QCC Course Assessment Form (Short) Course: CH-104 Chemistry and the Arts Term: Fall 2013 Curricula: AM1, DA2, LA1 Chemistry Department 15 May 2014 Part I: Student Learning Objectives Table 1: Educational context This laboratory provides hands-on experience of the overlap between chemical theory and the practice of art in such media as photography, painting, textiles, and sculpture. Various methods of chemical investigation, including visible-light spectroscopy, chromatography, and other modern instruments are used to examine the physical and chemical properties of materials used in art. A lecture component in Chemistry and the Arts (CH-103) is required as a co-requisite. Table 2: Curricular objectives Curricular objectives addressed by this course 1. Communicate experimental results in effectively written laboratory reports (LA1). 2. Use analytical reasoning and apply logic to solve problems (LA1). 3. Use quantitative skills to perform experiments to prepare and identify materials used in art (MA1). 5. Integrate knowledge and skills in the primary field and across disciplines (LA1) 9. Employ concepts and methods of chemistry to make informed judgments (LA1). Table 3: General education objectives General education objectives addressed by this course (select from preceding list) 1. Communicate experimental results in effectively written laboratory reports (LA1). 2. Use analytical reasoning and apply logic to solve problems (LA1). 9. Use modern instrumentation to perform experiments and interpret quantitative results (LA1). 1 Table 4: Course objectives and student learning outcomes Course objectives 1. Students will demonstrate safe handling of potentially hazardous materials used in art. 2. Students will apply the scientific method to explore natural phenomena such as light and color. 3. Students will perform experiments and gain hands-on experience of the overlap between chemistry and the arts. 4. Students will gather, analyze, and interpret experimental data and draw conclusions related to methods and works of art. 5. Students will write effective laboratory reports that exhibit research ethics and unbiased treatment of data. Learning outcomes a. Students will learn about the toxicity of chemicals in their art supplies. b. Students will recognize likely hazardous materials in an experimental procedure. c. Students will understand and follow all safety procedures in laboratory. d. Students will practice proper disposal of hazarous materials in laboratory. a. Students will formulate testable hypotheses about materials related to art by applying chemical and physical theory. b. Students will design experiments to test scientific hypotheses. c. Students will identify possible sources of error in an experimental procedure. a. Students will work in groups of two to accomplish the objective of a scientific investigation. b. Students will interpret and correctly follow a laboratory procedure. a. Students will read modern instrumentation as used in their field. b. Students will report all data accurately to the proper level of precision. c. Students will summarize data in an appropriate form, such as a table or graph. d. Students will perform basic calculations on collected data to determine the value of a physical or chemical parameter that is characteristic of the material at hand. e. Students will recognize and describe a trend in quantitative data. a. Students will master the proper format and style of a formal laboratory report, including Objective, Introduction, Materials, Procedure, Data, Results, Discussion, and Conclusion. b. Students will evaluate experimental success by comparing results obtained to theoretical expectation, to colleagues results, and to outside authority. 2 Part II: Assignment Design: Aligning Outcomes, Activities, and Assessment Tools Table 5: Objectives selected for assessment Course objective(s) selected for assessment: (select from Table 4) 1. Students will demonstrate safe handling of potentially hazardous materials used in art. 2. Students will apply the scientific method to explore natural phenomena such as light and color. 3. Students will perform experiments and gain hands-on experience of the overlap between chemistry and the arts. 4. Students will gather, analyze, and interpret experimental data and draw conclusions related to methods and works of art. 5. Students will write effective laboratory reports that exhibit research ethics and unbiased treatment of data. Curricular objective(s) selected for assessment: (select from Table 2) 1. Communicate experimental results in effectively written laboratory reports (LA1). 3. Use quantitative skills to perform experiments to prepare and identify materials used in art (MA1). 9. Employ concepts and methods of chemistry to make informed judgments (LA1). General education objective(s) selected for assessment: (select from Table 3) 2. Use analytical reasoning and apply logic to solve problems (LA1). 