----- ----- ---------- -- - ---------------------------i . 0 .0 0.2 0.4 0.6 0.8 Applied Strain (%) (b) Fig. 4.20. (a) Current data, and (b) n-values for IGC 157 Sample #2. -e-i-a- n1 Loading n2 Loading n1 Unloading _* n2 Unloading 155 Ic, IGC157 Sample #3 ------------------- 140 -------- ------- --- ------ --- --- --------------------- -------- --------------- ---- ------- ---------- -------- ---- 120 ---------100 80 .2 60 40 20 e+Loading 0 0.0 0.4 0.2 0.8 0.6 Applied Strain (%) (a) n-values, IGC157 Sample #3 14.0 -------- 12.0 ------ L--a--d-i-n----- --- ----------- ------------- ------------------------- ------------------------ 10.0 0 0----------Lod 8.0 6.0 o n1 Loading __3-n2 Loading 4.0 2.0 0.0 0.0 0.2 0.6 0.4 0.8 Applied Strain (%) (b) Fig. 4.21. (a) Current data, and (b) n-values for IGC 157 Sample #3. 156 Ic Data, EU153 Sample #1 160 140 - --- --- ----- ---- ------ -- -- -- -- -- ---------- 120 ------ --------- - -- ---- --100 ----------------------------C., - 80 60: 40 - --------- - - -------------------- 20 - ------ ---------- --- ---------------00 0.2 0.4 0.6 0.8 0 Quench -*- Loading -*- Unloading Applied Strain (%) (a) C) 12.0 - 10.0 - n-values, EU153 Sample #1 -- ---- --- -- - - --- ----- 8.0 - ------ ------------------------6.0 e.-n1 Unloading ia n2 Unloading 4.02.00.00 0.2 0.4 0.6 0.8 Applied Strain (%) (b) Fig. 4.22. (a) Current data, and (b) n-values for EU 153 Sample #1. 157 Ic Data, EU153 Sample #2 160 - ----140 - - - - ----- ------- -------- ------ - - - ---- ---- - - - - -- -- 120 --- - -- ------- -- ---- -- - -100 ----------- ---- ----- ---- -----80 - ------------------------------- ---60 - - - -------- --- - --------- -- 40 - Quench -s- Loading -&- Unloading -- ----- -- ------- - --- ----------- -- 20 - 0 0.2 0 0.6 0.4 0.8 Applied Strain (%) (a) n-values, EU153 Sample #2 12.0 - --- - 10.0- ---- ---- ------ - ------------ --- ----------- --- ---------- ~~- ----------------------- 8.0- -- ------ 'E 6.0 ------------------------------------- - - 4.0 --.- - - - --- - - -- - - 2.0 ------ -- --------- ----------------|0.00 0.2 0.4 0.6 -o-nl Loading 0.8 Applied Strain (%) (b) Fig. 4.23. (a) Current data, and (b) n-values for EU 153 Sample #2. n2 Loading -- n1 Unloading -x -n2 Unloading 158 1c, EU153 Sample #3 U ----- - -- 160 - -- - - -- -- - -- - -- --------- - - --140 120 - --------- - -- -- - - -- -- - - 100 -~~~~-------------- --- - 80 ------ -- ---- --- -- -- 60 - - - ---- - -- --------------40 20 - Quench -- i -- Loading Unloading 00 0.6 0.4 0.2 0.8 Applied Strain (%) (a) n-values, EU153 Sample #3 .a) 12.0 - 10.0 - 8.0 - ------ ----- - -------------- -- --- - - -- -------- - - - -- -- ----- --- --- -- ---------- ------- 6.0 - -- - - - - - - - 4.0 - - - - - -- --- 2.00.00 0.2 0.4 0.6 0.8 Applied Strain (%) (b) Fig. 4.24. (a) Current data, and (b) n-values for EU 153 Sample #3. -4-n1 Loading -s-- n2 Loading -- n1 Unloading --- n2 Unloading 159 The critical current plots for the first two IGC 157 samples show that the unloading traces closely follow the loading traces. The largest discrepancy is a 23% current reduction that was measured in Sample #2 at an applied bending strain of 0.4%, but a majority of the points are within 10% of each other showing good reversibility. The n-values in IGC 157 Sample #1 generally remain similar between strain loading and unloading. A drop of approximately 50% occurs when the sample was returned to a strain level of 0.1%. The voltage-current measurement for this point had a high amount of noise and it is probable that the data was somewhat offset. The n-values for IGC 157 Sample #2 show a more consistent degradation on the unloading path. And the correlation between the two different ni and n2 values calculated is very good. The quench current levels for the EU 153 samples at the lower applied strain seem to connect well with the loading critical current data. The general shape of these curves is similar to the IGC 157 loading plots. Unloading data of the EU 153 samples show a significant degradation in the critical current levels. The largest discrepancy for the samples was a 56% reduction measured in Sample #1 at a bending strain of 0.4%. The n-values for the EU 153 samples confirm the performance degradation in the strand. Although the data was not available for loading the strand at the lower strain levels, it seems that the n-values are initially high and significantly drop by an applied strain of 0.7%. The lowest nvalue generally holds for all strain levels as the sample is unloaded back to a zero strain. One of the most interesting aspects of the plots is the rise-drop-rise in the critical current for both the IGC157 and EU153 samples. The drop point is generally at an applied strain of 0.3% for the IGC157 samples and 0.2% for the EU153 samples. This critical current drop behavior occurs in the IGCi 57 samples for both loading and unloading. But it is not observed on the unloading path of the EUl 53 samples because of the severe critical current reduction. 160 It is apparent from both the Ic and n-value plots that the EUI 53 samples suffered more irreversible degradation than the IC157 samples. 4.9 Bending Results The quality of the bending distribution created by the bending mechanism is just as significant as the critical current measurements. This is because the test was intended to characterize the pure bending strain behavior of the samples. If the mechanism does not load the samples in a uniform distribution of bending strain, then the intended characterization is not valid. Strain gage data was collected by the data acquisition system during all of the test runs. This recorded strain data for the bending distribution in the beam both with and without the Lorentz force. Thus, allowing the effect of the Lorentz force to be plotted. On the first day of testing with the IGC153 samples, the strain gages were connected in a singlebridge circuit. This was done to try and collect strain data on both the compression and tension sides of the Support Beam as the bending load was applied. This data could then be used to determine the dynamic location of the neutral axis relative to the center of the test sample. Unfortunately, the measurements of the strain values drifted significantly. Each of the measurements drifted the same amount, and it did not matter whether the corresponding gage was mounted on the tension side or compression side of the Support Beam. It appeared as though the Support Beam was expanding or contracting with temperature changes. The measurement drift would go in one direction for a period of time and then suddenly reverse and begin drifting in the other direction. 161 It was soon realized that the drift was being caused by the rise and fall of the liquid helium level in the cryostat. The resistance of the instrumentation wires connected to the strain gages would lower as the liquid helium level increased and rise as the helium level went down. The measurement circuit showed this resistance fluctuation as being a change in strain. The solution was to connect the strain gages in a double-bridge configuration where this effect was canceled out. However, this eliminated the possibility of collecting data related to the position of the neutral axis. The double-bridge measurement circuit used strain gages mounted on opposite sides of the Support Beam with one on the tension side and the other on the compression side. The relationship for calculating the amount of strain from a double-bridge compensating Wheatstone strain gage circuit is given by equation 4.7 [4.2]. In this equation c is the measured strain and GF is the gage factor of the strain gages at the measurement temperature, which is equal to 2.12 at 4.2K for the gages used. The term VE is the excitation voltage of the Wheatstone bridge and 6V is the measurement voltage. For a double-bridge circuit in a temperature-compensating configuration, the bridge constant, K, is equal to 2. 9V VE 1CeGF(47= K -- (4.7) 4 Using equation 4.7 to solve for the measured strain, F, gives the average strain at the beam surfaces. This value must be divided by 2.038 to get the relevant strain in the strand, according to the strain relationship between the beam and the strand given by equation 4.5. Strain measurements were made for both the IGC157 and EU153 sample test runs. Recall from section 4.1 that the IGC157 configuration was based on a bending ratio off-1.57 which the analysis in section 2.5 showed would create more bending error than thef=1.53 ratio used in the EUJ 53 setup. This was verified by the collected data presented in figures 4.25 through 4.27. 162 The strain data did not change significantly between the different samples in the same Sample Assembly. The figures are measurements based on Samples #2 from IGC157 and EU153. IGC157, Measured Bending Strain --------- ---- -- --- ---0.007 ------- -------0.006- -- -- ----------0.005- - --- ------- - ----- --- --------- ------------0.004 ---------------------------------0.003 -------------- ----------------------------------0.002 - - - -------- ------ - - -0.001 - -- - ---- - -------0. 000 1 --- --- - --- S C 'a. -0. 001j I 0 0.006 0.002 0.004 Applied Bending Strain (in/in) -e--Center -Pos End -aNeg End 0.008 (a) EU153, Measured Bending Strain C C C U) 0 (U (U 0 0.007 - -------------------------------- -------- 0.006- --- ---- - - - -------------0.005 0.004 ------------------ - ----------0.003 ------------- - ------------- - 0.002 ---------- - --------------------0.001 - --- - ---------- ------- ---- 0. 000 1 -- ----------------------------- -e-Center -*-Pos End -*-Neg End -0.001 0 0.002 0.004 0.006 0.008 Applied Bending Strain (in/in) (b) Fig. 4.25. Measured bending strain for (a) IGC157, and (b) EU153 beams. 