MEMS Amplification of Piezoelectric Strain for In-Plane Actuation by Nicholas J. Conway B.S., University of California at Berkeley (2001) Submitted to the Department of Mechanical Engineering in partial fulfillment of the requirements for the degree of Master of Science in Mechanical Engineering MASSACHUSETTS INSTITUTE OF TECHNOLOGY at the LB MASSACHUSETTS INSTITUTE OF TECHNOLOGY 8 2003 -LIBRARIES June 2003 @ 2003 Massachusetts Institute of Technology The author hereby grants to Massachusetts Institute of Technology permission to reproduce and to distribute copies of this thesis document in whole or in part. Signature of Author ........................... Department cdflechanic ngineering i?/ 9 May 2003 Certified by ............................. - Sang-Gook Kim Professor of Mechnical Engineering hesis Supervisor A ccepted by ................................... Ain A. Sonin Engineering of Mechanical Professor Chairman, Committee on Graduate Students BARKER I g7 li I, MEMS Amplification of Piezoelectric Strain for In-Plane Actuation by Nicholas J. Conway Submitted to the Department of Mechanical Engineering on 9 May 2003, in partial fulfillment of the requirements for the degree of Master of Science in Mechanical Engineering Abstract To provide a competitive actuating solution, microelectromechanical systems (MEMS) based actuators need low operating power and form factors. Piezoelectrics provide substantially higher work output/volume for a given voltage, when compared to other actuating solutions. In addition, macro-scale piezoelectric based actuators provide the basis for many precision actuating solutions. To this date, however, there are few examples of precision piezoelectric devices fabricated in-situ at the MEMS level. There are two main factors to attribute this to: limited strain of the piezoelectric thin films, and fabrication difficulties. This thesis provides the solution to these two issues, as well as introduces a scalable design for developing compact in-plane actuating solutions for MEMS devices. Applications of low voltage, high displacement in-plane actuators include MEMS RF switches for mobile electronics applications as well for micro- and nano-transport. The actuator was designed using axiomatic design to address four functional requirements. The first requirement of high amplification is addressed using the angular advantage of bending beams. The second requirement of high force output is addressed by the high mechanical The third requirement that the efficiency of the amplifier through use of flexural pivots. amplifier end-effector move in a straight line is obtained through use of a four-bar guiding linkage design. The arrayable aspect of the design is addressed by an electrode bus which allows the actuators to additively move in series, and in parallel. The device is fabricated using the piezoelectric thin film of lead zirconate titanate (PZT), deposited in a sol-gel form and the resist SU-8. Fabrication was done at the Microsystems Technology Laboratory (MTL) at MIT. Preliminary results indicate the design achieved strain amplification in excess of 10:1, and can be arrayed successfully. Thesis Supervisor: Sang-Gook Kim Title: Professor of Mechnical Engineering 3 4 Acknowledgements I'd like to thank Professor Sang-Gook Kim for believing in my idea. My office-mates Stan Jurga, Yong Shi, Raj Sood, Chee Wei Wong and Dr. Yong-bae Jeon for helping me out whenever I needed it. Professor Triantaphyllos Akylas and Professor George Barbastathis provided support and gave me academic enthusiasm. The extra support of the staff at MTL, including Paul Tierney, Dave Terry, Kurt Broderick, Vicky Diadiuk, Dennis Ward, and Bob Bicchieri. My family for giving me support throughout my life. My friends here at MIT, Chris Dames, Ivan Skopovi, Ali Tabaei, Jeff Hiller, Denise Poy, and Dave Willis for helping me get started here at MIT. My friends in Westside for helping me stay grounded and my lady, Alicia, for the smiles at the beginning and end of the day. 5 6 Contents 1 Motivation 11 2 Piezoelectric actuation 14 3 4 2.1 The piezoelectric effect . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 2.2 Polarization and hysteresis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 2.3 Sol-gel thin film PZT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16 2.4 Strain induced by an electric field . . . . . . . . . . . . . . . . . . . . . . . . . . . 17 21 Design 3.1 Amplification (FR 1 with DP1) . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23 3.2 Constraining the end effector with a parallel guiding linkage (FR 2 ,DP 2 ) . . 3.3 Efficiency (FR 3 with DP 3 ) . . . 3.4 Powering an array of actuators with an electrode power bus (FR 4 with DP 4 ) .. . . . . . . . . . . . . . .. 26 . . . . . . . . . . . . 29 . 