5. Integrate knowledge and skills in the primary field and across disciplines (LA1) 3 Table 6: Assignment, outcomes, activities, and assessment tools Briefly describe the assignment that will be assessed: Students will be asked eight multiple-choice questions to assess eight different learning outcomes associated with one of the five course objectives for Chemistry and the Arts Laboratory. The assignment was designed by the course-coordinators and immediately follows this table. Table 7 provides the rubric that correlates each possible response with a student’s understanding of the underlying concept. The rubric anticipates certain common errors. All laboratory instructors will allot 20 minutes on the last meeting of the course to administer this assignment. The assignment will be graded immediately by the Scantron device. Desired student learning Description of the range Description of the outcomes for the assignment of activities student will assessment tools that engage in for this assign- will be used to meament sure how well students have met each learning outcome 1. Students will recognize likely haz- a. Students will attend class Students’ responses to eight ardous materials in an experimental to learn the necessary con- multiple-choice questions on procedure. (Course Objective #1; Cur- cepts, such as chemical termi- an assessment exam worth exriculum LA1; Gen. Ed. Objective #5 ) nology, to allow them to de- tra credit will be analyzed 2. Students will practice proper dis- scribe and evaluate art ma- according to the rubric beposal of hazarous materials in labora- terials from a scientific and low (Table 7). Students retory. (Course Objective #1; Curriculum chemical perspective. sponses will indicate their unLA1; Gen. Ed. Objective #5 ) b. Students will prepare for derstanding of central con3. Students will identify possible each meeting of laboratory by cepts, and particular wrong sources of error in an experimental pro- completing some combination answers will show which of cedure. (Course Objective #2; Curricu- of non-graded and graded ex- several common mistakes oclum LA1; Gen. Ed. Objective #2 ) ercises (pre-labs) prior to be- cur. Please see below for the 4. Students will interpret and cor- ginning each experiment. questions. rectly follow a laboratory procedure. c. Students will perform (Course Objective #3; Curriculum LA1; hands-on laboratory experGen. Ed. Objective #1 ) iments that require under5. Students will read modern in- standing and applying chemstrumentation as used in their field. ical principles. (Course Objective #4; Curriculum LA1; d. Students will apply stanGen. Ed. Objective #9 ) dard format and style in writ6. Students will report all data accu- ing laboratory reports that rately to the proper level of precision. summarize, interpret, and (Course Objective #4; Curriculum MA1; present experimental data Gen. Ed. Objective #3 ) gathered during an experi7. Students will perform basic calcula- ment. tions on collected data to determine the e. Students will take the Asvalue of a physical or chemical parame- sessment Exam at the end of ter that is characteristic of the material the semester. at hand. (Course Objective #4; Curriculum MA1; Gen. Ed. Objective #3 ) 8. Students will master the proper format and style of a formal laboratory report, including Objective, Introduction, Materials, Procedure, Data, Results, Discussion, and Conclusion. (Course Objective #5; Curriculum LA1; Gen. Ed. Objective #1 ) 4 Assessment Tool: An eight-question multiple-choice exam The following multiple-choice exam assesses a subset of eight student learning outcomes, each associated with one of five course objectives (Table 4). Each question assesses a single student learning outcome with regard to one of three course topics: instrumentation, preparation of a laboratory report, and safety in the laboratory. Instrumentation This section tests the proper reading of quantitative laboratory instruments. Successful performance in laboratory requires accurate measurement to the appropriate level of precision. Student learning outcome: Students will read modern instrumentation as used in their field. 1. An investigator pours distilled water into a graduated cylinder. Which of the following is the correct way to report the precise volume of water shown? (a) 10 mL (b) 10.2 mL (c) 12 mL (d) 12.4 mL (e) 12.8 mL Student learning outcome: Students will report all data accurately to the proper level of precision. 2. The line below represents the distance traveled by the solvent during a thin-layer chromatography experiment. Which of the following is the correct way to report the precise distance shown above? (a) 7.5 cm (b) 7.50 cm (c) 7.5000 cm (d) 8 cm (e) 75 mm Laboratory Reports This section tests preparation of a laboratory report, including pre-laboratory preparation. • Read the following Introduction and Procedure, adapted from Fundamentals of Laboratory Chemistry, 4th edition, by P. Wong, P. Irigoyen, S. Svoronos, and P. Svoronos (2005). 