163 Figure 4.25 shows a plot of the measured bending strain as a function of the applied bending strain for the IGC 157 and EU153 Support Beams. The line labeled "Center" is the strain measurement for the gages mounted in the center of the Support Beam. The "Pos End" and "Neg End" traces are for the strain gages mounted near the positive end of the Support Beam where the power supply current was applied at the Current Joints and the negative end which was the electrical ground. For the IGC157 Support Beam, the end gages were placed 1.81 inches (46mm) inches from the beam center. The EUl53 Support Beam had end gages positioned 1.75 inches (44mm) from the beam center. Incidentally, these end gages are positioned inside the length region measured by the voltage taps. The lines show the data for incrementally increasing the applied bending strain up to 0.7% (0.007 in/in) and then unloading. Ideally, the strain plots should trace the same path on loading and unloading. Looking at the center strain gage plots for both IGC157 and EU153, it is clear that center gages did not produce the same output on the unloading path. This is because the center gage on the tension side of IGC 157 delaminated at a loading strain of 0.6% (0.006 in/in) and the same gage on EU153 came loose just before reaching an applied bending load of 0.7% (0.007 in/in). This is understandable since the strain at the surface of the beams was approximately 1.2% and the strain gages were limited to 1.0%. Fortunately, the gages simply delaminated from the surface and did not break. This meant that they were still part of the double-bridge circuit and data could continue to be collected. However, there was a shift in the strain measurement because the bridge had been balanced with the gage attached to the titanium Support Beam. When the gage delaminated, the strain caused by the difference in the thermal coefficient of expansion of the gage and the beam was released and caused a shift in the measured data. This shift is shown in the data traces for both the IGC157 and EU153 center gage plots. In addition, the tension-side strain gage on the positive end of EU153 broke loose causing an open circuit. This data discontinues at a strain of 0.5%. 164 The figures show that both IGC 157 and EUI 53 have a very good bending distribution. The end gages exactly trace the same path on loading and unloading, showing that there was no plastic deformation. If the center gages had not broken loose, the measured center strains for both IGC157 and EU153 would have been slightly greater at an applied strain of 0.7% (0.007 in/in). IGC157, Bending Strain Error 0.0002 0.00001 0 tw C -0.0002 -0.0004-0.0006-0.0008-0.0010-0.0012 -0.0014- -------------- --- --- ------- -- ----- - - ---- --------- --- -- - -- ------ - --------- ----------------------------- --- --------------------- ------------------------- ---------------- --- - ----- - -- ----- ------- - 0.002 0.004 0.006 -.-- Center -g-Pos End -&-Neg End 0.008 Applied Bending Strain (inlin) (a) EU153, Bending Strain Error I- 0 I- C U, 0.0002 0.0000 -0.0002 -0.0004 -0.0006 -0.0008 -0.0010 -0.0012 -0.0014 - ---- -- ------ ---- -- -- -- - ---- --- --------- - - -- --- - -- -------- --- ---- ---- ------ -- -------- --- -------------- ----------- ---- ----------- -- ----- 0 0.002 0.004 0.006 0.008 Applied Bending Strain (in/in) (b) Fig. 4.26. Bending strain error for (a) IGC157, and (b) EU153 beams. + Center -*- Pos End ,- Neg End 165 The magnitude of the errors of the measured bending strain relative to ideal pure bending are shown in figure 4.26. These plots trace the amount of strain either below or above the intended strain setting. For example, the strain error shown in figure 4.26a is approximately -0.0013 on the positive end of the IGC157 beam at an applied strain of 0.007 in/in. This means that the measured strain was 0.0013 below the intended strain of 0.007, or 0.0057 in/in. This is a drop of 18.5% below the ideal value. The plots for the center gages again show the obvious shift near an applied strain of 0.6% (0.006 in/in) where the gages delaminated. Otherwise, these traces would have returned back along the same loading path, similar to the end gages. Up to the point of the gage delaminating, the bending strain error plot for the center gage of EUl 53 confirms that this configuration has the lowest bending error. It is almost perfect up to an intended ideal strain of 0.6% (0.006 in/in). On the other hand, the IGC157 plot for the center gage shows the increased divergence with continued applied strain. This was expected from the bending mechanism error analysis. The configurations for the IGC157 and EU153 Support Beams are not very different. The separation distance for the pivot axes of these beams is the same at 2.9757 inches (75.583mm), but the ratiof=1.57 has a sample length of 4.67185 inches and the ratiof=1.53 has a 4.55282 long sample. This is only a difference in length of 0.119 inches (3mm). It is interesting that the strain error levels on the end gages are almost identical for both IGC 157 and EU153. It was known that the positive and negative end gages should trace the same path due to their symmetric placement about the beam centerline, but it was not clear how the two different configurations would compare in the end regions. These traces are approximately linear and maintain an error near 19% below the intended ideal strain over the entire operating range. 166 IGC157, Strain Change from Lorentz Load --- - - - -- - -- -0.00020 ---- -) 0.00015 0.00010 0.00005 0.00000 -0.00005 -0.00010 -0.00015 -0.00020 -- - --- ------ -- ------ - ---- -- - - -------- ----------- ------- - ------ -----------0 0.002 0.004 0.006 -o- Center -m- Pos End --- Neg End 0.008 Applied Bending Strain (in/in) (a) 0.00020 0.00015 0.00010 0.00005 0.00000 -0.00005 -) C -0.00010 -0.00015 -0.00020 EU153, Strain Change from Lorentz Load ------- - -- ----- - ------- - --- --- - - - - - - -- --- --- -C----------t--rS0---------------------------E _-oCenter ---------------- ---a ------ ---* -Pos End -- -- - ----- -------------------* Neg End - - - - - -- - -- ---- -- --- ------ - -- - -- - -0 0.002 0.004 0.006 0.008 Applied Bending Strain (in/in) (b) Fig. 4.27. Effect of Lorentz load on bending strain for (a) IGC157, and (b) EU153 beams. 167 The effect of the Lorentz load on the bending distribution is shown in figure 4.27. These plots demonstrate the amount of change in the measured bending strain caused by the Lorentz force at the maximum current in the test sample. These traces do not show the deviation from ideal bending; rather they are the effect on the measured strain. The plots were generated by subtracting the measured beam strain with no Lorentz force from the measured beam strain at full sample current and maximum Lorentz load. The effect of the Lorentz force on the bending distribution in the beam becomes less significant as the applied bending state increases. This is because the contribution of the Lorentz force becomes a smaller portion of the total bending strain in the beam. At high bending states the large majority of the strain comes from the bending mechanism. But at low strain states, the bending mechanism is applying little or no load and so the Lorentz load is the dominant force. At this state only the bending stiffhess of the Support Beam is left to resist the distributed force. The error plots for the center gages show that the Lorentz force tends to lower the strain in the center of the beam. This was expected since the Support Beams were bent so that the test samples were on the outer curved surface of the beam. The Lorentz force was then directed inwards to hold the samples in the groove. This tended to flatten out the beam and lower the strain in the middle. But because the ends are fixed, the strain near the ends was increased with this flattening effect, as verified by the end gage plots. 4.10 Sample Strain The collected strain data shows that the bending mechanism produced a very good bending strain distribution in both the IGC 157 and EU153 Support Beams. However, this does not mean that the samples themselves were in a state of uniform bending. 168 After testing, the sample Support Assembly was removed from the probe and the samples were examined. The samples appeared to have been placed in tension during the testing because they were outside of their mounting grooves. Figure 4.28 shows the Support Assembly for EU153 before and after testing. Even though some of the samples were loose in the grooves before testing, all of the samples had been plastically deformed during testing. Samples (a) (b) Fig. 4.28. EUl 53 test samples (a) before testing, and (b) after testing. 169 Some plastic deformation was expected because of the high strain level of the bending mechanism and the low elastic limit of the copper portion of the superconducting strand. Several measurements were taken of the samples shown in figure 4.28 to try and estimate the amount of deformation. Assuming that the samples had initially been in the groove and were bent into an arc, the average measurement corresponded to an elongation of approximately 0.005 inches (0.001mm) or 0.1% strain. This is the value for the plastic deformation rather than the applied strain. To achieve this amount of deformation, the strand had to experience strain beyond its elastic limit. This value is an upper bound on the plastic deformation because each of the strands did not start out settled in the grooves, as the picture in 4.28a confirms. Aside from the bending strain applied by the mechanism, there are two sources that would have placed the sample in tension. The first source is the difference in the thermal coefficient of expansion between the Nb3Sn strand and the titanium alloy Support Beam. The second source of tension could have come from the offset between the center of the strand and the center of the beam as described in section 4.2. These two effects will be estimated to determine how much influence they might have had on the strand bending. The thermal expansion of the strand, as a single unit, from room temperature to 4.2K is -0.27%, and -0.15% for the Ti6Al4V Support Beam. Since both of these components start out with the same length, the tensile strain in the strand from thermal contraction is 0.12% which is rather significant compared to the applied bending strain levels. Note that this strain level is for the strand as a whole and not for the intrinsic strain of the Nb 3Sn filaments. The effect of the strand offset relative to the centerline of the Support Beam will be estimated with an upper bound argument. Referring to section 4.2, the centerline of the strand was offset from the centerline of the Support Beam by 0.012 inches (0.3mm). To compensate for this offset, the beam was machined so that the geometric neutral axis would be coincident with the strand centerline. The Support Beam and strand were then assembled and placed in the bending mechanism. 