30 33 Modeling the device 4.1 Static Analysis: Amplification ratio expectations. . . . . . . . . . . . . . . . . . . 33 4.2 Dynamic Analysis 4.3 The coupled device dynamics: expectations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39 . . . . . . . . . . . . . . . . . . . . . 44 5 Fabrication 48 6 Results and Discussion 54 6.1 Q uality of PZT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54 6.2 A ctuation Test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56 7 7 Conclusion and Future Work 7.1 Conclusion 7.2 Future Work ......... . . . . . . . ... 58 ....................................... . .. . . . . .. . . . . . . . . . . . . .. 58 . . . . . 58 A Process Details 64 B MATLAB Scripts 68 C Miscellaneous 73 8 Nomenclature T Stress, internal D Electric displacement P Polarization Y Elastic modulus S Strain E Electric Field 6T Free dielectric constant ES Clamped dielectric constant k 33 Longitudinal coupling constant k 31 Transverse coupling constant k1 5 Shear coupling constant dij Piezoelectric constant (Strain/field) eij Piezoelectric constant (Stress/field) SE Compliance at constant field (short circuit) sD Compliance at constant electrical displacement (open circuit) cE Stiffness at constant field k Torsional stiffness linear constant kL Axial stiffness linear constant K Material stiffness 9 10 Chapter 1 Motivation To provide a competitive actuating solution in the embedded electronics world, microelectromechanical systems (MEMS) based actuators need low operating power and voltages, and a small form factor. Traditionally, a majority of MEMS devices use electrostatic actuation. The positives of electrostatic actuation include high micro-scale displacement, ease of fabrication, and linearity of actuation, balanced by the negative of a large form factor required to obtain a large micro-scale forces, at high operating voltages. Thin film piezoelectrics for MEMS, con- versely, have the exact opposite qualities: small displacement, difficult fabrication, non-linear, high power output (forces) at a small form factor and operating voltages. Robust fabrication and displacement or strain amplification of micro-scale piezoelectrics would enable an actuator that has good performance in all five qualities. Figure 1-11 shows a comparison of different types of actuators. As is evident, the piezo- electric PZT has not only a substantially higher work per volume ratio than many other types of actuators, but also operates at high cycling frequencies. Note that this data is for bulk PZT. Thin film PZT can withstand much higher electric fields. Assuming the elastic modulus of thin film PZT changes very little from the bulk value, the equation given in Table C.1 for piezoelectric work per volume 2 , gives 1.2x10 7 J/m 3 . This is two orders of magnitude larger 'From: P. Krulevitch, A.P. Lee, P.B. Ramsey, J.C. Trevino, J. Hamilton, and M. A. Northrup, "Thin Film Shape Memory Alloy Microactuators," JMEMS Vol. 5, No. 4. 1996 pp 270-282. Added to the figure by the author is the thin film PZT point. 2 Thin film PZT typically has strain coefficients about 50% of the bulk value, so let d 33 = 200xlV12 m/V. Thin film PZT has demonstrated it can withstand electric fields as high on the order of 100V/ yim[20]. This comes 11 108 la SMA i04 Zsolid- thin film +1bSMA S PZT 3 thermo. pmaic 106- 5ae=, 04 themal expanion 6ae.s e 1.05- 7&PZT # * Sbe.. +8 muscle 1S-- 6b e-. 5Ce n.. 103 9W9pbbble 7b Zat O 1 02 1 10 102 1. )4 101 106 167 Cycling Frequency (Hz) Figure 1-1: Work per volume versus cycling frequency for various microactuators. Numbers refer to Table C.1, which gives details on the calculations. Ideal values, shown with unfilled diamonds, represent the energy available for actuation. Other values (filled diamonds) are based on actual microactuator data. than the bulk value in the table, putting thin film PZT actuators in the same regime as shape memory alloys, but with the added benefit of faster response times[261. Piezoelectrics have a maximum extensional strain limit on the order of 0.1%. For MEMS applications where a displacement of 10 pim might be desired, a piezoelectric would need to be on the order of 1 cm long if it were directly coupled to the end effector 3 . For a practical micro-scale application, that form factor is unacceptable. Therefore, it is imperative that we develop a means of amplification of piezoelectric strain[3]. In the last decade, several methods have been used to amplify piezoelectric strain in macrofrom the relation between electric displacement, D, and the electric field, E, which the authors approximate as (Y and d 33 are the elastic modulus and strain coefficient respectively): work/volume= ID - E :: Y (d33E)2 3 An end effector is the part of an actuator that interfaces the non-fixed components in the mechanical system. 