5 Introduction There are many physical methods for separating the components of a mixture based on their properties. These methods include formation of solutions, filtration of solids, evaporation of liquids, precipitation of insoluble solids, attraction to a magnet, and others. In this experiment, a mixture of sand and salt is separated by first dissolving the salt in water, and then filtering out the sand. The salt remains dissolved in the clear solution that passes through the filter. Heating this solution causes the water to evaporate, leaving pure solid salt. Procedure 1. Obtain an unknown mixture of sand and salt from your instructor and record the number of the unknown. Different unknowns contain different proportions of the two components. 2. Weigh a clean 150-mL beaker and a clean watch glass. Record both weights. 3. Place about 1 gram of the mixture in the beaker and record the weight. 4. Place about 10 mL of water in the beaker and stir to dissolve the salt. 5. Fold a circle of filter paper as demonstrated by your instructor and place it in a funnel. 6. Pour the mixture of salt, sand, and water through the funnel and filter paper and collect the filtrate in a small beaker. Allow the sand and filter paper to dry on the watch glass. Discard the dry filter paper. 7. Heat the filtrate on a hot plate until the salt appears dry. 8. Weigh the beaker with the dry salt and the watch glass with the dry sand. Student learning outcome: Students will interpret and correctly follow a laboratory procedure. 3. The following diagram illustrates an important step in the experiment. The arrow points to the filtrate. Which components of the mixture will be found in the filtrate? (a) Oil only (b) Sand only (c) Water only (d) Water and salt only (e) Salt, sand, and water 6 Student learning outcome: Students will master the proper format and style of a formal laboratory report, including Objective, Introduction, Materials, Procedure, Data, Results, Discussion, and Conclusion. 4. Which of the following sentences is most appropriate to include in the Materials and Methods (or Procedure) section of a laboratory report? (a) Place about 1 gram of the mixture in the beaker and record the weight. (b) Placed about 1 gram of the mixture in the beaker and recorded the weight. (c) A 1.15-gram quantity of the mixture placed in the beaker and weighed. (d) We placed 1.15 grams of the mixture in the beaker. (e) We had to place 1.15 grams of the mixture in the beaker and weigh it. Student learning outcome: Students will perform basic calculations on collected data to determine the value of a physical or chemical parameter that is characteristic of the material at hand. 5. If 0.8 grams of an unknown mixture were found to contain 0.2 grams of salt and 0.6 grams of sand, what percentage (fraction) of the mixture was salt? 2 ) (a) 2% ( 100 6 (b) 6% ( 100 ) Student learning outcome: dure. (c) 20% ( 51 ) (d) 25% ( 14 ) (e) 33% ( 13 ) Students will identify possible sources of error in an experimental proce- 6. An investigator reported that 1.50 grams of the mixture contained 1.00 grams of sand and 0.75 grams of salt. Which of the following sentences is appropriate to include in the Discussion and Conclusions section to explain this Result? (a) The sand was wet during weighing, therefore the reported weight of the sand is lower than the true weight. (b) The investigator neglected to subtract the weight of the beaker or watch glass holding the components, therefore the reported weights of both salt and sand are higher than the true weights. (c) The investigator did not heat the filtrate for sufficient time, therefore the reported weight of the salt is higher than the true weight. (d) The investigator heated the filtrate for excessive time, therefore the reported weight of the salt is lower than the true weight. (e) The experiment was completed successfully and all results matched expectations. 7 Chemical Hazards This section tests students’ ability to recognize chemical hazards and to dispose of waste in a safe, environmentallysound manner. Student learning outcome: Students will recognize likely hazardous materials in an experimental procedure. 7. Which of the following materials is most toxic? (a) calcium sulfate (b) iron sulfate Student learning outcome: (c) mercury-II sulfate (d) sodium sulfate (e) zinc-II sulfate Students will practice proper disposal of hazarous materials in laboratory. 8. Which of the following materials is acceptable to place in a laboratory sink? (a) broken glass (b) detergent (c) plaster (d) silver-I nitrate 8 (e) none of the above Part III: Assessment Standards (Rubrics) Table 7: Assessment standards (rubric and expectations) Student learning outcome: Students will read modern instrumentation as used in their field. Question 1: Which of the following is the correct way to report the precise volume of water shown? (medium) Response (a) 10 mL (b) 10.2 mL (c) 12 mL (d) 12.4 mL (e) 12.8 mL Evaluation Student incorStudent misinterStudent incorCorrect. StuStudent reads the rectly rounds to prets the markrectly rounds to dent reads the instrument to the by Rubric Expected Share (%) the coarsest unit of measurement (mL). ings on the instrument. the finest explicit unit of measurement, despite the fact that the instrument proviides additional information. instrument and correctly estimates the position of the bottom of the meniscus. appropriate level of precision, but incorrectly reads from the top of the meniscus instead of from the bottom. 