M ING AND CONDITIONIN G GLUED JOINT S Information Reviewed and Reaffirme d July 196 1 No. 475 I111111 I Ir~ l 111IIIIIIIIIIIIIIIIT1, l i 111111IIIill,lilllill l FOREST PRODUCTS LABORATOR Y UNITED STATES DEPARTMENT OF AGRICULTUR E FOREST SERVICE MADISON . 5, WISCONSIN DRYING AND CONDITIONING GLUED JOINTS By Forest Products Laboratory, 2 Forest Servic e U .S . Department of Agricultur e In order to maintain quality of product and prevent warping, checking, sunke n joints, and other defects in the finished article, it is essential that woo d after gluing be brought to the moisture content most suitable for the sub sequent use of the article and that the moisture be evenly distribute d throughout . The moisture content of the wood may be either increased or decreased durin g gluing, by an amount depending on (1) the process used, (2) the form an d composition of the glue, (3) the amount of glue spread, and (4) the dimensions of the wood parts glued . In general, hot-press methods reduce the moistur e content and room-temperature gluing increases it . Glues of high water content add more moisture to the wood than glues of low water content, and heav y spreads add more than light spreads . More water is added by the glue to a construction made of thin plies than to one of equal thickness made of thic k plies . Furthermore, the percentage increase in moisture content from a give n amount of glue spread will be greater in woods of low specific gravity than in woods of high specific gravity . The older types of woodworking adhesives such as animal, vegetable, and casei n glues add considerably to the moisture content of the wood, and frequentl y effect an uneven distribution of moisture within the construction . The moisture added with the more recently developed synthetic-resin glues is much less and sometimes practically negligible . Table 1 illustrates the approxi mate effect on moisture content of gluing with several room-temperature-setting glues . The table is based on the assumption that the wood absorbs all of the water added by the glue . This is not strictly correct, since some of the glu e squeezes out of the joints and some water evaporates during the pressure period . The calculated percentages, however, are reasonably close to the results obtained in actual gluing . 1 "Original report dated May 1955 . 2 -Maintained at Madison, Wis ., in cooperation with the University of Wisconsin . Report No . 475 It is evident from these values that regardless of the type of room-temperature setting glue used, a panel consisting of plies of thin veneer throughout will require a drying period following the gluing operation, even though the - veneers were previously dried to 3 or 4 percent moisture content . Far les s moisture will need to be removed, however, when one of the resin glues is used rather than casein, animal, or vegetable glue . Conditioning Glued Thick Stock • When the moisture increase in the wood is small, as in thick lamination s dried to a suitable moisture content before gluing, only conditioning to uniform moisture content is necessary . A ', i -1 . . Sunken joints are common defects in the manufacture of thick edge-glued lumber glued at room temperature . They are caused by surfacing the stock too soo n after gluing . The wood at the joint absorbs more water from the glue than the N .remainder of the piece and therefore swells more . If the piece is surface d before this excess moisture is distributed, more wood is removed along th e joints than at intermediate points . Then, during subsequent drying and con - = :' r~= ?NG: ditioning, greater shrinkage occurs at the joints than elsewhere, permanent depressions are formed . Such depressions along the glue line may ,_ .,,'-.;x show very conspicuously in the finished panel when viewed under a side light .' - :_ .,rl . To avoid sunken joints in edge-glued lumber 1 inch thick, the following con. "r r ditioning treatments are recommended : - 7 days at 8o° F . and 30 percent relative humidity 4 days at 12 00 F . and 35 percent relative humidit y • 24 hours at 160° F . and 44 percent relative humidit y 16 hours at 200° F . and 55 percent relative humidit y The conditioning schedules given above are suggested for edge-glued panel s that will be used with a high-gloss finish and without veneering . If ther e is an appreciable layover period between the surfacing and the sanding an d finishing operations, the conditioning period can probably be shortened some what, since surface irregularities of certain magnitudes are usually remove d by the sanding . For edge-glued furniture panels that are subsequently covered with .crossbands (usually 116 or 1/20 inch) and face veneers (usually 1/28 inch), the con ditioning times shown above can be shortened at the different temperatures , perhaps as much as one-half . Report No . 