12 scale size actuators, these include multi-morphs (cantilevers), moonies[4], rainbow ceramics[3], and hydraulic piston based actuators [2]. More recently, the moonie-type actuator was refined by Jaenker to form a hybrid actuator using parallel guiding linkages and flexural pivots. Of theses solutions, only multi-morphs have been implemented in full at the MEMS level to this author's knowledge [5]. A hydraulic piston actuator with a peak amplification of 50:1 has been implemented at the MEMS level, but was assembled a microfabricated device with a piezoelectric stack and had dimensions of 20x20x10mm[27]. MEMS piezoelectric multi-morphs fabricated thus far, operate normal to the wafer plane, due to constraints of fabrication, and as such, there are limitations on the geometry and path of the end effector. Residual stress levels of films in the multi-morph must be carefully monitored in order to set and control the end effector position. The moonie-type design, in which the displacement of the end effector is significantly uncoupled from stress in the actuating member as neither end of the actuating member is fixed solves this problem4 . In-plane actuation5 is important for the design of sophisticated compliant mechanisms, as compliant mechanisms can most easily be micro-fabricated by 2-D photolithography. To this date, however, there are limited examples of piezoelectric devices fabricated in-situ6 at the micro-scale, most of which are cantilever-type (not in-plane). There are two main factors to attribute this to: limited strain and fabrication difficulties associated with piezoelectric thin films. This thesis provides the solution to these two issues, as well as introduces a scalable compact design for developing in-plane actuating solutions for many MEMS devices. 4 Chapter 3: Design will make this clear. Refer to Figure 3-6 for an example of a macroscale-precision piezoelectric actuator. 5Actuation in a plane parallel to the substrate surface on which a microdevice is fabricated. Typical substrates are silicon, quartz, and pyrex wafers. 6 Many MEMS devices have been made by assembling a piezoelectric element with a separately fabricated microfabricated structure. 13 Chapter 2 Piezoelectric actuation In choosing a piezoelectric to work with, the author chose sol-gel lead zirconate titanate (PZT) for three main reasons: 1) of piezoelectric materials available for micro-fabication, lead based ceramics like PZT have relatively high piezoelectric strain coefficients compared to other piezoelectrics, 2) the author's research group has experience with sol-gel PZT, and 3) time constraints on development prevented the search for other materials and methods of deposition (including sputtering PZT). Compared to other piezoelectrics for MEMS such as ZnO and Polyvinyledenefluoride (PVDF), PZT has a significantly better piezoelectric strain coefficients[11]. 2.1 The piezoelectric effect The "piezoelectric" effect occurs due to spontaneous, or self, polarization of the crystal structure. Piezoelectric materials tend to have high dielectric constants and function well in capacitors. The ions in the crystal can be stable at non-polar equilibrium positions, and do not have a center of charge symmetry in the crystal structure. When a stress is applied to a piezoelectric, positive and negative charges builds up on surfaces, in a phenomena called the piezoelectric effect. The inverse or anti-piezoelectric effect manifests when an electric field applied across a piezoelectric shifts the crystal ions, inducing a strain. For the sake of this paper the anti- prefix will be dropped for brevity as it is the anti-piezoelectric effect that is used in actuators[14]. Piezoelectrics function well as quasi static-micropositioning actuators using feedback control to compensate for any non-linearities, hysteresis, and drifts[24]. 14 a) P b) s E E Figure 2-1: Typical hysteresis of a piezoelectric in response to an applied electric field. a) polarization, and b) strain. 2.2 Polarization and hysteresis Piezoelectric ceramics are randomly polarized prior to exposure to an external electric field. Before using, the dipoles of each grain need to be alligned in order to get a uniform piezoelectric effect, in a process called poling. Thicker film dielectrics typically need to be poled at an elevated temperature in a high electric field. For the case of thin films (< 1 pm), the field is usually high enough at lower voltages, that the film polarizes during operation. Increasing the electric field for thin film PZT beyond a critical field (between 40 and 100 V/ Am depending on film quality), results in dielectric breakdown. Excessive current draw can also cause problems. After polarization, when the applied field is small, the strain is proportional to the applied electric field. If the electric field becomes too large, the strain curve deviates from linear behavior and hysteresis occurs due to polarization reorientation and polarization magnitude changes'. This generates a butterfly strain hysteresis curve[15]. Figure 2-la) shows a plot of a typical polarization hysteresis, and Figure 2-1b) shows a typical strain hysteresis that results in response to the application of an electric field. In each case, an initial polarizing field applied leaves a remnant polarization, and a remnant strain. 