10% 10% 10% 60% 10% Student learning outcome: Students will report all data accurately to the proper level of precision. Question 2: Which of the following is the correct way to report the precise distance shown above? (difficult) Response (a) 7.5 cm (b) 7.50 cm (c) 7.5000 cm (d) 8 cm (e) 75 mm Evaluation Student reads Correct. StuStudent inStudent incorStudent incorthe instrument dent correctly correctly exrectly rounds up rectly rounds by Rubric Expected Share (%) and incorrectly reports to the finest explicit unit of measurement (1 mm = 0.1 cm), despite the face that the instrument provides additional information. reads the instrument to the appropriate level of precision; the final ‘0’ indicates a length of precisely seven and a half centimeters. aggerates the precision of the instrument; a ruler does not measure length to the nearest thousandth of a centimeter. to the coarsest unit of measurement (cm). to the finest explicit unit (1 mm = 0.1 cm) and needlessly converts units (7.5 cm = 75 mm). 15% 40% 15% 15% 15% 9 Student learning outcome: Students will interpret and correctly follow a laboratory procedure. Question 3: The arrow points to the filtrate. Which components of the mixture will be found in the filtrate? (easy) Response (a) Oil only (b) Sand only (c) Water only (d) Water and (e) Salt, sand, Evaluation by Rubric Expected Share (%) salt only and water Student does not understand (or has not read) the Procedure: oil is not part of this experiment. Student does not understand that filter paper traps large, insoluble particles, such as sand. Student does not understand that salt dissolves in water and passes through filter paper with the water. Correct. Student understands that soluble salt passes through the filter paper with the water. Both collect in the beaker as filtrate. Student does not understand that the Objective of the experiment is to separate the various components of the mixture, and that filter paper traps large, insoluble particles, such as sand. 5% 5% 5% 80% 5% Student learning outcome: Students will master the proper format and style of a formal laboratory report, including Objective, Introduction, Materials, Procedure, Data, Results, Discussion, and Conclusion. Question 4: Which of the following sentences is most appropriate to include in the Materials and Methods (or Procedure) section of a laboratory report? (medium) Response (a) Place about (b) Placed about (c) A 1.15-gram (d) We placed (e) We had to Evaluation by Rubric Expected Share (%) 1 gram of the mixture in the beaker and record the weight. 1 gram of the mixture in the beaker and recorded the weight. quantity of the mixture placed in the beaker and weighed. 1.15 grams of the mixture in the beaker. place 1.15 grams of the mixture in the beaker and weigh it. Student does not recognize that imperative sentences are inappropriate in a laboratory report. Student does not recognize that a sentence without a subject is incomplete. Student omitted “was” and therefore failed to write the sentence correctly in the passive voice. Correct. Although many writers prefer to avoid the first person (“We”) in scientific writing, the sentence is complete and written in the past tense. Student uses unnecessary words (“had to”), and creates ambiguity with “it”. 10% 10% 10% 60% 10% 10 Student learning outcome: Students will perform basic calculations on collected data to determine the value of a physical or chemical parameter that is characteristic of the material at hand. Question 5: If 0.8 grams of an unknown mixture were found to contain 0.2 grams of salt and 0.6 grams of sand, what percentage (fraction) of the mixture was salt? (medium) 2 6 Response (a) 2% ( 100 (b) 6% ( 100 (c) 20% ( 15 ) (d) 25% ( 14 ) (e) 33% ( 13 ) ) ) Evaluation Student does Student does Student does Correct. StuStudent misunnot understand not understand not understand dent understands derstands the by Rubric Expected Share (%) the definition of percentage or proportion, and incorrectly guesses that “0.2 grams” means “two hundredths”. the definition of percentage or proportion, and incorrectly identifies the digit “6” as the most important piece of data. the definition of percentage or proportion, and incorrectly interprets “0.2 grams” as a proportion (0.2 = 20%) instead of a raw measured quantity. the definition of percentage or proportion, and can calculate the ratio of the relevant part to the whole. definition of percentage or proportion, and incorrectly calculates the ratio of the relevant part to the remainder instead of the ratio of the relevant part to the whole. 