170 The Support Beam was accurately positioned in the bending mechanism so that its centerline was coincident with the pivot axes of the Torque Arms. It is likely that under bending operation of the mechanism the rotation of the Torque Arms forced the neutral axis of the Support Beam to dynamically shift to the centerline of the beam. Consequently, the neutral axis was no longer coincident with the strand centerline. Assuming that the neutral axis was shifted to this new position in the Support Beam, an estimate can be made about the strain state of the strand when a bending load is applied. The development will follow the procedures and definitions used in section 4.4. Figure 4.29 is an exaggerated diagram of the beam and strand. The dashed line represents the shifted neutral axis of the beam and the phantom line is the centerline of the strand. Since the beam is in a state of bending it has a radius of curvature, p. The strand is offset from the neutral axis by an amount, 6. Since the neutral axis position of the beam is not elongated during pure bending, it has a constant length which is equal to the initial, undeformed, length of the strand, L. The angle subtended by this arc is a. Strand Centerline.- ~- S P Beam neutral axis Fig. 4.29. Offset between beam neutral axis and strand centerline. 171 At a chosen bending strain state, a, the radius of curvature of the beam can be found from equation 4.1 with the subtended arc, a, being equal to twice the value of equation 4.3. The radius of curvature for the strand is equal to the radius of curvature of the beam and the offset of the strand, as given by equation 4.8. (4.8) P,trand = p +8 The length of the strand after the beam has been placed in a state of pure bending is found by combining equation 4.8 with 4.2, which yields equation 4.9. Lt,,tr = p(0+ p 8x (4.9) Making the substitutions for p and a described above into equation 4.9 produces equation 4.10. This expression gives the new length of the strand, Lstrand, in terms of its original undeformed length, Ls, its diameter, ds, and the intended bending strain level, a. (4.10) =~a =L ± +J Lt The tensile strain in the strand caused by the offset is then given by equation 4.11. ET = (4.11) Ltran L, Substituting 4.10 into 4.11 and simplifying shows that the tensile strain is independent of the original length of the strand as shown by equation 4.12. CT = _ + 2c -. -d, -1 (4.12) 172 Representative values, given in table 4.3, were substituted into equation 4.12 to calculate the amount of tensile strain in the strand caused at different levels of applied bending strain. Table 4.3. Tensile strain in an offset strand with applied bending strain. 5 0.012 (inches) d, (inches) 0.03189 Bending Strain, , 0 0.001 0 0.00075 0.002 0.003 0.004 0.005 0.006 0.007 0.00151 0.00226 0.00301 0.00376 0.00452 0.00527 ST The offset of the strand also causes its bending state to be modified by a small amount. The offset of the strand centerline from the beam neutral axis means that it has a new radius of curvature given by equation 4.8. This radius of curvature can be combined with equation 4.1 to find the bending strain state of the offset strand. It is important to realize that equation 4.1 is true in general and so care must be taken not to confuse the different strains in the definitions being used. The new bending strain in the strand, SB, caused by the offset in the beam neutral axis is given by equation 4.13. 6B = d(4.13) d, + 29c 173 It should be clear from equation 4.13 that when 6 is small the bending strain in the offset strand, -B, is very nearly equal to the bending strain in the ideal strand, F. As proof, table 4.4 was generated using equation 4.13 and the present parameters. Table 4.4. Bending strain in an offset strand. 5 (inches) d, (inches) Bending Strain, aB 6 0 0.012 0.03189 0 0.001 0.00100 0.002 0.003 0.004 0.005 0.006 0.007 0.00200 0.00299 0.00399 0.00498 0.00597 0.00696 The final strain state of the offset strand can be found by combining the tensile strain from the temperature expansion coefficient mismatch, the tensile strain from the offset of the strand, and the corrected bending strain. The bending strain is not really a single strain in the same sense as the tensile strains. Rather, it is a linear distribution of strain through the sample that is tension on one side and compression on the other. The tensile strains must be added to the bending strains keeping this in mind. Figure 4.30 conceptually illustrates how to add these strains together. 174 6B St ET SB-new Fig. 4.30. Conceptual method for adding tensile strains to bending strain. To add tensile strains to a bending strain, the tensile portion of the bending strain is added directly to the other tensile strains to get the new tensile portion. The magnitude of the compression portion of the bending strain is subtracted from the combined additional tensile strains. If the magnitude of the compressive term is larger than the other tensile strains, then the new bending strain will have a reduced compression portion. But if the other tensile terms combine to be larger than the magnitude of the original bending compression, then the new strain is in tension and the local neutral axis has moved off of the strand. The strain state of the offset strand was calculated using the procedure outlined above and is given in table 4.5. A temperature-induced tensile strain of 0.0012 (0.12%) was combined with the offset tensile strains in table 4.3 and the refined bending states of table 4.4. Because the bending distribution is no longer uniform through the strand, it has been given in terms of the tensile strain on the first surface, &1, and the corresponding compressive strain on the opposite surface, 82. 175 Table 4.5. Strain distribution in offset strand. 8 (inches) ds (inches) t (in/in) 0.012 0.03189 0.0012 Bending Strain, c s1 0 0.00120 0.00120 0.001 0.002 0.003 0.004 0.005 0.006 0.007 0.00295 0.00471 0.00645 0.00820 0.00994 0.01169 0.01343 0.00095 0.00071 0.00047 0.00022 -0.00002 -0.00025 -0.00049 62 The strains in table 4.5 show that the ideal offset sample is mostly in a state of tension. Only at the larger applied bending strains does the strand have a surface with compression. The calculations were based on an idealized situation where the neutral axis of the Support Beam moved as far away from the centerline of the strand as was allowed. In reality, the neutral axis will not move this far and so the bending distribution in the actual strand will be better. However, the significant amount of tensile strain from the temperature expansion coefficient mismatch will remain. It was known before performing the bending tests at the National High Magnetic Field Laboratory that the thermal mismatch would place the strand in tension. This is why the samples were purposely mounted loose in the Support Beam in an attempt to ameliorate the tensile effect, as verified by figure 4.28a. Although the strain analysis shows the possibility of a large tensile strain on the samples, it does not explain why the critical current measurements were lower than expected when no bending load was applied to the samples. 176 4.11 Conclusion In conclusion, a bending mechanism has been designed, constructed, and used to measure the critical current of Nb 3Sn superconducting strand. The mechanism loaded several titanium alloy beams holding superconducting samples over a range of large-displacement bending motion from an initial undeformed state to a maximum bending state of 0.7% strain. The loading occurred in a 4.2K liquid helium bath and a magnetic field of 12T. The measured data showed that the mechanism produced a bending distribution along the loaded beam that remained within 20% of the intended strain level for all of the strain states. The critical currents of two different types of internal tin Nb 3Sn superconducting strand samples manufactured by Intermagnetics General Corporation (IGC) and Oxford Superconductor Technologies (OST) were measured using the bending mechanism. The test results showed that the critical currents and the n-values of the samples decreased with increased applied strain. After testing, the samples appeared to have been plastically deformed by excessive tensile strain. An analysis showed that the offset of the strand from the centerline of the support beam could have caused the tensile strain. This offset did not significantly change the applied bending, but it could have superimposed a large tensile strain that would have contributed to the degradation of the samples. In addition to the offset, a temperature expansion coefficient mismatch between the test samples and the titanium alloy support beam added to the tensile strain. It is hoped that future efforts will be able to improve on the work that was undertaken to develop a new method for characterizing the bending strain behavior of Nb 3Sn superconducting strand. This has been the case with uniaxial testing which has benefited from 25 years of refinement. 