'Every time an electric field is applied, the piezoelectric is re-poled to a certain extent. 15 Figure 2-2: Perovskite crystal structure of ABO 3 -[17 2.3 Sol-gel thin film PZT The advantages of using PZT sol-gel are two fold: (1) the film composition is more uniform than sputter-deposited PZT, and (2) the equipment costs are low, as only a spin coater, hot plates and a furnace/RTA 2 machine are required to create the PZT. Spin coating the PZT necessitates a flat substrate surface. Typically, a polished silicon wafer is used. Since each coating is less than 0.25 pm thick, the surface roughness and feature heights need to be on that order 3 . Also, the thin coating means many coating steps are required to obtain ~1 pm films. PZT is suspended in a solvent (propylene-glycol based), that needs to be removed in order to allow the PZT to be annealed to the proper crystal structure. Pyrolysis, or drying, on a hotplate after each coating removes the solvent. This process is critical as it defines the adhesion (interface stress) of the film to the substrate beneath it. Lead is a highly volatile metal, so it is important that diffusion of the lead to the substrate not occur during the annealing process (650+ 'C). A diffusion barrier of Si0 2 (insulator) and Pt (electrode) is used to prevent interdiffusion of Si and Pb. In order to anneal to the proper piezolelectric crystal structure, the perovskite phase, the PZT film needs nucleations sites to stimulate crystal formation during annealing. 2 3 To create RTA: rapid thermal anneal The coating thickness is particular to the PZT sol-gel used in this work, see appendix for details. 16 these sites, a bottom electrode layer of platinum/titanium on top of the silicon-dioxide is used. TiO. forms perovskite nucleation sites by titanium diffusing through platinum to the PZT. Without nucleation sites, PZT can form the wrong crystal structure (pyrochlore phase, poor or no piezoelectric properties). Figure 2-2 shows a general perovskite crystal structure. PZT is a solid solution consisting of PbZrO 3 and PbTiO 3 (A = Pb, B = Zr,Ti) . Below a certain temperature (Curie temperature), the positively charged Pb, Zr, and Ti displace from the positions shown in Figure 2-2 with respect to the negatively charge oxygen atoms and generates The crystal lattice is elongated by the polarization to a self-polarizing dipole in the crystal. form a tetragonal, rather than the depicted cubic structure. X-ray diffraction crystallography can confirm the proper crystal structure. The necessity of the metal layer (as a diffusion barrier and crystal nucleation enhancer) beneath the PZT limits the geometry of the substrate prior to PZT deposition. Processing is complicated further because the etch selectivity of annealed PZT is similar to SiO 2 . The solution to these problems proposed and used during this research is to pattern and etch the sol-gel coated PZT film prior to annealing, when it has a much higher etch rate than SiO 2 (not densified) [21]. 2.4 Strain induced by an electric field Lead-zirconate-titanate, ( Pb(Zr,Ti)0 3 or PZT) has a tetragonal crystal structure, and is a member of the class 4mm point group4 . PZT behaves electromechanically as follows in equations (2.3) and (2.4), relating the tensor-based constituitive properties of piezoelectric strain, the strain coefficients, dmi, the compliance, s9, and the free dielectric constanct, &6k, to the strain, Si, the stress, T, the electric field, Em, and the electric displacement, Dm[22]. For simplicity, these equations ignore thermal effects, which can be important in determining the dielectric constant and strain. Si = sET + dmiEm (2.1) 4Crystal types are classes. Out of the 32 crystal classes, 20 are piezoelectric. Although piezoelectrics lack full crystal symmetry, the symmetry that they do have allows for the simplification of the property tensors. 