10% 10% 10% 60% 10% Student learning outcome: Students will identify possible sources of error in an experimental procedure. Question 6: Which of the following sentences is appropriate to include in the Discussion and Conclusions section to explain this Result? (difficult) Response (a) The sand (b) The investi- (c) The investiga- (d) The investi- (e) The ex- Evaluation by Rubric Expected Share (%) was wet during weighing, therefore the reported weight of the sand is lower than the true weight. gator neglected to subtract the weight of the beaker or watch glass holding the components, therefore the reported weights of both salt and sand are higher than the true weights. tor did not heat the filtrate for sufficient time, therefore the reported weight of the salt is higher than the true weight. gator heated the filtrate for excessive time, therefore the reported weight of the salt is lower than the true weight. periment was completed successfully and all results matched expectations. Student does not recognize that at least one number in the reported Results is too high, not too low: the sum of the two components’ weights is expected to equal the weight of the original mixture. Student does recognize that at least one number in the reported Results is too high, but does not realize that the magnitude of the difference is much too small to attribute to a major error like including the weight of an entire beaker. Correct. Student understands that the purpose of heating the salt or salt solution is to remove the water, and that insufficient time heating may lead to an overestimate of the weight of the salt due to unevaporated water. Student incorrectly believes that excessive heating can destroy salt. Student does not recognize that at least one number in the reported Results is too high; the sum of the two components’ weights is expected to equal the weight of the original mixture. 15% 15% 40% 15% 15% 11 Student learning outcome: Students will recognize likely hazardous materials in an experimental procedure. Question 7: Which of the following materials is most toxic? (medium) Response (a) calcium sul- (b) iron sulfate (c) mercury-II sul- (d) sodium sul- (e) zinc-II sulfate fate Evaluation by Rubric Expected Share (%) fate fate Student does not recall that calcium is a necessary nutrient and component of safe pigments, not a heavy metal or toxic element. Student does not recall that iron is a necessary nutrient and a component of safe pigments, not a toxic element. Correct. Student remembers that mercury is a dangerous heavy metal and pollutant. Student does not recall that sodium is very common and a necessary nutrient, not a heavy metal or toxic element. Student does not recall that zinc is a necessary nutrient and component of safe pigments, not a toxic element. 10% 10% 60% 10% 10% Student learning outcome: Students will practice proper disposal of hazarous materials in laboratory. Question 8: Which of the following materials is acceptable to place in a laboratory sink? (easy) Response (a) broken glass (b) detergent (c) plaster (d) silver-I nitrate (e) none of the above Evaluation by Rubric Expected Share (%) Student does not remember that solid waste never belongs in a sink, or that broken glass belongs in a dedicated waste container. Correct. Student realizes that detergent is a form of soap, and may go down the laboratory sink in reasonable quantities. Student does not remember that solid waste, such as plaster, never belongs in a sink. Student does not remember that heavy metal ions, such as silver, are typically toxic and therefore hazardous to the environment. Student does not realize that detergent is a form of soap, and may go down the laboratory sink in reasonable quantities. 5% 80% 5% 5% 5% 12 Part IV: Assessment Results Table 8: Summary of assessment results (N = TBD) Student learning outcome: Students will read modern instrumentation as used in their field. Question 1: Which of the following is the correct way to report the precise volume of water shown? (medium) Response (a) 10 mL (b) 10.2 mL (c) 12 mL (d) 12.4 mL (e) 12.8 mL Evaluation Student incorStudent misinterStudent incorCorrect. StuStudent reads the rectly rounds to prets the markrectly rounds to dent reads the instrument to the by Rubric Expected Share (%) Actual Share (%) Difference (% points) the coarsest unit of measurement (mL). ings on the instrument. the finest explicit unit of measurement, despite the fact that the instrument proviides additional information. instrument and correctly estimates the position of the bottom of the meniscus. appropriate level of precision, but incorrectly reads from the top of the meniscus instead of from the bottom. 