177 4.12 Recommendations There are several recommendations that can be given for any future efforts in performing bending-strain behavior characterization tests on Nb 3Sn: The bending mechanism was designed to test the longest possible sample in the chosen magnet bore. This decision limited the strength of the mechanism and, consequently, the thickness of the support beam that could be used to hold the Nb 3Sn test samples. This beam thickness meant that the samples were not positioned with their centerlines coincident with the centerline of the support beam. This might have caused a significant tension in the strand at the higher applied bending levels. If a large-displacement variable-strain bending mechanism were going to be used to perform bending-strain behavior tests it would ideally be of a stronger design. This would allow a thicker support beam to be used where the strand could be positioned directly on the beam centerline. A stronger mechanism made out of the same material would mean that the test sample length would be shorter. It would be of the same fundamental configuration as the present mechanism, but use stronger single-enveloping wormgears rather than the helical gears. However, it is important to remember that a thicker beam would be limited by its elastic strain limit. The existing bending mechanism could still be used for characterization tests. The mechanism is capable of bending a thicker beam than the conservative thickness which was used in the critical current tests. The selected titanium alloy support beam was chosen to be as thin as practical so that there would be no risk of damaging the mechanism before the initial tests had been completed with the unproven device. And the grooves in the beam were machined to a shallow depth so that there would be little risk with the beam failing. If subsequent tests were done, a beam of the same thickness could be machined with deeper grooves so that the strand would be positioned at the centerline of the beam. However, as 178 discussed earlier, this might result in high stress concentrations near the grooves and result in beam failure. An alternative would be to purchase thicker beam material and then have it ground to a specified thickness before machining the strand support grooves. Because of strength limitations, this thickness should be no more than 0.079 inches (2mm) for a titanium alloy beam used in the present bending mechanism and loaded to a maximum strain state of 0.7%. If a thicker support beam were used, the maximum testing strain state should be lowered. Otherwise, the beam would plastically yield at the surface and significantly affect the bending distribution. The chosen beam thickness used in the critical current tests was approximately twice the thickness of the sample diameter. This meant that at a sample bending strain of 0.7%, the strain in the beam was double, or 1.4%, which is the elastic limit for Ti6A14V titanium alloy at 4.2K. The present design has difficulty supporting the samples at the lower strain levels. Ideally, the samples would be enclosed on all sides, but this would limit access for the voltage taps. Perhaps a Support Beam could be gun drilled with tunnels for the samples. Holes would then be machined to attach the voltage taps. This sample mounting configuration would require straight samples and would limit the length of the current joints in the present bending mechanism. None of the sample measurements had a resistive component. The voltage-current plots were flat until the sample either transitioned or quenched. This indicates that the current had satisfactorily redistributed in the sample before the voltage taps. The loose mounting of the samples possibly contributed to the lower than expected critical current measurements for the conditions of zero applied bending strain. But it is not clear what the primary cause of the initial degradation was because it continued even at the higher and better-supported bending states. The degradation may have somehow been caused by the heat treatment fixture affecting the temperature distribution in the strand during the heat treatment, or it might have been the result of handling damage during soldering. Handling damage is unlikely 179 because similar degradation occurred for all of the samples, not just a few. Whatever the cause, it had to be common to both the IGC and OST samples. The bending mechanism was designed to be as universal as possible. This means that a new sample support system could be designed and used with the same mechanism. The only important thing to remember is to have the flexible portion be the same length as specified in section 4.1 and have it centered on the pivot axes. There was a problem with the bearing surface on the Input Shaft worm, which can be seen in figure 4.31. The design dictated that the worm threads should be machined over a limited distance, leaving extra material for the bearing thrust surfaces. Unfortunately, the gear machinist did not follow the drawing and machined the worm thread along the entire length, which significantly reduced the thrust face of the bearing surface. The thrust face should have been the entire larger diameter shown in the figure rather than the smaller machined diameter. This weakness was the primary concern for failure when the mechanism was operated. Reduced Bearing Thrust Surface Larger Diameter of Intended Thrust Surface Fig. 4.31. Bearing surface of bending mechanism Input Shaft. 180 Appendix A - Bending Error Estimates Displacement Error Effect It was shown in section 2.4 that the bending mechanism produces a displacement error at the ends of the beam when compared to the ideal case. The effect of this error on the bending distribution can be estimated using several methods such as a finite element model, solving the governing differential equations, or approximating with a small-displacement analysis. Each of these procedures is complicated and either requires a considerable amount of time or does not produce accurate results. An alternative and more tractable procedure can be used for estimating the magnitude of the effect of the displacement error in the bending mechanism on the bending strain distribution. It estimates the bending strain at the center of the beam by comparing the ideal displacement to the actual mechanism displacement. The procedure follows: The ideal displacement at the ends of the beam as a function of rotation angle, 0, and sample length, Ls, was given by equation 2.34 and is restated as A.1. The displacement caused by the bending mechanism is expressed in equation A.2 after combining equations 2.35 and 2.37 and expressing L,/L, in terms off The displacement error is the difference between the mechanism displacement and the ideal bending displacement as shown by equation A.3. = L 1 sin ] 0 2 _ U - Umech - 1 -- LS 2 (1 I f)( ~ (A.1) f - cos 0) (A.2) 182 U ero = Umech - (A.3) ideal The ends of the beam must be moved in order to change from one bending state to another. The amount of this movement is expressed in terms of the rotation angle for the ideal situation and the bending mechanism in equations A.4 and A.5. The overall displacement error that results from changing between the two bending states is given by equation A.6. Auideal =ideal (02 ideal (01 (A.4) Auuech =cmech(2)Umech (1) (A.5) Auerror = Aumech (A.6) ideal When changing from one bending state to another, the significance of the displacement error at the center of the beam can be determined using equation A. 7. This equation compares the displacement error at the center of the beam to the amount of ideal displacement required to move between the two strain states. For example, if a beam were displaced to a bending strain of 0.004 in/in from an initial bending state of zero and equation A. 7 gave a value of 0.1 then the largest effect that the displacement error could have is to increase the bending strain at the center of the beam by (0.1)*(0.004in/in) or 0.0004 in/in. This would result in a maximum bending strain at the center of the beam of 0.0044 in/in. If equation A.7 gave a negative value then the bending strain would be reduced. Error Multiplier = Auerror (A.7) Auideal The use of equation A. 7 in estimating the bending strain error assumes a linear relationship between the displacement and the bending state of the beam, which is not correct. Since the bending state of the beam is directly proportional to the applied rotation angle, the form of the 183 actual relationship between the displacement and the bending state is shown in figure 2.6. The trace in this figure could be reasonably approximated with a straight line, which means that equation A. 7 actually provides a fair estimate. The connection between the rotation angle and the bending strain state of the beam was originally given by equation 4.1 and has been rearranged to yield equation A. 8. 0 =LI d, (A.8) By substituting equation A. 8 into A. 7, estimates can be made about the bending errors in the center of the beam at various strain levels. Table A. 1 lists the estimates of the actual bending strain at the center of the beam produced by the mechanism according to equation A.7. The estimates were calculated for a beam length of 4.672 inches (118.7mm) and a bending ratio of f=1.57. The strand diameter for setting the bending strain state was 0.032 (0.81mm). These values were chosen because they correspond to one of the actual beams that were tested in the bending mechanism. The first column of table A. 1 represents the bending strain for the ideal case. The second column is the result of applying equations A. 7 and A. 8 to the bending strain in column one. Equation A.7 uses equations A.4 and A.5 to determine the changes in the displacements. These equations need two strain states; a zero bending strain (0 = 0) was used for the initial strain state and the bending strain listed in column one was used for the second strain state. The strain error in the third column is the product of the values in columns one and two. And the last column is the estimate for the bending strain in the center of the beam which is calculated by adding the first and third columns. 184 Table A. 1. Estimate of actual bending strain at center of beam. f 1.57 Ls 4.67185 0.03189 ds Ideal Bending Displacement Strain Bending Strain, s Error Error Strain (in/in) 0 0.001 0.002 0.003 0.004 0.005 0.006 0.007 Fraction 0 0.08839 0.08605 0.08216 0.07669 0.06967 0.06107 0.05090 (in/in) 0 0.00009 0.00017 0.00025 0.00031 0.00035 0.00037 0.00036 Estimate 0 0.00109 0.00217 0.00325 0.00431 0.00535 0.00637 0.00736 The bending estimates can be compared with the measured data for the IGC 157 sample in section 4.9. The results presented in figure 4.25a for the strain at the center of the beam are very close to the estimates up to a bending strain of 0.005 in/in, when one of the strain gages delaminated. At an ideal strain of 0.005 in/in, the measured strain was 0.00519 which compares well with the estimate of 0.00535 given in table A.1. The derivation of equation A.7 ignores the nonlinear relationship between the bending displacement and the strain level. A more accurate estimate can be found which accounts for the nonlinearities using a differential approach to the change in displacement. In this procedure, the derivatives given by equations A.9 through A. 11 replace equations A.4 through A.6 and equation A.7 becomes A.12. Equation A.8 remains the same. Table A.2 reflects the updated calculations. 