17 Dm (2.2) dmiTi + ernkEk s2 s3 0 0 0 T1 0 Gd SE 0 0 0 T2 0 0 d 0 T3 0 0 d33 S s S2 s2 E8 S3 SE sf SE 3 0 0 13 E 13 3 +E2 31 S4 0 0 0 s4 0 0 T4 0 S5 0 0 0 0 sE 0 T5 d15 0 0 0 0 0 0 sE0 T6 0 0 0 T 1 0 0 (S6 -0 Di D2 = D3 0 6 0T1 0 -0 0 0 0 0 di 0 0 0 d15 0 0 d 31 d 33 0 0 0J [d 31 (2.3) d15 0 T 150 T3 + < 24 (2.4) 0E 0 - - T5 Ei 6T 3 E3 kT6) For simplicity of design, it is convenient to utilize the transverse strain mode (contraction/expansion) of PZT. Figure 2-3 shows this transverse mode. An electric field is applied in the 3-direction(determined by polarization) which is in the thickness direction (dimensioned by t) of the film. When the field is applied, strain is induced in the 1,2,and 3 directions of the film. In the 1- and 2- directions, strain is proportional to the d31 strain coefficient. In the 3-direction it is proportional to the d 33 coefficient. Equations (2.3) and (2.4) reduce to equation (2.5) in the transverse mode. S2 S3 D3 s11 1a2 S8E E S8E E 13s3 1f3 d31 d31 S13 d31 T1 Esf3 d Ef? 12d331 T2 833 d33 T3 d33 63_ 11 13(2.5) {E3 Strain is equal in the 1- and 2- directions, but the displacements, AL and AW are not necessarily. They are linearly dependent on L and W. 18 This generalization ignores the effect S t E I A2 | 9t W Figure 2-3: PZT actuated in the tranverse mode. Field in the E 3 direction. of the stiffness of the structure, and mechanical coupling in general (Poisson effects, etc.). To simplify the system further, we can ignore internal bias, or residual stresses in the PZT generated during fabrication (T = 0). To estimate the strain in the L direction only, we use strain we use: SL = AL =d L 31 (2.6) E 3. For a capacitor E 3 can be approximated by, _V (2.7) E3 = -, t Where V is the applied voltage across the capacitor, generating the electric field. Stress, -, is, approximating PZT as isotropic with an elastic modulus YPZT, -= YPZTSL = V t YPZTd31-- (2.8) The axial force, FPZT, is stress times cross sectional area. This is given by[18], FPZT = V = YPzTd31WV. o-A = O-Wt = YPZTSLWt = YPzTd31-Wt t (2.9) Taking into account the structural stiffness, kL, the actual displacement, AL, becomes, 19 AL - FPZT kL where kL is the stiffness of the structure. YPZTd31WV kL _ (2.10) For a PZT member, considering the stiffnesses of surrounding electrodes and dielectrics of each layer, j, kL is, Y2Aj .Z k_ = L Strain gradients across the thickness of a thin film result in bending. (2.11) Symmetry of stress in the actuating member about its neutral axis is important to prevent bending and to maintain a transverse mode. Piezoelectric actuators operating in an transverse mode described, can have frequency responses as high as 100kHz. Operating in a bending mode (like a multi-morph), the response is in the range of 100Hz to 10kHz[16]. The micro-scale offers an opportunity to increase natural frequencies further because mass sizes are so small. 20 Chapter 3 Design The axiomatic design process[6] was chosen such that the goals and design space of the project could be clearly defined. In short, axiomatic design consists of relating the functional require- ments (FRs) ,or goals of a project, to the design parameters (DPs)of a particular design upon Two key guiding axioms in the design process are: (1) attempt which the goals will depend. to maintain the independence of each functional requirement and (2) minimize the information content of the system, that is, to keep the design simple. the constraints of the design and manfacturing space. All this must be done subject to An uncoupled design is a design such that a particular functional requirement can be adjusted independent of other functional requirements of the system. A decoupled design is a design such that functional requirements may be achieved by the selected design parameters, but the functional requirements can only be satisfied by adjusting design parameters in the proper order. A coupled design is one such that the functional requirements are not inpendent of each other. The following equations provide a simple matrix representation of each design type, to better understand these concepts. Equations (3.1), (3.2), and (3.3) depict uncoupled, decoupled and coupled designs respectively. Notice that the uncoupled design is diagonal, the decoupled design is triangular (lower), and the coupled design is neither1 . FR1 X 0 FR2 L0 X DP1 J DP2 'For a thorough discussion of axiomatic design, refer to Nam P. Suh's "Axiomatic Design" [6]. 21 (3.1) FR1 X 0 DP1} FR2 X X DP2 FR1 X X DP1 FR2 X X DP2 (3.2) (3) To embark upon this design, a design paradigm was needed for several reasons. because this is a proof of concept project, it is important to keep the goals in mind. First, MEMS devices tend to have highly coupled designs, decoupled at best, because of the serial nature of fabrication, material constraints, and fabrication constraints 2 . Therefore in MEMS design it is challenging to keep functional requirements independent [25]. This design is very uncoupled from a purely design standpoint, but the micro-fabrication process leaves the design decoupled due to the forward and backward coupling nature of thin film fabrication. Functional Requirements (FRs): FR 1 : Amplify piezoelectric strain by a factor of 10 or more FR2 : End effector motion must remain in a straight line. FR3 : High efficiency of energy transfer FR 4 : Device must be arrayable Chosen Design Parameters (DPs): DP 1 : Angle