10% 10% 10% 60% 10% 0% -10 5% -5 7% -3 76% +16 0% -10 Student learning outcome: Students will report all data accurately to the proper level of precision. Question 2: Which of the following is the correct way to report the precise distance shown above? (difficult) Response (a) 7.5 cm (b) 7.50 cm (c) 7.5000 cm (d) 8 cm (e) 75 mm Evaluation Student reads Correct. StuStudent inStudent incorStudent incorthe instrument dent correctly correctly exrectly rounds up rectly rounds by Rubric Expected Share (%) Actual Share (%) Difference (% points) and incorrectly reports to the finest explicit unit of measurement (1 mm = 0.1 cm), despite the face that the instrument provides additional information. reads the instrument to the appropriate level of precision; the final ‘0’ indicates a length of precisely seven and a half centimeters. aggerates the precision of the instrument; a ruler does not measure length to the nearest thousandth of a centimeter. to the coarsest unit of measurement (cm). to the finest explicit unit (1 mm = 0.1 cm) and needlessly converts units (7.5 cm = 75 mm). 15% 40% 15% 15% 15% 59% +44 22% -18 0% -15 0% -15 7% -8 13 Student learning outcome: Students will interpret and correctly follow a laboratory procedure. Question 3: The arrow points to the filtrate. Which components of the mixture will be found in the filtrate? (easy) Response (a) Oil only (b) Sand only (c) Water only (d) Water and (e) Salt, sand, Evaluation by Rubric Expected Share (%) Actual Share (%) Difference (% points) salt only and water Student does not understand (or has not read) the Procedure: oil is not part of this experiment. Student does not understand that filter paper traps large, insoluble particles, such as sand. Student does not understand that salt dissolves in water and passes through filter paper with the water. Correct. Student understands that soluble salt passes through the filter paper with the water. Both collect in the beaker as filtrate. Student does not understand that the Objective of the experiment is to separate the various components of the mixture, and that filter paper traps large, insoluble particles, such as sand. 5% 5% 5% 80% 5% 0% -5 5% 0 22% +17 46% -34 12% +7 Student learning outcome: Students will master the proper format and style of a formal laboratory report, including Objective, Introduction, Materials, Procedure, Data, Results, Discussion, and Conclusion. Question 4: Which of the following sentences is most appropriate to include in the Materials and Methods (or Procedure) section of a laboratory report? (medium) Response (a) Place about (b) Placed about (c) A 1.15-gram (d) We placed (e) We had to Evaluation by Rubric Expected Share (%) Actual Share (%) Difference (% points) 1 gram of the mixture in the beaker and record the weight. 1 gram of the mixture in the beaker and recorded the weight. quantity of the mixture placed in the beaker and weighed. 1.15 grams of the mixture in the beaker. place 1.15 grams of the mixture in the beaker and weigh it. Student does not recognize that imperative sentences are inappropriate in a laboratory report. Student does not recognize that a sentence without a subject is incomplete. Student omitted “was” and therefore failed to write the sentence correctly in the passive voice. Correct. Although many writers prefer to avoid the first person (“We”) in scientific writing, the sentence is complete and written in the past tense. Student uses unnecessary words (“had to”), and creates ambiguity with “it”. 10% 10% 10% 60% 10% 41% +31 20% +10 5% -5 12% -48 5% -5 14 Student learning outcome: Students will perform basic calculations on collected data to determine the value of a physical or chemical parameter that is characteristic of the material at hand. Question 5: If 0.8 grams of an unknown mixture were found to contain 0.2 grams of salt and 0.6 grams of sand, what percentage (fraction) of the mixture was salt? (medium) 2 6 Response (a) 2% ( 100 (b) 6% ( 100 (c) 20% ( 15 ) (d) 25% ( 14 ) (e) 33% ( 13 ) ) ) Evaluation Student does Student does Student does Correct. StuStudent misunnot understand not understand not understand dent understands derstands the by Rubric Expected Share (%) Actual Share (%) Difference (% points) the definition of percentage or proportion, and incorrectly guesses that “0.2 grams” means “two hundredths”. the definition of percentage or proportion, and incorrectly identifies the digit “6” as the most important piece of data. the definition of percentage or proportion, and incorrectly interprets “0.2 grams” as a proportion (0.2 = 20%) instead of a raw measured quantity. the definition of percentage or proportion, and can calculate the ratio of the relevant part to the whole. definition of percentage or proportion, and incorrectly calculates the ratio of the relevant part to the remainder instead of the ratio of the relevant part to the whole. 