475 Drying Plywoo d It is necessary to dry a part of the glue moisture from plywood and venee r panels pressed at room temperature . For example, assuming a moisture content of 3 percent in the veneer and an increase of 14 percent from the glue, th e panels when removed from the clamps or press would contain about 17 percent o f moisture . Such percentages are common in many types of plywood immediatel y after gluing, especially if made with casein or soybean glue . For use in cabinets, in furniture, or ride buildings, more than one-half of thi s moisture should be removed before the panels are ready to be put into th e finished article . For use outdoors or in unheated buildings, plywood con taining about 12 percent moisture will generally prove satisfactory . Wher e veneer is glued over a lumber core, the increase in moisture content of th e whole panel at thetime of removing the panels from the press is not so larg e as with thin plywood . In thick-core panels, however, the moisture from th e glue is largely confined to the outside of the core and to the veneer . There fore, the excess moisture of these parts is as great as in thin plywood an d must be dried out or allowed to equalize through the core . The moisture content of panels made with lumber core is also affected by th e type of glue used, but to a less extent than those made of thin veneer s throughout . Table 2 shows the amount of moisture added by the glue to tw o particular lumber core panel constructions . This table also shows that the moisture added by the resin glues is considerably less than the amount adde d with casein, animal, or vegetable glue, and this fact must be taken int o consideration both in drying the core lumber and in conditioning the glue d panels . If, for instance, the core in the first panel listed in table 2 i s dried to 5 or 6 percent moisture content and a urea or resorcinol glue i s used, final drying will not be required if an opportunity is afforded for th e moisture to become equalized among the plies . If thick cores (1-1/2 inches) are dried to a low moisture content before gluing , the water added in gluing the veneer onto the core may not bring the whol e panel above 7 or 8 percent moisture content, even when casein, animal, o r vegetable glues are used . Under such a circumstance, the panels are sometime s stacked solid in piles and allowed to condition . This practice requires a long conditioning period, and the absorption of moisture by the core afte r the crossbands have been glued to it subjects the whole panel unnecessaril y to severe stresses . A better practice for conditioning thick-core panels that contain excessiv e moisture, is to place the panels on stickers and allow them to dry in pane l kilns or in factory workrooms . This practice allows the excess moisture to b e dried from the panel faces, where it is largely concentrated, and does no t necessitate drying the thick-core stock to an extremely low moisture conten t before gluing . Panel kilns permit more rapid drying than factory workrooms , give a better means for controlling the conditions during drying, and sav e factory space . Report No . 475 -3- In panel kilns it . is- very easy to dry most three-ply and five-ply panel s satisfactorily in 24 hours . .Thtck stock and low drying temperatures increas e the required drying time . Results of tests at the Fores t . Products Laboratory in panel kilns show that under normal conditions the moisture added in .,glaing three-ply panels 3/16 of an inch thick, can be . dried out satisfactorily i n from 8 1t a16-hours : These tests also indicate that the desired essentials in . drying car be met b y - maintaining a constant temperature and relative, humidit y throughout the drying-. To save time in such kiln operations, . it i s _'advantageous to maintain conditions that correspond to a-moisture conten t slightly below that to which the panels are to be'dried .. Table 3 shows, several combinationa of temperatures and relative humiditie s that will bring-the stock to . approximately the desired moisture content, bu t that will not allow an appreciable amount of drying beyond this point . Panels_should be-open-piled on strips called stickers . The stickers shthild be made from dry, straight-grained wood, entirely free from stain or decay . Moreover, the stickers should be dressed to a uniform thickness . Seven-eighths by 1-1/4-inch stickers should be used in drying the usual run•of .panels . In loading a kiln t--ruck, stickers should be placed at the extreme ends of th e panel and the intervening space so divided that the distance between sticker s will .not exceed 18 inches : Where there is danger of warping, the sticker s may be spaced a That apart . It is important that the stickers in each tie r be placed in verticca1 alinement on solid foundations'to prevent the_panel s from sagging . .The possibility of Carping in the upper panels may be furthe r reduced by placing a cover board On stickers on top of the'pile Sometime s the piles are weighted, but experiments indicat e-,that the application o f .-- . pressure to panels during drying 'does not reduce warp to an important,degi'ee : ' Whenever practicable, plywood should be so piled as to provide flues from .the top to the bottom of the load in order that-air may readil y- move in a vertica l plane-through it . Drying .'panels to an'excessively low moisture content materially increase s warping,' checking, opening 'of 'joints, and other defects . Tests show that the ;-amount of warping'on three-ply veneer panels is approximately preTortionalto, . the percentage of moisture removed from the panel in drying : In a few instances, plywood has been dried on mechanical veneer driers and o n hot-plate presses . _- These methods, however, have been confined to plywoo d of a high- .moisture content that was glued with water-resistant glue . Plywood dried in this way is usually comparatively thin and not of--the highest quality . The use of mechanical driers and hot-plate presses results in quick drying o but involves more expensive equipment than the other methods . Plywood and other members glued on hot presses at around 300° F . commonly contain some 2 or 3 percent moisture when removed from the press . Such - material should be conditioned to about 6 to 8 percent if intelded for, . This may service interior use and to about 12 percent if made for exterior be done in conditioningtrooms in-which a relative humidity is maintained tha t . is approximately equal to or slightly in excess of that corresponding to th e Report No . 