of amplifying structure DP 2 : Four-bar linkage controls the rotation of the end effector direction DP 3 : Dimensions of flexural pivots to minimize energy loss. DP 4 : Electrode bus must conduct potential in such a way as not to impede amplifying dynamics or efficiency. Constraints: C 1 : Form factor of 500 pm X 500 ptm C 2 : Photolithography precision (2 1 am precision with facilities used) C 3 : Etching fabrication precision and adhesion 2 MEMS devices are usually fabricated in place. That is, parts are not assembled, but rather built into the device. This makes fabrication a coupled process. Parts fabricated earlier are affected by later parts (backward coupling), and later parts depend on the geometry of prior fabricated parts (forward coupling). 22 C y or jowl SLFP's Figure 3-1: Compliant parallel guiding linkage amplifying structure. Small length flexural pivots (SLFP) act as pivot points. C 4 : PZT strain limit of ~0.1% This thesis is to prove the concept of a device that the FR's comprise, and as such, there will be no more functional requirements. Process variables and flows have been determined Figure 3-1 depicts the 2-D top view of the during production and are given in the appendix. design, which satisfies the functional requirements. 3.1 Amplification (FR 1 with DP 1) Figure 3-2 represents the design's amplification principle. Two ends of a link are constrained to move along two perpendicular walls. The angle, 0, that the beam makes with the horizontal wall, fully defines the link's position in space. Let the left end of the link be the input and the right end be the output, defined by x and y respectively. If 0 changes, then the change in y versus the change in x is clearly going to be, 23 y x Figure 3-2: Amplification principle Ay Ax sinG - sin00 cos 0 - cos 0 0 2 cos - (0 2 sin . (0 + Oo) sin 21 (0 - 00) (0+Oo) sin (0 -0o) Cos 1 (0 -sin' +0o) sin - (0 - 00) + 0o) sin - (00 - 0) 1 = - cot -(0+00), where the displacement amplification, Ay/Ax, is a cot 0-like relationship. Ay/Ax, from 0 to 45 degrees, with 0 (3.4) 2 If we plot 0 = 0,we get the plot shown in Figure 3-3. For small angles, the displacement amplification is huge, with a negative change in x causing a positive change in y. For the small strain of piezoelectrics, this technique would be ideal for amplifying the strain. Since the strain limit is small, operating an amplifier around a small initial angle would be ideal. Also notice that amplification is only dependant upon the initial angle, 00, and the actual angle, 0. When 0 is less than 450, the mechanism is a displacement amplifier and a Fi,, is reduced. When 0 is more than 45 , the structure becomes a force amplifier and a displacement reducer. For maximum displacement amplification, 0 should be as close to 0 as possible. For maximum force amplification, 0 should be as close to 900 as possible. We now can decompose the DP for the amplification ratio into two parameters due to the PZT strain limit constraint. DP 1 : The initial angle, 0 0, of the actuating arm. DP1 2 : The angle 0. Since we are not decomposing the associated functional requirement, it is evident that this is a redundant design. As will be evident in the analysis section, the output force does not follow 24 0 -20 -40 Ay/Ax -60 -80 -100 -120 5 10 15 20 25 0(deg) 30 35 Figure 3-3: Plot of the amplification ratio versus theta. 25 40 0 = 0. 45 a reciprocal relationship, but neglecting to losses due structural stiffness (the hinges/pivots), the output force F0 .t is, |Fout| = |FinIt an 0. Eq. (3.5) satisfies conservation of energy (integrating from 3.2 (3.5) f() F tdy = x( Findx). Constraining the end effector with a parallel guiding linkage (FR2 ,DP 2 ) The amplifying mechanism in Figure 3-1 is created in a high-aspect-ratio MEMS material such as by etching the structure in a silicon wafer, or the spin-on SU-8 resist. An actuating member connects locations A and A' on one face of the structure (parallel to the xy plane). This member is made up of the active material, PZT. Let A and A' be the input surfaces. Let location B be fixed and C is free to move. As locations A and A' are drawn together a certain distance, that displacement gets amplified non-linearly by the four four-bar linkages that connect B to A,A'to C, the end effector. The guiding linkage ensures that the end effector surface, C, will stay aligned to the fixed surface at B (the end effectors will not rotate) and external disturbances will preferentially result in end effector motion in the y direction, and input surface motion (A and A') in the x direction, thus satisfying FR 3 . The actuating member's symmetric boundary conditions (it is suspended between points A and A'), significantly uncouples effects of bending moments induced by stress from the amplifying mechanism 3 . Because the amplifying mechanism is designed to