10% 10% 10% 60% 10% 20% +10 12% +2 15% +5 29% -31 10% 0 15 Student learning outcome: Students will identify possible sources of error in an experimental procedure. Question 6: Which of the following sentences is appropriate to include in the Discussion and Conclusions section to explain this Result? (difficult) Response (a) The sand (b) The investi- (c) The investiga- (d) The investi- (e) The ex- Evaluation by Rubric Expected Share (%) Actual Share (%) Difference (% points) was wet during weighing, therefore the reported weight of the sand is lower than the true weight. gator neglected to subtract the weight of the beaker or watch glass holding the components, therefore the reported weights of both salt and sand are higher than the true weights. tor did not heat the filtrate for sufficient time, therefore the reported weight of the salt is higher than the true weight. gator heated the filtrate for excessive time, therefore the reported weight of the salt is lower than the true weight. periment was completed successfully and all results matched expectations. Student does not recognize that at least one number in the reported Results is too high, not too low: the sum of the two components’ weights is expected to equal the weight of the original mixture. Student does recognize that at least one number in the reported Results is too high, but does not realize that the magnitude of the difference is much too small to attribute to a major error like including the weight of an entire beaker. Correct. Student understands that the purpose of heating the salt or salt solution is to remove the water, and that insufficient time heating may lead to an overestimate of the weight of the salt due to unevaporated water. Student incorrectly believes that excessive heating can destroy salt. Student does not recognize that at least one number in the reported Results is too high; the sum of the two components’ weights is expected to equal the weight of the original mixture. 15% 15% 40% 15% 15% 20% +5 34% +19 15% -25 7% -8 7% -8 16 Student learning outcome: Students will recognize likely hazardous materials in an experimental procedure. Question 7: Which of the following materials is most toxic? (medium) Response (a) calcium sul- (b) iron sulfate (c) mercury-II sul- (d) sodium sul- (e) zinc-II sulfate fate Evaluation by Rubric Expected Share (%) Actual Share (%) Difference (% points) fate fate Student does not recall that calcium is a necessary nutrient and component of safe pigments, not a heavy metal or toxic element. Student does not recall that iron is a necessary nutrient and a component of safe pigments, not a toxic element. Correct. Student remembers that mercury is a dangerous heavy metal and pollutant. Student does not recall that sodium is very common and a necessary nutrient, not a heavy metal or toxic element. Student does not recall that zinc is a necessary nutrient and component of safe pigments, not a toxic element. 10% 10% 60% 10% 10% 2% -8 2% -8 73% +13 5% -5 2% -8 Student learning outcome: Students will practice proper disposal of hazarous materials in laboratory. Question 8: Which of the following materials is acceptable to place in a laboratory sink? (easy) Response (a) broken glass (b) detergent (c) plaster (d) silver-I nitrate (e) none of the above Evaluation by Rubric Expected Share (%) Actual Share (%) Difference (% points) Student does not remember that solid waste never belongs in a sink, or that broken glass belongs in a dedicated waste container. Correct. Student realizes that detergent is a form of soap, and may go down the laboratory sink in reasonable quantities. Student does not remember that solid waste, such as plaster, never belongs in a sink. Student does not remember that heavy metal ions, such as silver, are typically toxic and therefore hazardous to the environment. Student does not realize that detergent is a form of soap, and may go down the laboratory sink in reasonable quantities. 5% 80% 5% 5% 5% 0% -5 29% -51 5% 0 0% -5 51% +46 17 Table 9: Evaluation and action plan A. Analysis and interpretation of assessment results: What do the results show about what and how the students learned? The current work represents the first assessment of Chemistry and the Arts laboratory and also the first ever assessment conducted of a laboratory section. The tool was designed to assess several learning outcomes, including use of instrumentation, safety, and writing formal laboratory reports. Despite the breadth of our goals, we chose to use a multiple-choice format to simplify administration and processing, and also to increase student participation. The average score among the 41 students taking the assessment quiz was 3.3 correct out of 8 questions. This performance is far better than students would achieve through random guessing, but also falls somewhat short of our—somewhat subjective—a prior expectations. Clearly, we underestimated the difficulty of some of the questions. Questions 1 and 2 assess students’ ability to use laboratory instrumentation correctly. Although the course largely eschews quantitative calculations, students must be able to measure accurately and read their instruments properly. On Question 1, 76% of students correctly estimated the final digit in the volume (60% correct expected). Question 2 was more challenging, many STEM students frequently make the same error as 59% of the current group by omitting the extra zero at the end of a particularly precise reading. Even though only 22% of students answered Question 2 correctly (40% correct expected), the correct answer was the second most