185 L sin0 2 s 02 dui_I dO dumc I ._ dO L s I- 2 cos 0 (A.9) 0 I - sinO f due,,or dumech duid"al dO dO dO (A.10) (A.11) Error Multiplier = duerrorldO (A.12) du ,,dO Tmidealro Table A.2. Derivative estimate of actual bending strain at center of beam. f Ls ds 1.57 4.67185 0.03189 Ideal Bending Strain, , (in/in) Displacement Error Fraction Strain Error (in/in) Bending Strain Estimate 0 0.001 0.002 0.003 0.004 0.005 0.006 0.007 0 0.08761 0.08292 0.07507 0.06399 0.04960 0.03179 0.01040 0 0.00009 0.00017 0.00023 0.00026 0.00025 0.00019 0.00007 0 0.00109 0.00217 0.00323 0.00426 0.00525 0.00619 0.00707 The bending estimates in table A.2 are even closer to the measured values than table A. 1. For a measured strain of 0.00519, the new estimate is 0.00525 in/in. 186 Effect of Lorentz Force The effect of the Lorentz force on the bending strain of the beam can be estimated using smalldisplacement beam theory as follows: For the critical current measurements, the beam is first bent by the mechanism to the desired bending strain state. Current is then applied to the samples and the critical current is measured. This applied current in the magnetic field creates a distributed Lorentz load on the beam. Because the test sample follows the curvature of the support beam, the Lorentz load is perpendicular to the beam for all strain states. The Lorentz load on the beam causes the strain state to diverge from the intended setting. The direction of the current in the sample tests was chosen so that the Lorentz load would tend to flatten out the center of the support beam, reducing the center strain. But because the ends of the beam were prevented from moving by the beam clamps, the outer portions of the beam increased in bending strain. The magnitude of the strain changes can be approximated by assuming that the beam is straight and fixed at the ends with a distributed load as shown in figure A. 1 a. Thus, standard beam formulas apply. The internal moment distribution of the beam shown in figure A. lb is given by equation A. 13 [A. 1]. The distributed load, w, is evenly applied over the entire beam length, 1. The straight beam configuration serves as a good approximation because, even though the beam is bent into a curvature, the Lorentz load always remains perpendicular to the beam. The cumulative strain state of the beam is estimated by simply superimposing the strain caused by the Lorentz load onto the bending strain set by the mechanism. Equation 3.6 gives the relationship between the internal moment in the beam and the bending strain state of the strand. It has been restated as equation A.14. The variables E, b, and h are, respectively, the elastic modulus, height, and thickness of the support beam. 187 'II 1 I 4~L4~444kI1] M + Fig. A. 1. (a) Beam with uniform load and fixed supports, and (b) moment distribution. M = ' 12 (6lx-6x2 _12) M = 1 Ebh' (A.13) (A.14) 6 d, Equations A. 13 and A. 14 can be combined to express the bending strain (in terms of the strand strain) that is caused by the Lorentz force, yielding equation A. 15. strand = wd 3 (6lx -6x2 _/2) 2Ebh (A.15) 188 The estimate of the Lorentz force effect on the bending distribution can be compared with the measured data, using the information collected for beam EU153. This beam was 4.553 inches (115.6mm) long, 2 inches (50.8mm) high, and 0.065 inches (1.65 mm) thick. At 4.2K it had an elastic modulus of approximately 18.9 Mpsi (130 GPa). The test strand had a diameter of 0.03189 inches (0.81mm). At an applied bending strain of 0.001 in/in (0.1%) the maximum current in the test sample was 138 A. In a background magnetic field of 13T this created a distributed Lorentz load of 1794 N/m (10.244 lb/in). Using equation A. 15 at the center of the beam (x = 1/2), the calculated bending strain caused by the Lorentz load is estimated at -0.000326 in/in. This is more than double the actual measurement value of -0.000144 in/in. For an applied bending strain state of 0.7%, the distributed Lorentz load was 1105 N/m (6.31 lb/ft). This corresponds to an estimated strain change of 0.000201 in/in. The actual strain change was 0.00003 in/in. The straight beam model is more accurate at the lower applied strain levels, because the beam has less curvature and is closer to the model conditions. The simple beam model is able to estimate the Lorentz effect at the lower bending strain levels within an order of magnitude. This estimate is accurate enough to show that the Lorentz load would have a minor effect on the bending distribution in the beam. It was known before testing that the effect of the Lorentz load would be most significant at the lower bending strain levels. The first reason is because the current limit of the samples was expected to be higher at the lower bending strains. The second reason is because the curvature of the beam at the higher bending strain levels gives it more support against the distributed load; much of the force goes into shear rather than bending. The Lorentz effect is more important at the lower applied bending strains because it is a larger fraction of the total strain. A change of -0.0003 in/in at 0.1% strain is more significant than that same change at 0.7% strain. Appendix B - Gear and Spline Calculations The gears and splines used in the bending mechanism were designed using the equations included in this appendix (see references B. 1, B.2, B.3 and B.4). Helical gears were used for the wormgears so that the center distances could be optimized and built with readily available tooling. Gear Calculations To select a gear combination the designer chooses the first five parameters listed below and then the remaining dimensions are calculated using the following equations. This process is iterated until a gear combination is found which satisfies all of the space and strength requirements. Normal Diametral Pitch: Pn Tooth Pressure Angle: Lead Angle of Worm: Number of Worm starts: Teeth in wormgear: A n Ng Common Dimensions (these dimensions are the same for both the worm and the wormgear) Transverse Circular Pitch: Pt Addendum: a- Whole Depth of Tooth: ht = P, cos(A) 1 P. -2.200 +0.002 P, Working Depth of Tooth: hk = 2a Tooth Clearance: C Tooth thickness at Pitch Circle: t2 Worm Dimensions ht - 2Pn hk 190 Lead of Worm: L = p,n Pitch Diameter: d =( Outside Diameter: do =:d+2a Root Diameter (minor diameter): di = do - 2h, L 7r tan(A) Helical Wormgear Dimensions Helix Angle: Pitch Diameter: D= N g Pn cos(i/) Outside Diameter: Do =D+2a Root Diameter (minor diameter): Di =Do - 2h, Gear Set Dimensions (the set includes the worm and wormgear) Center Distance between worm and wormgear: C= Minimum Face Width for Wormgear: FG =1.125 (d + 2c) 2 -(do - 4a)2 Minimum Face Width for Worm: Fw = VD2 - D 2 2 (D + d) 191 Gear Strength The strength of the gear teeth were estimated using the modified Lewis bending equation [B.2]. This equation is intended for spur gears and so it provides a conservative design when applied to helical and worm gearing. Failure by bending will occur when the significant stress equals or exceeds either the yield strength or bending endurance strength. K W' FY Bending stress in gear tooth: where Transverse Load on tooth: W Gear Face Width: F Lewis Form Factor: Y (Derived from tooth geometry; usually looked up in a table) 1 Velocity Factor: 50+ 50 (V is the pitch-line velocity in ft/min) Table B. 1. Gear parameters for bending mechanism wormgears and worms. Wormgear Worm P, 0 X n Nm Torque Gear Drive Shaft 16 200 50 1 36 Drive Shaft Input Shaft 24 200 30 1 27 192 Involute Spline Calculations [B. 1] Basic Dimensions (ANSI B92.1-1970, R1993) To select a spline configuration the designer chooses the first three parameters listed below and then the remaining dimensions are calculated using the following equations. This process is iterated until a spline size is found which satisfies all of the space and strength requirements. Flat Root Side Fit Number of Splines: Pressure Angle: Diametral Pitch: N P N Pitch Diameter: D Base Diameter: D, = D cos($) Circular Pitch: p=- P P Minimum Effective Space Width: S = 2P D N +1.35 Major Diameter, Internal Spline: P N+1 Major Diameter, External Spline: P Minor Diameter, Internal Spline: Di Minor Diameter, External Spline: Dre Form Clearance (radial): CF N-1 P N -1.35 P 193 Form Diameter, Internal: Form Diameter, External: DFi = DFe = N±+12 + P N-I - F 2cF Circular Tooth Thickness, Maximum Effective\Actual: c, Max (table look-up) Circular Tooth Thickness, Minimum Actual\Effective: c, Min (table look-up) Table B.2. Spline parameters for bending mechanism components. External Spline Internal Spline Tolerance Class N # P Torque Gear Input Shaft Torque Arm Coupler 5 5 12 8 300 300 20/40 24/48 194 Appendix C - Drawings Bending Mechanism Fig. C. 1. Bending mechanism model. 196 12 11 16; 17 9 10 7; 2 Bending Mechanism Parts List 1. Bottom Plate 2. Top Plate 3. Torque Gear A 4. Torque Gear B 5. Drive Shaft 6. Input Shaft 7. Torque Arm 153 8. Torque Arm 157 9. Beam Clamp A 10. Beam Clamp B 11. Beam Clamp C 12. Beam Clamp D 13. Thrust Bearing 14. Plate Spacer 15. Shaft Coupler 16. Support Beam 153 17. Support Beam 157 (1) (1) (1) (1) (1) (1) (2) (2) (1) (1) (1) (1) (2) (4) (1) (1) (1) PBD-001-001 PBD-001-002 PBD-001-003 PBD-001-004 PBD-001-005 PBD-001-006 PBD-001-007 PBD-001-008 PBD-001-009 PBD-001-010 PBD-001-011 PBD-001-012 PBD-001-013 PBD-001-014 PBD-001-015 PBD-001-016 PBD-001-017 Fig. C.2. Bending Mechanism Parts List. 131 31 34 -5 I- F2 . 3-7 2 0.26 (FDRILL) 0.266 (F DRILL) .. .4X X0CHAMFE 4," X .03 21 0 2.700 0 0 r 0 12K 2.752| 2CHANFER 00 0 0535 4 .000 0 .1005 2 410-257 (F DRILL] 1# 10. 005JAIlal 12 *0.OODI z 490221(#2 DRILL] EDOI FEI .500 415 2N 0; I 32 U% 2.752 |X2 15 4X 0.257 (F DR ILL) 0 0 1F2 MIT Pian Science rFusion Centsr UNLESS OTHERWISE SPECIFIED DINEHIONS: INCHES NATERIAL: TOLERANCES: DRAWN BY: DATE: 20 FED 3CALE; 0.333 .xK ± .01 :k .001 FRACTIONS ± ANGLES A Xxx PART NAME: BOTTOM PLATE PART NAME: BOTTOM PLATE TY BEOP: At: ASTN A240 UNS 311600 I PER ASSEMBLY DAVID L. HARRIS 095 SIZE: A PART No: PHDal-001 IPART No: P80-001-001 1REV: C IREV: C rS 0 00 0 11*Be 0.0 2x A B.06 CHANTER 4i" X .O41340'04Q l 0.880 0 0-50 0% ~500 T .2502 J*1 .000a A1 0 29.CHANFER 10- X 7HAFE 0 $.266 (F DRILL] 0.256 | .1 1-2- 0 0. 