be least stiff in the x and y directions, the majority of the motion will occur in those directions. The parallel guiding linkage effect is accomplished using small length flexural pivots (SLFP's), which are compliant pivots that closely approximate a pure rotation as all of the bending stress is concentrated at the SLFP rather than the surrounding material (see Howell[7] for a full discussion of SLFP's). Bending occurs at the location and directions of least resistance, in the xy plane, because the high-aspect-ratio structure is very thick at all points other than the middle 3This is important in microactuator designs because residual stress in thin films can often undesirably deform actuators when they are released. This is a particular problem in cantilever-type designs. 26 F_ in Figure 3-4: Idealized model of the mechanism. of flexure hinge. This is similar to a big resistor and a small resistor in parallel; most of the current goes through the small resistor as the small resistor can be likened to a wire when compared to the big resistor. Figure 3-4 shows an equivalent model of the device. The SLFP's behave as torsional springs and the device itself is made up of four parallel guiding linkages. Lines represent links and spirals represent hinges. The input force is Fi, and the output force is Fost. Using symmetry we can look at one of the four linkages at a time. Figure 3-5 shows that the dynamics of the system can be described using one generalized coordinate, 0. The amplifying mechanism design is similar to the macro-scale design by Jaenker[23] (see Figure 3-6), but with the difference that the pivots are 1) notch-type hinges and 2) each hinge's longitudinal axis is aligned with the normal to the direction of the hinge motion, ensure that each hinge is bending in its most compliant mode, leaving the least resistive directions, the x and y. The asymmetric notch hinge design limits stress concentration since each hinge is operating in a non-fully reversed stress regime, and also concentrates bending in a smaller 27 y k F k out 2 F. in Figure 3-5: Symmetry model Figure 3-6: A hybrid design by Daimler-Benz AG Research. ~10cm wide. Peter Janker, Frank Hermle, Thomas Lorkowski, Stefan Storm, and Marc Wettemann, "Development of High Performing Piezoelectric Actuators for Transport Systems". Actuator 98: 6th International Conference on New Actuators, 17-19 June 1998, Bremen, Germany, pp 181-185. 28 Figure 3-7: Asymmetric notch hinge region, more closely behaving like an ideal pivot (see Figure 3-7). The PZT film thickness is small, less than 1 Iam, so the voltage required to actuate is small. The amplifying mechanism's structural stiffness should compensate for bending moments generated by the off-neutral axis PZT member (high-aspect-ratio). Lastly, the design takes advantage of batch micro-fabrication such that no assembly is required. Jaenker claims an amplification ratio of 10. 3.3 Efficiency (FR 3 with DP 3 ) We want the output force of this amplifying transmission to follow the reciprocal tan To do this, we look to the efficiency of 0 (cotangent) relationship as closely as possible. a piezoelectric member and amplifier system, with associated stiffnesses respectively. KPZT and Kamp, The amplier and piezoelectric member are acting as springs in series. If we look to the mechanical efficiency of the amplifying structure, it would be the ratio of work of the piezoelectric member and amplifier to the work of just the piezoelectric member. Since the work done is proportional to the stiffness, we can say, K1 7 lmechanical = Wamp+PZT WPZT Kamp + KPZT) KPZT 1+ KpzT (3.6) Kamp Equation (3.6) says that the stiffer the amplifying structure is, the higher the efficiency. Therefore, if we concentrate deformation to specific points with low stiffness about the axis of desired deformation, we can make the design highly efficient, allowing for maximum force output 4 . The stiffness of the stucture is a function of how many flexural pivots there are. The 4 Jaenker et al. derive the same result for mechanical efficiency[23]. 29 Figure 3-8: Electrode potential bus powering three actuators in series. Loops are compliant to prevent increased device stiffness. addition of a four-bar linkage increases the stiffness, so a mildly coupling effect is that not only is it dependent on the hinge dimensions, but also the number of hinge. The efficiency of the structure will effect the force transmission ratio. 