common response. Question 3 required students to read a short laboratory manual procedure and correctly label a figure. Although the students were not familiar with the specific experiment described, it did use the filtration technique they had performed earlier in the semester. A correct response required carefully reading the procedure, and 46% of students did so (80% correct expected). This underperformance is consistent with other assessment questions that require careful reading. Question 4 asked students to recognize which of five choices was a complete sentence correctly rendered in the simple past tense. Students write thirteen laboratory reports over the semester, and they are expected to master the required format. As these assessment results show, many students never adopt the proper style: 41% incorrectly copied the imperative form, and only 12% (60% correct expected) gave the correct answer, which also happened to be the shortest, simplest, and most precise. Question 5 asks students to perform a simple calculation, similar to the only calculation performed during the semester. Only 29% did so correctly (60% correct expected). That the other answers were chosen with similar frequency suggests that many students simply guessed. Question 6 addresses one of the most challenging aspects of writing a laboratory report: identifying and rationalizing unreasonable results. If a sample contains 1.00 grams of one material and 0.75 grams of another, then the total sample must weigh at least 1.75 grams, not 1.50 grams. A careful reading of the procedure would show that the experiment required evaporating water, and that insufficient evaporation time would leave the sample wet and “too heavy”. It is likely that these students do not become familiar enough with the metric system to realize that a discrepancy of 0.25 grams is far too little to be explained by including a piece of glassware. The correct answer was the third least popular, being chosen by only 15% of students (40% correct expected). Questions 7 and 8 assess safety procedures. More students than expected correctly identified the toxic mercury compound (75% vs. 60% expected), and although only 29% knew that detergent was safe to place in a laboratory sink (80% expected), the most common response was that none of the materials ought to go down the drain. That answer is, of course, wrong, but the collective impulse to err on the side of caution is encouraging. • Strong understanding of instrumentation and safety • Clear problems with following a procedure and writing a laboratory report 18 B. Evaluation of the assessment process: What do the results suggest about how well the assignment and the assessment process worked both to help students learn and to show what they have learned? Chemistry and the Arts laboratory is generally more popular than the lecture component of the course, and students’ grades are typically rather high compared to the lecture. The experiments are mostly short and relatively straight forward, so students can succeed in the class primarily by participating and submitting acceptable written work. What these assessment results may show is that the writing students do as part of the laboratory section is not sufficient to achieve the targeted learning outcomes with respect to writing. It is less surprising that few non-STEM students develop strong quantitative skills during the course. An encouraging result is that most students internalize the practical requirements of working in the laboratory, despite the fact that many have never taken such a course or plan to do so again. Although the tool prooved to be more challenging than expected, it has provided valuable insight into students’ strengths and weaknesses upon completion of the course. • Hands-on learning occurs in the laboratory and shows up in the assessment • Students seem to exert little effort outside of class C. Resulting action plan: Based on the above, what changes, if any do you anticipate making? Because the content and experiments for this course are somewhat less familiar to most chemists, it may sometimes feel unnatural to require formal laboratory reports as most of us understand them. However, as long as the targeted learning outcomes include writing effective laboratory reports, instructors ought to standardize the format and grading. The assessment results also indicate difficulty with interpreting a laboratory procedure, and additional standardization of pre-laboratory preparation may improve student performance. Course coordinators have begun to discuss common pre-laboratory assignments and implementation of a general rubric for assessing (not grading) laboratory reports. Along with those efforts, all laboratory instructors now know the areas assessed by the tool, and can choose to include more time discussing instrumentation, waste disposal, and proper interpretation of results. • Seek to establish common standards for written work across sections • Consider a project to assess writing separately 19