2X 2.752 .0 (F DRILL] 2%.3T5l 11 F44CR 2x1. 1 .410,.88 0 9E7 01 FE .500 .475 -L 4X 0.251 0 (F D-RILL) 1*1#.0951AJsi 2M 2.152 212.155 2.52 42 32 410 ,257 (FDRILL) 1#1.005 JAJ MIT Plasma Scince & Fwain CAmter UNLESS OTHERWISE SPECIFIED DIWENSIONS; INCHES TOLERANCES: .11 :1- .01 FRACTIONS 6: .]I t: .001 ANGLES ± PART NAME: TOP PLATE Re: NATERIAL! UNS S3110 I PER ASSEMBLY OTY REMD; DRAIN Y: DAVID |, HARRIS DATE; 31 AY 2005 SCALE: 0333 SIZE; A PART No: PBOD-O-D2 *ASTA2AD IREV: C 1.250 1.100 .55- -750 WORW46EAR . 0" X .03 SPLINE 10 ,00081 AM - INVOLUTE HELICAL WC091EA Numbor of Toth Rl5 Normal Premnure Angle Normal Diametral Pitc Helix Anglc Transcric Circular Pitch Pitch D iffeter 2,25850 Outoldo Digmtor Fait Width 0.050 Addendum Ihole Depth 0. 13150 lorking Dcpth 0.12500 Clearance 0.01450 Tooth Thcicness 0.0981 ? Center Dialanta Iref) 1.48785 Backlash ii Assembly 0.003 Reftrcncc AGNA Guali1y Na. 9-10 32 R,-1Pie el -A NATING MORN IREFERENCE PART Na. PD-001-DDn Number of Threads Narmal Prcssurc Angie Lead Angle Hand of Lead Axial Pitch Pitek DIameter Outaide Diaeter 20' 5,00on RH 0.19110 0.71711 0.84211 Add idumh 0. 13950 Whole lfepth NOTES: I. All of the Scar tenth iurfates and Ihe surfucas that have a llnlah aptelfleatlen arm aurfare to hai. the following cLating applicd: Malybdenum Diiulfidc 2. Clock the Exterial Sp line relative 1o the Wora ear so that each Spline Tooth enterlilnd exactly a Igns with a lermgar Tenth cenler lino. MrrP a. Machl e the 01.25 hale in that It is ccitered an a spline tooth canteriinc. DINENlIONS: INCHES TaLERANCES: Xxx # .250 02.3816 X .03 2 Places EXTERNAL INVOLUTE SPLINE (ANSI B92.1-1910. R1193) Flat Root Sidc Fit Number of Teath Pitch Preuuilre Angle Boaa Diametar Pitch Diameter Major Diumctcr Farm Diameter Miner Diameter Full-Depth Tooth Face WldtI Circular Teeth Thickness Max Effectine Min Actual Talerance Clsa Reference PART No. 12 2040 30' 0.51162 ror D.60011 ref 0.65000 0.549 0,533 min C:) 0.500 0 0.07854 0.01191 H 5 P50-001-007 iKmla Science & Fusion Cmntar FRACTIONS ± ANGLES ± UOS 531600 ReF! ASTN A216,AAT1 YTREID; I PER AMEWLY DRAWN rY: DAVID L. HARRIS 20 FEB 2015 DAM SCALE; 1.000 ilE:; TORQUE GEAR A PART No: PSl-O0l-OO3 UNLESS OTHERWISE SPECIFIED .xx 21 4 16 h ARID ± .01 t .001 PART NAME: NATERIAL: REV: B L 1,100 .2ID- .T5D - IORNOEAR 0 2Place 0 I -. 0v - i . SPL INE -t J10.00081A 10 0D 2.0 1. INVOLUTE HELICAL UERNGEAR Numbcr of Teeth Normal Pressure Angle Hermal Olametral PItch Helis Angle Tranzmiorse Circilar Pitch Pitch Diameter Outside Diameter Face idth Addendum Whale Depth Workiug Depth Clearanc e It A 30 20' ii 0 19710 2.25559 2.34359 0.150 0.06250 0.13950 0.12500 0. 01450 Tath Thickness 0.09817 Center Distance (ref) 1.48785 0.003 Backlaih In Aiently Rafrentn AGMA Quality No. I-iD U4 V NKa0 N 03 YU.1 =-AI 32 4ir X .03 R.0O 4 Places MATING WDRM (REFERENCE] EXTERNAL INVOLUTE SPLINE PART No. P80-001-005 Number of Threads Narmal Pressure Angie Lead Angle Hand af Lead Atial Pitch Pitch Dianeter Outside Diameter Addendur Ehole Depth Flat Reat Sid. Fit Number if Teeth Pitch Pressure Angle Base Diameter Pitch Dialftcr Major Dieter Form Diameter Minor Diencter Full-Depth Tenth FaCe Width Clriular Tooth ThIckneis (ANSI 092.l-170, i193) In' 1.000 RH U,ISTIG 0,71111 0.84211 o.05250 0.1I3950 NOTES: Ma I. All ef the gear tooth surfacci and the surfaces that hare a surtae fInlIh specIfIcatIon are it have the following coatings applied! 2. Cloek the Erternal Spline relallrn to the Warmgear so that ach apl ine Spare centerline ezactly align: with a worigear Tooth centerlle. Nathine the 0.125 hole so Ihat It is cantered on a apl ine fitth contrline- Effeetlire win Actual Tolerence Class Rcference PART No. Molybdenum Disulfide 3. 2 Places 12 20'40 0.51962 ref 0.60000 ref 0.65000 0.541 0.533 min 0.500 0.0?554 0.01531 VD-QI-0 PBD0l-0 MIT Plasma Sciatca & Fusion Center MATERIAL: UNLESS OTHERWISE SPECIFIED DINENSIONI; INCHES TOLERANCES: .u1 -: .01 FRACTIONS : . 1K d:.001 ANGLES 1 UN$ $1I00. Wv AST TY RE0P ER ASSENBLY DRAIN aY: DAVID L. HARRIS DATE; 20 FEB 2005 SCALE: 1.000 SIZE: A PART NAME: PART No: PD-00i-004 TORQUE GEAR B 4 REV: B .10 .10 r - .000 WORMBEAR ---. 0 1.70 ref - .80IVH N M 55 5.2 II .3741 3741 0L3745 ----- ------ _-CH MFER CHANFER 45"45 HELICAL WORM6EAR of Teeth Preisure Angle Dlmnatral PItch Hells Angle Trananerie Circular Pitch Pitch Diamcier Otside Diameter Fate Width Addendum olf Depth lorking Depih Clearance Tooth Thichiess Center Dlitante Iref) Backlash In Assembly iRefaranea AGMA Quality No. INVOLUTE Nunber Normal Normal I 2 Places .. 27 21r 24 3.Doe 0.13101 1.12154 1.20988 0.800 0.0416? 0.09361? 0.00333 0.01033 1.106345 0.96134 0.003 9-10 X 0380 CH MFER CHAMFER 457 .03 2 Place& MATING WORM [REFERENCE) PART Ng. PBD-001-006 Number of Threads Normal Prestura Angle Lead Angle Hand of Lead Acigd Pitch Pitch Diemcticr Outside Diarieter A4dendum Uhola Depth 2r 3.000 RH 0.13105 0.19814 0.8947 0.04167 0.0367 .4 INVOLUTE WOHN Number of Threads Normal Preiamra Angle Lead Angle Haid of Lead Aiial Pitch Plich Diameter Ouislde Dlmamter Full-Depth Tooth Threaded Length [min) Toial Threaded Length [ma:) Addendum Whole Depth Working Depti Clearantes Tooth Thickness Cciter Distaice (rcf Backlash in Assembly Reference MANA Ovality N. 2t 5.ood RH . 19710 0.71711 0,84211 I.000 I.600 Q.06230 0. 13950 0.12500 0.01450 0.09817 x .03 MATING WORMEAR (REFERENCE] PART No. PBD-001-003 PART No. PBD-0DI-004 Number af Teeth 3' Normal Preaire Angle 20" Normal Dlameiral Pitch Helle Angle 5. coop Tranararue Circular Pilch U.111710 Piich Diameter 2.25059 Ouiside Diameter 2.38359 Addendum 0.01250 While Depth 0.13950 in 1.4BTS 0.003 0-10 0 Cd U NOTED: I. All of thu gear toath iur farea and the sur faces that hold a Surface finish ipelfcatlon are to hdre the folybeing coaunga applied: Mblybimnum Diullide Mrr Plafna Science & Fusion Center UNLESS OTHERWISE SPECIFIED DINEN4IONS: INCHES TOLERANCES: .ix ±.01 .KK ± .001 PART NAME: PART NAME: FRACTIONS ± ANGLES ± DRIVE SHAFT OH lYE SHAFT MATERIAL: OHS 331500 Her: ASTM AZTGAI? GTY RIOD: I PER ASSEMBLY DRAWN BY: DAVID L. HARRIS DATE; N FED 2005 3CALE; 1.011 SIZE: A PART No: POD-001-005 IPART No: PDD-OOI-005 1REV: B B IRFY: to ZI. l.E5U -25 rat 00 - .50 -4. SPL INE C . S~uME32 - 32 0.,315 c-fl A z0 12 51 1250 41X0 I.1 0 0.8 Places £7 .001 -0-1 a a a WAING WORNSEAR 4REFERENCE0 INVOLUTE WORM Number of Threads Nnrmal Pressure Angle Lead Angle Hand of Lead Axial Pitch Pitch Diameter Outuid Dinameter a ED 3.000 RH 0.13108 0.81947 Full-Depth Taotl Threded Lenith Imii Total Threaded Lenlth Imail) Addendum Whale Depth Wnrkimg Depth CIcarance Tuath Thirkneia Center Distance (ref) Backlash In Asieably ReFerene ASMA Quality No. S. 5000 0. 1500 0.04161 0.0136T o. 0333 0.01033 0.01543 PART Na. POD-001-005 Number of Teeth Normal Prcssure Angle Normal Diaiietral Plitch Helix Angle iranosyr4 Circular PItch Pitch Dianeter Outside Diameter Addendum Ihole Depth 27 21f 24 3.s OW 0.13101 1.12654 1.209811 0.0414 7 0.0936? 0.08134 0,003 N-19 45" N .03 2 Plncai EXTERNAL INVOLUTE SPLINE (ANSI 892,1-1970, R113) Flat Root SIde Fit Number if Tooth a Pitch 24141 Pressure Aigle Base Diameter 0.M64 ref Pitch Diandter 0.33333 ref Mfjor Din ter Form DIlamler Minor Diuaeter Full-Depth Teth Faec Iidth Cirtular Tooth Thickneis Nal Effectiri Win Actual Tolerance Class Reference PART Na. 0.31100 0.291 0.277 min 0.500 0.064 0.DIII S PBD-D-01 l NOTE!; of the gear tenth iurfaces end the surfaces that have a surface finish speilfIcatlei are to hare the following coot ings applied: All Malybdanum Diumifido 2. Mach Ine the $ .125 hole ha that It i4 centered on a spline Iooth centerline. MIT Plasma Scienca & Fusion Center UNLESS OTHERWISE SPECIFIED DIMENSIOHN; INCHES TOLERANCES: 11 := .01 FRACTIONS ±.ImI .001 ANGLES 1 PART NAME: PART NAME: INPUT SHAFT INPUT SHAFT MATERIAL UNS 531500 Ref- &STW A2?ILA479 OTY REOD; I PER ASSENBLY DRAIN BY: DAVID L. HARRIS DT: 20 FEB 2005 SCALE: |,000 SIZE: A IPART No: PBeD00-00 IPART No: PBO-O0i-000 IREV IREV:: a 2X R. 12 (N e-.I 000 5255 0500 1 I25 l.144 0:2_ Drilli 000niA HO12 |4|10 051A10| ticr ibe "1.5' n"end CHANFE 2K 4&1.07 1* 1. I na y.10 t53 .5UU -- |2N~~1 F- .. 1 N - #2 7 100 -000 6 Intcrnal lirstutC Splint (ANSI 1 H2. 1- 190, R1031 Flit Root Side Fit Number of Teeth 12 Plit 20140 Prassure Angla se Bnsc Diaratpr 0.519512 rcf Pitch Diameter 0.10000 r cf 0.66?50 mat NaJor Diameter 0.651 Form Diameter MInar DIameter 0.550 Faca Vidih Thru All Ciriular Spacr Width 91011117 Nax Actmal Nin EffactIve 0.0?654 lerance Clisi 5 Referente PART No. PBD-001- 003 POD-001-004 z CHANFER - 4f 03 -il ---- Ii gn the sp Iin cut ( the part's _ as shown - -- . T. Mfl Pwra Sciiice &Fusion Cnter UNLESS OTHERWISE SPECIFIED D1NEN1ONS: INCHES TOLERANCES: .Kx .xxx ±.01 I.001 FRACTIONS ± ANGLES ± PART NAME: TOROUE ARM 153 PART NAME: TORCUE ARM 153 _ I- UNS S3160D Ref: ASTM A240 2 PER ASSENRLY DRAWN BY: MAVID L. HARRIS DATE: la FED 2005 3CALE: 1.000 SIZE: A NATERIAL: OTY REOD: PART No: PART No: PSvo-ooi00 p~i-oai-aoj JREV: ~ 0 IREV: C H & b t E5 R.12 0 a H C -t C CD 250 |* - - 2.900| - 10 000 1A 1B I = 0.44 1#27 Brill I z C Ins r i be '1.51' a end CHANFE 2X 5'z07.01 .5500 0 a a a . 1250 0 .501223 00 z1.350 -* .00 .15E0 .j34j*21-Drill] 1*0 . 0SA1 003 .70 3D Inforial Invelu4. Spline 4ANSI 59E.1-1970. R1113) Flat Root Side Fit Number of Teck PItch Preiiure Angle Dsi Diameter Pitch Diameter Major Diameter Form Diameter MInor D I ameter Fact Wtldth Circular Spaeed 1Ith Mai Actual Min Effectiic Tolerance Clvi. Referente PART No. CH BFE 451.03 12 20)40 30" 0.51962 ref 0.60000 ref 0.16750 max 0.651 0.550 Thru Al 0.091171 0.0754 5 P0D-001 -003 POD-001-004 -E-- - MIT Plasma Sdene & ( -I- FWin Canter UNLESS OTHERWISE SPECIFIED DIMENSIONS; INCHES TOLERANCES: . :6 .01 FRACTIONS :I .mt .001 ANGLES 1 P A RT NAME : TORQUJE ARM 151 PART NAME: li I the spliae cut with the port'u 4. TORQUE ARM 157 MATERIAL! OTY REO0: 31600 Ref: ASTM A240 ? PER ASSEMBLY DRAIN BY: DAVID L. HARRIS DATE: I FEB 2005 SCALE: 1000 silE: A PA RT No: No: IPART UNS POD-001 -008 PBD-0QI-008 IR E V: B B IREV: V)~ 1.150 K ~I .350 1.000 31 .200 Frb-i ,~s0 -f.255 IN .250 io o o I 0 0 o 5 I I.000IIAI I 2 ._________ 3x - 129 3x R064 - - 0 0 0 1 105 0 R.063 0 3 0 HOLES 4-40 UNC-2b TAP T 0.25 #43 DR ILL M09) 0.40 II.005 A 1I--- 5I$!.I44 f*2? DRILL] .003 AB IR064 I 4K ~- ~ .53 ~ 0 . cd ~ TOD reF CHANFERED 4VW XEDGE--\, ) D .25 Too1 rtf .415 1l W0.3- ;] 2.30 - wc -A NOTE ; 1.Three chonnca Qrc machin-ed into ihe pnrt'a 5*I1d SANG wIre wI0 aurfae aa ahovn. Neep ihib in miud bc mplaed in ihe channell. wh i machInIng the chanieI ge metry. Ml PLwra Sciencx & Fusion Cmntar UNS S31611 Rif: ASTM A240 I PER ASWENDLY DRAWN BY: AVID L. HARRIS DATE: 21 APR 2005 MATERIAL: UNLESS OTHERWISE SPECIFIED DIMENSIONS: INCHES GTY REID; TOLERANCES: .KK ± .01 K : i.00 PART NAME: PART NAME: FRACTIONS± ANGLES i BEAM CLAMP A UEAM CLAMP A SIZE! A 3CALE: 1.000 PART No:- POD-001 -009 IPART No: PBD-OOI-DO~ REVIR[V: U .12500 ~0.I25T ~X .350 2.155 2. 