475 -4- desired moisture content . Another method is•to apply sufficient water to the . hot-pressed panels to bring th'ilt to the required moisture content and then . ' to stack the. solidly, allowing the "moisture to equalize : throughout . . should be used to apply only :-sufficient water to bring the panels . to-th e desired moisture content . The correct amount of water can be readily ' calculated after determining . the moisture content and weight of thedry ga elp :. The moisture is conveniently applied by passing the panels between. rater'.: ' : covered rolls, .such as in a glue spreader ; or by spraying By weigiing a number of panels before and after the application of . the . water, the amount and uniformity of-theapplication can be checked . The_time required fo r equilization it the solid piles again varies with . the .thickmessof the individual . panels . While. the panels " are usually warm .whe.n. the`.waater ts ' applied , a circumstance that .aids equilization, the glue lines/especially o f synthetic-resin glues," . retard diffusion . Conditioning periods for plywdo l .Of •.1 . different thickness , and number of plies should- be based . on actual .moistu content determinations of_ both the interior and ekterior plies . Report No . 475 Table 1 .--Calcu.latedpercdntagesl of moisture added to wood ingluin g five-plyconstructions with roam-temperature-setting glue s Species Thickness : Moisture added in gluing• with • of each : : ply or : Casein, :Room-temperature- :Room-temperature :lamination :animal,or : setting urea - :setting resorcinol resin glue s resin glue s : :vegetable : : glues Inch Percent : Percent Percent 23 .6 17 .4 11 .8 8. 7 15 .1 11 . 1 : 7 .6 5.6 15 .5 : 5 .9 4.3 3/8 5 .2 : 2..0 1.5 Sitka spruce : 3/4 2 .6 : 1 .0 .7 Yellow birch 1/8 10 .0 : 3 .8 2.8 Yellow birch : 3/8 3 .3 : 1 .3 .9 Yellow birch : 3/4 1 .7 Yellow-poplar : 1/32 62 .0 Yellow-poplar : 1/16 31 .0 Yellow birch 1/32 40 .0 Yellow birch : 1/16 20 .0 Sitka spruce : 1/8 Sitka spruce : . .6 - .5 -Calculated percentages are based on oven-dry weight of wood and volum e at 12 percent . In the calculations it is assumed that all the sur plus solvent added by the glue is absorbed by the wood . This assump tion is known to be somewhat in error, but it nevertheless affords a satisfactory basis for comparison . Spreads of 75 pounds of wet casein, animal, or vegetable glue and 4 7 pounds of wet'urea- and resorcinol-resin glues per 1,000 square fee t of single glue line are assumed in these calculations . It is assumed ' that the casein, animal, or vegetable glue is mixed one part dry glu e to two parts of water (solids content•33 percent), the cold-setting _ urea resin one part dry glue to 0 .65 parts of water (solids conten t 60 percent), and that the mixed resorcinol-resin glue has a solid s content of 70 percent . Report No . 475 ti Table 2 .--Calculated percentages) of moisture added to wood in gluing five ply lumber core panels with room-temperature-setting glue s Face and back : Cross : bands : Core : : Moisture added in gluing- with : Casein, : RoomRoom animal, : temperature- :temperature or :setting urea- : settin g vegetable resin glues : resorcinol glues : resin glue s Percent 1/28-inch :1/20-inch :15/16-inch : black : sweetgum : sweetgum : walnut : 1/20-inch :1/20-inch :5/8-inch mahogany : yellow- : chestnu : poplar . tor sweetgum : : 7 .0 10 .7 : Percent Percen t 2 .6 2 .0 4 .0 . 3 .0 -Calculated percentages are based on oven-dry weight of wood and volum e at 12 percent . In the calculations it is assumed that all the sur plus solvent added by the glue is absorbed b y. the wood . This assump tion is known to be somewhat in error, but it nevertheless affords a satisfactory basis for comparison . 2 "Spreads of 75 pounds of wet casein, animal, or Vegetable glue and 4 7 pounds of wet urea and resorcinol-resin glues per 1,000 square fee t of single glue line are assumed in these calculations . It is assume d that the casein, animal, or vegetable glue ismixed one part dry glu e to two parts of water (solids content 33 percent), the cold settin g urea resin one part dry glue to 0 .65 parts o f 1 water (solids conten t 60 percent), and that the mixed resorcinol-resin glue has a solid s content of 70 percent . Report No . 475 Table 3 .--Combinations of temperatures and relative humiditie s suitable for dryingplywoodpanels to moisture contentvaluesof4to 12 percent, inclusiv e Moisture content desired (percent) 6 7 : Percentage of relative humidity for use with stated temperatureZ •• : • ° . ° . 100° F . :110° F . 120° F . 140° F . 90° F :. : 70 F . s 80° • : 19 : 24 rr ;rrrr .r .rr- ;-r-r-rrr=-rr rr---r~-rrrrr : : • • : : 20 26 : -27 : -28 : 29 : 32 : 33 : 35 45 : 46 : 48 57 : 58 .30 s 31 10 43 : 44 12 55 : 56 : rrr-r-ri ;rrrrrr--'r 22 19 8 • 1 4 21 59 24 26 : 31 34 : 37 41 •5o 53 61 ..b5. • : The relative humidities shown for the lower temperatures and moisture content values are obtainable ordinarily only during the winter season . Where a low moisture content is necessary during warm, humid weather , it can be obtained by raising the temperature . Report No . 475