50 o.12?570 f .1000 * -0 .000|A eBI A o fl o o o as I wj L .IJ .A- 0 LIII .250 r cf CHANFERED EDGE-4f X .0 0 0 o Isx .35 -1 0 4E 0 5X 0,144 (#2 0 -- 0 0 0 DRILL] 0.005 A B I . 13 ,- 3 HOLES-0.25 A-40 UHC-2b TAP 0.40 #43 DRILL (0.0911 +10.0051 AC 1Z2V + + r~~ir vrf R..063 .4375 I. IBIS I ~3I5 MIT Plasma Sdencx & Fuom UNLESS OTHERWISE SPECIFIED DIMEN101N:; INCHES TOLERANCE3: FRACTIONS : ,1: : ,01 , i .001 ANGLES i PART NAME: K BEAM CLAMP 0 W Cvnter RAf! ASTM k240 UNS 31600 I PER ASSEMBLY DAVID L, NARRIS 2'lAPR 2005 1.000 SIZE: A MATERIAL! TY REOD; DRAIN BY: DATE: SCALE; PART No: PBD-001-010 IREV: B r-i -- 0000 - 2- 0.1257v .255 AI .3S0 -20 0 1.000 0' 2x -f 0 m 0250 0 311.200 0 I 0 -v-LEI -A 0 . 30.700- . 215 0 0 ,.460 00 CHANFERED EDGE-2-"'r250 ...... 59 .144 1#2M DR ILL) 1 1 HB .0051A .0 . I. 23 700 3 HOLE #43 DRILL (D.09) V 0.40 4-40 UNC-Eh TAP T 0.25 6 141.095 1A IC R. 063 L-c-" X.03 rc f 33 R.06447 NOTES: I. Three hanneli ire machli4 Into fit partU Solid 8 AWG wire willUNESOHRIEPC aurfaca asn ahegnbc p~uird in fit channuii. Keep Ibi in mid whon mehInIng tha thainnel gTnmOtry MrT Pltma Scikrics &Fusion OTHERWIE SPEC & Cntar IFIED DINE11IONS: INCHES IGLERANCES: ± .01 FRAC TIONS ± .ii .KK J -001 ANLES PART NAME: - EAM CLAMP C PART NAME: BEAM CLAMP C ± z MATERIAL: 1113 331600 ReV: ASTIM A240 %TV gREgD; I PER ASSEMBLY DRAWN BY: DAVID L. HARRIS DATE: 21 APR 29) tCALE 1.000 ShE: A PART No: ~PART No: PBO-001-011 PBD-OOI-OIl JREV: 0 D IR[V: 00 C 350 / 00 2 .1250 2N eV0 A 5 .550 0 1* 10.D ooo A 0 3 HOLE 4-40 UNC-2b TAP T 0.25 #43 DRILL t0-01) T 0.40 1*10 250 0 [ 0 0 I. 0 ISIS 0 - -I .530 59 0.144 4927 DRILL .UU5 ADB .150 o 4- LIII -r~448 11 0-oC T T ref CHAMFERED EDGE 4Y 250 re {A-] & Fusion 'Plasma Sdcie UNLESS OTHERWISE SPECIFIED MIT DIWENSIONS; INCHES FRACTIONS : . : ,01 .i L : ,001 ANGLES 1 PART NAME: _ _ _ _ BEAM CLAMP D BEAM CLAMP I~ _ _ _ _ Rif MATERIAL! UNS 531600 _ _ _ ASIM A240 OTY RE00; I PER A33MUiLT DRAIN BY: DVI TOLERANCES: PART NAME: Ciritar 111 fif 45" X . 2. 30Q L HARRIS DATE. 2 APR 2005 SCALE: 1,000 SIZE: A PART No: PART No: PBO-001-012 PBD-D0I-012 IREV : IREV: B 0.' C 1.00 - LOU - LF 1.153 2X 0.257 (F OHILL) 1* 1 .005|A .0005 A B L7 .DOI 060 .250 E-0:E a l - -- w en .7530 C 2350?5 .500 .475f45" 1 1 .0. C C CHAMFER x .03 ALL AROUHD 6 1 z *1 CHAMFER X .03 ALL AROUIND C) Mrr Pina Sciance &Fusion Cnter UNLESS OTHERWISE SPECIFIED DINEIS1ONS: INCHES TOLERANCES: .K .xx ± .01 ± .001 FRACTIONS ± ANGLES d PART NAME: THRUST BEARING PART NAME: THRUST BEARING MATERIAL: UNS S31100 Ref: ASTM A240 GTY REqD; 2 PER ASSEMBLY DRAWN BY: DAVID L. HARRIS DATE: 21 APR 2005 SIZE! A 3CALE; 1.000 PART No: PBD3-001-a13 PART No: PBD-OOt-013 JREV IR[V: In U H B :1:| 0 I.T53 t 2k CHAMFER 45II 1 0 0.257 IF DRILLI + 0.00s A B MIT Plasma Sdcence & Fusion CAter UNLESS OTHERWISE SPECIFIED DIMEN3IOHI; INCHES TOLERANCE5: = D1 -9 , .=i .001 FRACTIONS :1 ANGLES ± PART NAME : PLATE SPACER PART NAME: PLATE SPACER MATERIAL! U|4P 31E 0 L Rev AJIM A216.Af?0 OTY RE00; 4 PER ASSEMBLY DRAIN BY! DAVID L. HARRIS DArE: ED JAN Z905 -SCALE: 1,000 SIZE: A PART No: POD-001-014 PART No: PBD-0OI-014 IREV: A A IREV: r-A -A 0 .50 ref +10.0051 A E 0 250 Internal Infoluto Spline Dato (ANSI 802.1-I1?0, RII31 Flat Root Side Fit Humber of Teeth a Pitch E4/46 Preijurt Angle )f Bass DIameter 0.28568 rof Plfteh DIamstir 1.33333 ref Najar Diameter 0.386 ma Farm Diamrter D.37U Ninar Digmeter 0.M2 Face 114th A1 SPLI NE .5D5 0.500 CHAMFER Circular Space Wldth Nas Acual Nin Effective inleruace Class Referencc PART No. 4" 0.0678 0.0154 N|,03 6 | POD-001-005 SECTION NOTES: 1. Clock the 0.125 hel. be that It ii centered on a splinc cut centerlinc. A-A 0 U M r PI-ma SCience &Fusion Cmtar UNLESS OTHERWISE SPECIFIED DINENliONS: INCHES TOLERANCES: .u ± .01 ,KKK : .001 FRACTIONS ± ANGLES i PARTf NAME: SHAFT COUPLER PART NAME: SHAFT COUPLER MATERIAL: UNS 331600 Rcf: ASIM A27G.A479 GTY REOD: I PER ASSEPELY DRAWN BY: DAVID L. HARRIS DATE I FEB 2005 3CALE: 1.000 SIZE! A PART No: PBD-001-al PART No: PBI~-~OI-OI~ JREV: IREV: B6 1 t'J ~j. q 00 5.253 I- 0 1.305 .416 1.000 I.188 Z-000 zp P. 00. 4K R.0125 (0.125] .500 .125 1-975 1.20 .750 I -----------------------------no ----------------------- 4 .032) 0 i ------------------------ ----------------------- 9SCALE 1,500 MIT Plasma Sditnc & UNLESS OTHERWISE SPECIFIED DIWENSIONS; INCHES FWiae Cuiter TOLERANCES: 6i D. I =: .001 FRACTIONS -L ANGLES h PART NAME: a E~m Is3 PART NAME: 5EAN 153 MATER IA L! S R544QQ ITl A lf OTY RE00; I PER AHMEBLY DRAIN By! DAVID L.HARRIS DATE; 20 FEB 2005 SCALE: 0.500 $12E; A PART No: P'OD-001-016 PART N~: rDD-OOI-0I6 !REV: IREV: C C 5.~ -7- i-iT I.9X.B 1= A .4~S .250 5.072 1.150 2.000 1.000 I. U -- I .0310 1~ -til -- 6%R..062 1.250 .500 .125 T59 1.375 1.go .01 50- ---------------------------- -0z -- -- -- -- -- -- -- -- -- - -- -:0- ----------------------------S.0321 --------------- ------ z SCALE 500 .. C Mfr PIwa Science & Fusion Cmtwr UNLESS OTHERWISE SPECIFIED DINENIONS: IWCHES NATERIAL: UN5 R56400 MiBAMI4 IY REED; I PER ASSEMBLY TOLERANCES: .xx ± .01 , .001 DRAWN BY: DAVID L. HARRIS PART NAME: FRACTIONS ± ANGLES ± BEAN 151 DATE, V FE 2005 3CALE; 9,500 $IZE A PART No: PBD-0l-0l1 REV: C 214 Probe 'c Fig. C.20. Probe model. 215 4 3* 2 10 19 9 87 Probe Parts List 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. Fig. C.21. Probe parts list. Flange Plate Large Probe Plate Upper Small Probe Plate Lower Small Probe Plate Flange Insulating Plate Hand Crank Support Rod Current Lead Tube Liquid Helium Fill Tube Bending Mechanism (1) (1) (1) (1) (1) (1) (8) (2) (1) (1) PBD-002-001 PBD-002-002 PBD-002-003 PBD-002-004 PBD-002-005 PBD-002-006 PBD-002-007 PBD-002-008 PBD-002-009 PBD-002-010 ON 0 0 0 L 0 0 0 750 12X 0 766 o0 ON A 014.25 B.C. CD o a 0- SCALE 0.125 0 W 3K 2.700 1.844 5.038 TAP 1/2-13 4M 0.4 219 TAP' 112 -13 FLANOE PLATE BOLT HOLES; ItZ HOLES ON A 0 14. 25 BOLT C IRCLE -.- 9038 MA P.l [i CA r. & UNLESS OTHERWISE SPECIFIED 1mATERIAL AL 6061 TY REOD; I PER A53ENDLT DRAIN By! DAVID L.HARRIS bDIEN310N; INCHES TOLERANCES: :1 0.01 . = 0.001 rC FRACTIONS : ANGLES ± PART NAME: FLAMGE PART NAME: FLANGE PLATE PLATE bArE; SCALE: IZ APR 2005 0.250 IPART No: p5o-on-ou IPART No: P60-002-001 REV: IREV: U N- ---2., 21 75 2X - cZ. TO-.m 2.9?5 - - -'-2.70 -. So 00 501- 0 a1 $.516 3X ZR 2.85 s.641 0 oo 000 0 0 SCALE (CW4 DRILL (41/64 0.200 DRILL)b 21 2.0.50 CD -i 2X 2.5fl 2-00 2K T 2.20 21 c1 .266- (17104 DRILL) .961 Mrr Pira Scirce & Fusion Cnter UNLESS OTHERWISE SPECIFIED DIMENSIONS: INCHEW TOLERANCES: .KX ± .01 FRACTIONS ± .001 ANGLES ± .KKK MATERIAL: GIB GTY HEQD; I PER ASSEMBLY DRAWN BY: DAVID LHRRI PART NAME: PART No: PBD-002-002 LARGE PROBE PLATE DATE; 21 NAB 2005 SZE! A 3CALE; 0.350 REV: t 00 fl tQ (p -I 2. 70 21,0 CA S . 00 2. T - -+ 1.60+- 000 0 a 1.40 - - 0 0 SCALE 0.250 ~1 0 (P CD U 04 DRILL) C C K' C C -T 2000 zx 2.70 ax 0.641 (it4 DR ILL (11164 RILL) .Dll --- MIT Plasma Sdence & Fusion Canter UNLESS OTHERWISE SPECIFIED DINEN310N; INCHES TOLERANCES: . : .01 FRACTIONS & . =: .001 ANGLES 1 PART NAME :UPPER SMALL PROBE PLATE MATERIAL! 610 TY RE00; I PER ASSEMBLY DRAIN BY: DAVID L. HARRIS DATE; AR 20 SCALE: 0,400 SIZE: A IPART No: PDD-0D2-003 IREV: 0 Cl 2.70 - 2 2.70 - - 2x I..m 2x BI p- 2x 1.81 2K - 60 -- 1.85 2x 60 - I.50 1.501.40S3x - .4 29 00 2x 0 0A0 SCAL E 0.250 12% 0.144 13#2 DRILL) 3raE% 2X 0. 141 f 0. 25 (41164 IR I .L) ~1~ 2X 55~ 2x 4X2 ~ 21 0 0.i0 x #.255 a X. 51 I3314 DRILL 411)64 DRILL) . Mrr Plana Science -4 1 & Fusion Canter 0 010 I PER UNLESS OTHERWISE SPECIFIED MATERIAL: DINEN4lON$: INCHE ASSENBLY DRAWN BY: DAVID L. HARRIS TOLERANCES: .KK ± -l .ANN b .00l FRACTIONS ± ANGLES h qITY 111D DAE:; 21 MAR 2005 SCALE; 0.400 SIZE: A PART NAME LOWER SMALL PROBE PLATElPART No: PBD-OD2-004 REV- a 220 Appendix D - Photos Fig. D. 1. Bending Mechanism. 222 Fig. D.2. Bending mechanism gear train. 223 Fig. D.3. Bottom Plate, Part No. PBD-001-001. 224 Fig. D.4. Top Plate, Part No. PBD-001-002. 225 Fig. D.5. Torque Gear A & B, Part No. PBD-001-003 & PBD-001-004. 226 yI D1 Fig. D.6. Drive Shaft, Part No. PBD-001-005. Fig. D.7. Input Shaft, Part No. PBD-001-006. 016 227 iM 1111'11 01 Fig. D.8. Torque Arm 153, Part No. PBD-001-007. 1 9 8 a Fig. D.9. Front View, Support Beam 157, Part No. PBD-001-017. fl OT ~ II L. 228 80 Fig. D.10. Back View, Support Beam 157, Part No. PBD-001-017. Fig. D. 11. Machining Support Beam 157. 9 229 Fig. D.12. Beam Clamp C, Part No. PBD-001-011. Fig. D.13. Beam Clamp D, Part No. PBD-001-012. 230 Fig. D.14. Top portion of Probe. 231 Fig. D.15. Probe prepared for testing. 232 Fig. D. 16. Flange Plate, Part No. PBD-002-001. Fig. D.17. Flange Insulating Plate, Part No. PBD-002-005. 233 Fig. D. 18. Large Probe Plate, Part No. PBD-002-002. Fig. D. 19. Upper Small Probe Plate, Part No. PBD-002-003. 234 Fig. D.20. Lower Small Probe Plate, Part No. PBD-002-004. Fig. D.21. Bending Mechanism Insulating Plate, Part No. PBD-002-01 1. Appendix E - Strand Heat Treatment 1.0 Sample Holder Preparation Holders: (2) Ti6Al4V fixtures with 5.953" section and fixture caps (1) Ti6A14V fixture with 6.072" section and fixture cap Name Tags: "IGC"and "European" 2.0 Test Wires Wire: ITER IGC Billet #B6770-1 (MIT 97-6) ENEA OST Type 1, Billet #7567 3.0 Wire Preparation Cut wires a. For each wire = Tail 30" x 2 + (6" + 3.8") x 6 = 119" b. Cut 119" long wire from each spool and put the name tag. c. Loop each wire in 4" diameter. Remove Cr-plating a. Remove Cr from the wires by etching with HCl (no diluting) in an ultrasonic bath (about 3 min). b. Rinse thoroughly with water and then with 100% ethylalcohol and dry. 4.0 Mount Samples in Heat Treatment Fixture a. Mount wire on heat treatment fixture. Keep 30" long tail from each end. b. Pinch each end a few times c. Store the sample in the plastic bag. 5.0 Sample Positioning in Furnace Holder SUPERCONDUCTING 811WIRE 811 3 6" 5.5" STAI NLESS STEEL RODS TEST SA MPLES CENTER OF F URNECE TL S 236 a. Position all samples corresponding to furnace centerline in the holder. b. Wrap the holder with stainless steel tool wrap foil carefully. Gas feeding tube end should be kept in the wrapping foil. c. The gas outlet tube on the furnace flange should be upper (at 12 o'clock). 6.0 Sample Heat Treatment Schedule IGC Heat Treatment Schedule Ramp rate 6 0C/hour to 185'C and hold for 20 hours Ramp rate 6 0C/hour to 350'C and hold for 3 hours Ramp rate 6 0C/hour to 460'C and hold for 25 hours Ramp rate 6VC/hour to 570'C and hold for 220 hours Ramp rate 6 0C/hour to 650'C and hold for 175 hours Ramp down 25 0 C/hour Total Time 23 days, 21:36:10 ENEA OST Heat Treatment Schedule Ramp rate 6VC/hour to 210 C and hold for 50 hours Ramp rate 6VC/hour to 340'C and hold for 25 hours Ramp rate 6VC/hour to 450'C and hold for 25 hours Ramp rate 6VC/hour to 575'C and hold for 100 hours Ramp rate 6VC/hour to 660'C and hold for 100 hours Ramp down 25*C/hour Total Time 18 days, 0:16:10 237 Fig. E. 1. Furnace for heat treating IGC samples. Fig. E.2. Furnace for heat treating OST samples. 238 Fig. E.3. Sample heat treatment fixture made from Ti6Al4V. Fig. E.4. Heat treatment fixture and cap coated with Graphokote to prevent sintering. Fig. E.5. Grooves machined in sample heat treatment fixture. 239 Fig. E.6. Heat treatment fixture after removing from furnace. Fig. E.7. Samples after heat treatment. 240 Fig. E.8. Samples are one continuous strand. Fig. E.9. Removing samples from fixture. Appendix F - Critical Current Test Results This appendix lists the test measurements for the bend tests. The tables present the data in the order in which it was taken. If a field in the table is left blank it means that measurements were made but no results could be determined from the data. This could be because the noise level was too high or the sample quenched before the electric field criteria was reached. The critical current was measured at an electric field level that was appropriate for short samples. Ec = 2 pV/cm Critical current criterion: The n-values were calculated using equation F.1. Two different n-values were determined using different electric field criterion. This was done because many of the samples quenched soon after they had reached the critical current criterion and measurement data was not available for the preferred n2 points. n L: E = 3.5pV/cm with corresponding current n2: E = 7.1 pV/cm with corresponding current -= EC (F.1) IC Table Nomenclature Ic = Critical Current Q = Quench Event H = High noise in data acquisition M = Medium noise in data acquisition L = Low noise in data acquisition Table F. 1. Test sample voltage tap separation distances (inches). Sample IGC153 IGC157 EU153 1 4.176 4.466 4.162 2 4.211 4.421 4.161 3 4.183 4.351 4.145 242 Table F.2. Test data for IGC 157, Sample #1. IGC157 #1 Test Number Strain (%) Current (A) IGC157.002 IGC157.008 IGC157.010 IGC157.016 IGC157.017 IGC157.021 IGC157.024 0.0 0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0.0 0.3 0.2 0.1 0.0 IGC157.025 IGC157.029 IGC157.031 IGC157.034 IGC157.035 IGC157.038 IGC157.041 IGC157.042 IGC157.045 IGC157.046 IGC157.047 IGC157.050 IGC157.052 Type nvaluel nvalue2 21 41 112 78 104 96 90 79 13 77 89 97 103 73 94 Ic-L Ic-L Ic-M Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-H Ic-H 7.39 12.08 11.03 11.5 12.25 6.07 6.04 5.77 4.88 5.32 5.18 6.48 6.87 10.79 5.2 8.45 12.18 103 106 Ic-L Ic-L 6.21 6.38 13.64 11.16 8.23 6.72 3.25 5.81 6.37 7.86 9.33 9.04 6.29 243 Table F.3. Test data for IGC 157, Sample #2. IGC157 #2 nvaluel nvalue2 17.9 14.6 22.3 11.4 6.9 2.0 5.0 5.0 5.2 5.5 6.7 11.8 7.5 2.2 5.1 5.6 6.0 6.5 10.6 Ic-M Ic-M 7.2 5.6 7.5 6.0 nvalue1 nvalue2 12.1 9.7 10.0 10.0 Test Number Strain (%) Current (A) Type IGC157.003 IGC157.011 IGC157.015 IGC157.020 IGC157.022 IGC157.023 IGC157.026 IGC157.027 IGC157.032 IGC157.033 IGC157.036 IGC157.037 IGC157.040 IGC157.043 IGC157.044 IGC157.048 IGC157.049 IGC157.053 0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0.0 0.2 0.1 0.0 55 114 108 121 115 97 56 7 52 72 89 96 82 Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-M 97 101 Table F.4. Test data for IGC 157, Sample #3. IGC157 #3 Test Number Strain (%) Current (A) Type IGC157.004 IGC157.012 0.0 0.1 0.2 59 75 94 Ic-L Ic-M Ic-L IGC157.013 244 Table F.5. Test data for EU 153, Sample #1. EU153 #1 Test Number Strain (%) Current (A) EU153.006 EU153.012 EU153.013 EU153.014 EU153.020 EU153.021 EU153.026 EU153.027 EU153.033 EU153.034 EU153.039 EU153.040 EU153.045 EU153.047 EU153.056 EU153.057 0 0.1 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0 91 104 114 146 105 144 100 98 60 60 61 64 65 65 65 67 Type nvalue 1 nvalue2 4.6 5.3 5.5 5.1 5.5 5.5 5.1 4.9 5.6 6.1 5.9 6.4 6.5 5.8 6.3 6.3 Q-H Q-H Q-H Q-L Q-L Q-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-L Ic-M Ic-M Ic-H 245 Table F.6. Test data for EU 153, Sample #2. EU153 #2 Test Number Strain (%) Current (A) EU153.007 EU153.011 EU153.015 EU153.019 EU153.022 EU153.025 EU153.028 EU153.032 EU153.035 EU153.038 EU153.041 EU153.044 EU153.048 EU153.055 EU153.058 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.6 0.5 0.4 0.3 0.2 0.1 0 91 139 157 148 149 154 125 57 70 88 103 112 117 116 118 Type nvaluel nvalue2 17.7 9.1 3.1 3.3 3.9 5.1 4.5 4.4 3.6 4.2 9.0 3.3 3.4 4.0 5.0 4.4 4.4 4.1 4.6 Q-M Q-L Q-L Q-L Q-M Ic-H Ic-H Ic-L Ic-L Ic-L Ic-L Ic-L Ic-M Ic-L Ic-M 246 Table F.7. Test data for EU 153, Sample #3. EU153 #3 Test Number Strain (%) Current (A) Type EU153.008 EU153.009 EU153.017 EU153.018 EU153.023 EU153.024 EU153.029 EU153.030 EU153.036 EU153.037 EU153.042 EU153.043 EU153.049 EU153.050 EU153.051 EU153.052 EU153.053 EU153.054 EU153.059 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.6 0.5 0.4 0.3 0.2 0.5 0.2 0.2 0.2 0.1 0 70 Q-H 125 100 117 102 111 72 45 46 48 49 50 Q-M 49 54 43 43 52 52 nvaluel nvalue2 Q-L Ic-L Ic-L Ic-L Ic-M Ic-M Ic-L Ic-M 7.3 3.2 5.3 4.9 3.8 3.7 10.2 3.8 4.2 4.2 3.8 4.0 Ic-L Ic-H 4.3 N/A 4.1 N/A Ic-H Ic-H Ic-H Ic-H 3.1 6.0 3.7 6.3 3.4 4.2 4.4 4.4 Q-L Q-L References Chapter 1 [1.1] Y. Iwasa, Case Studies in Superconducting Magnets Design and Operational Issues, 2nd edition, Springer-Verlag, New York, 2005 (draft). [1.2] J.V. Minervini, "Analysis of loss mechanisms in superconducting windings for rotating electric generators", Thesis (Ph.D.), Massachusetts Institute of Technology, Dept. of Mechanical Engineering, 1981. [1.3] Y. Iwasa, J.V. Minervini, "Superconducting Magnets", Course 2.64J, Lecture Notes, Massachusetts Institute of Technology, Dept. of Mechanical Engineering, Spring 2005, Lecture 7A, p5,12. [1.4] U. Essmann and H. Trauble, "The direct observation of individual flux lines in type II superconductors", Physics Letters, v.24A, 1967, p.526. [1.5] University of Wisconsin Applied Superconductivity Center website, http://www.asc.wisc.edu/plot/plot.htm, accessed July 2205. [1.6] Y. Iwasa, J.V. Minervini, "Superconducting Magnets", Course 2.64J, Lecture Notes, Massachusetts Institute of Technology, Dept. of Mechanical Engineering, Spring 2005, Lecture 6A, p11. [1.7] Y. Iwasa, J.V. Minervini, "Superconducting Magnets", Course 2.64J, Lecture Notes, Massachusetts Institute of Technology, Dept. of Mechanical Engineering, Spring 2005, Lecture 6A, p12. [1.8] Y. Iwasa, J.V. 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Tuck, "Long sample high sensitivity critical current measurements under strain", Cryogenics, v26, n7, July 1986, p 406-12. [1.29] N. Cheggour and D.P. Hampshire, "A probe for Investigating the effects of temperature, strain, and magnetic field on transport critical currents in superconducting wires and tapes", Review of Scientific Instruments, v71, n12, Dec. 2000, p 4521-4530. [1.30] D.M.J. Taylor and D.P. Hampshire, "Effect of axial strain cycling on the critical current density and n-value of ITER niobium-tin wires", Physica C, v401, nl-4, 15 Jan. 2004, p 40-6. [1.31] D. Uglietti, B. Seeber, V. Abacherli, M. Thoner, and R. FhIkiger, "Critical Current vs. Strain Measurements of Long Length Nb3 Sn Wires up to 1 OGGA and 17T using a modified Walters Spring", IEEE Transactions on Applied Superconductivity, v.13, n2, June 2003, p 3544-3547. [1.32] D. Uglietti, B. Seeber, V. Abacherli, A. Pollini, D. Eckert, R. Flukiger, "A device for critical current vs. strain measurements up to 1 OOOA and 17T on 80cm long HTS and LTS technical superconductors" Superconductor Science and Technology, v16, n9, Sept. 2003, p 1000-1004. [1.33] L.T. Summers, M.W. Guinan, J.R. Miller, P.A. Hahn, "A Model for the Prediction of Nb3Sn Critical Current as a Function of Field Temperature, Strain, and Radiation Damage", IEEE Transactions on Magnetics, v27, n2, pt III, Mar. 1991, p 2041-2044. 250 [1.34] A. Godeke, B. ten Haken, H.H.J. ten Kate, "Scaling of the critical current in ITER type niobium-tin superconductors in relation to the applied field, temperature and uni-axial applied strain", IEEE Transactions on Applied Superconductivity, v.9, n2, June 1999, p 161-164. [1.35] S.A Keys and D.P. Hampshire, "A scaling law for the critical current density of weaklyand strongly-coupled superconductors, used to parameterize data from a technological Nb 3Sn strand", Superconductor Science and Technology, v16, n9, Sept. 2003, p 1097108. [1.36] N. Cheggour and D.P Hampshire, "The unified strain and temperature scaling law for the pinning force density of bronze-route Nb 3Sn wires in high magnetic fields", Cryogenics, v42, n5, May 2002, p 299-309. [1.37] From Appendix A10.2, Expt'l Techniques in Low Temp. Measurements, Oxford Univ. Press, 2005. [1.38] J.W. Ekin, "Effect of transverse compressive stress on the critical current and upper critical field of Nb 3Sn", Journal of Applied Physics, v62, n12, 15 Dec. 1987, p 4829-34. [1.39] W.A.J. Wessel, A. Nijhuis, Y. Ilyin, W. 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