3.4 Powering an array of actuators with an electrode power bus (FR 4 with DP 4 ) In order to actuate devices in series, some sort of electrode, or power bus is necessary to transmit charge to the piezoelectric. Figure 3-8 shows one possible design in place. The bus connects to the top and bottom electrodes of the actuator. Here it is connecting three actuators in series and is symmetric about each actuator. Any electrode bus designed, cannot be stiffer than the SLFP's, to maintain fuctional indepedence. Therefore, a compliant electrode bus was designed, taking into account photolithography constraints C 2 . The electrode bus is made out of 2000 on top of 200 A A of platinum (bulk elastic modulus ~171 GPa) of titanium (bulk elastic modulus ~116 GPa), deposited by electron-beam evaporation. Because of Ti/Pt is required for making sol-gel PZT, using it as the electrode bus does not add additional fabrication steps. The electrodes have a "robust" line width of 11 /m, and have a compliant "loop" hinge structure to make the bus stiffness less than that SLFP stiffness, while maintaining conductivity integrity. While the complex structure of the 30 loop hinge limits strain concentration, it makes an exact stiffness calculation difficult, so the following very rough, conservative calculation will be made. The equivalent length of this hinge structure in the active range is 120 Itm. This hinge structure has a torsional stiffness of roughly 5, kr For this case 1 = 120[pm, YbulkPt = YI (3.7) 7r-y2--. 171 GPa, -y = 0.852, and is the characteristic radius, and I is the cross sectional area moment of inertia of equation 4.16, where b = 2000 A, and t = 11 pm. This yields a ke of 7.2 x 10-8 N-m/rad. Compare this to the stiffness of the hinges mentioned above, for SU-8 with a 2 /um thick hinge that is 10 ,am long, and we get 1 = 10 /1 m, Y = 4 GPa[13, and where t = 2 pim, and b = 30 [im. This yields a kh of 8x10- 9 N-m/rad, which is an order of magnitude smaller. Admittedly, the ratio ke/kh should be much less than 1 and not greater than 1, as was the case with the original design based around silicon rather than SU-8 (silicon is 40 times stiffer than SU-8). A couple of factors should help of the hinges should be less stiff than calculation makes them out to be. Residual stress in platinum makes the film bend out of plane. This changes the area moment of inertia significantly, since the electrode can bend through the thickness of the film as opposed to the line width, lowering the stiffness by orders of magnitude, as in Figure 3-9. For a proof-of-concept design, this is acceptable, even though stress levels in the platinum/titanium on SiO 2 were not determined. The experimental "floating" nature of the loops provides a significant fabrication challenge that, once achieved, will enable more robust future designs. Functional requirement coupling is intended to be ignorable because the ke/kh ratio. Figure 3-10 shows the effect in reality, from an image captured by an optical microscope. In the end, the design matrix is made as shown in equation (3.8): FR1 X 0 0 0 DP1 FR2 0 X 0 0 DP2 FR3 0 X X 0 DP 0 0 0 X FR4 FR4 ausing the pseudo rigid body model of Howell (eg 5.73)[8]. 31 DP4 De4 (3.8) no stress no curl stressed (curled) Figure 3-9: Curling of platinum electrodes due to residual stress Figure 3-10: Image of a loop on a real released device, bending out of plane due to residual stress 32 Chapter 4 Modeling the device 4.1 Static Analysis: Amplification ratio expectations. Let us perform a static analysis of the symmetry modell: Proceeding with Lagrangian analysis: F = Fni + Fo(ti1 z = -ri cos (- - rl sin 0) 3 (4.1) (4.2) There are four springs, but only two different spring constants, giving the factor of 2 in front. The Langrangian, X,is given by, X=T*-V. (4.3) The potential energy, V,of the system is given by V = 2 [ki ( -_ oi)2 + k2 (0 - 002)2 (4.4) All calculations assume that the amplifier is so stiff in the out of plane direction that bending out of plane can be ignored. Note the coordinate system. 33 and for the static case the kinetic coenergy, T*, is, T* = 0. (4.5) The equations of motion can be determined through, d Of-\ (4.6) 7-'K~J) '9 qj where q is the generalized coordinate, and the generalized force, -j is, N Ef - O (4.7) i=1 For this model, q = 0 and R = Z. Computing the derivatives we get, (4.8) = r1 sin Oi - r cos Oj, so, Fir1 sin 0 - Foutri cos 0, - 809-2- [ki (0- 00 1) + k 2 (0-0 02 )], (4.9) (4.10) Putting it all together we get, Firl sin 0 - Fostri cos 0 = 2 [ki (9- Go1) + k2 (0 - 002)] , ->' Fot = Fi, tan 0 - 2 rl cos 0 [ki (0 - 001) + k2 (0-002)], (4.11) (4.12) Ignoring the structure stiffness, the output force is proportional to the tan 9 of the input force. For small 9 angles, order 1 ', this is about 2%. So Foot is about 2% of Fin after the stiffness of the amplifying mechanism is overcome. Assuming small stiffness,and a PZT input 34 force is order 5 mN , then the output force is then the output force should be about 100 pN which should be satisfactory for a MEMS applications, satisfying FR 2 . This is reasonable for thin film PZT at 10 V, 100 pm wide, and an elastic modulus of 60 GPa, similar to SiO 2 , as in equation (4.13). The piezoelectric force expected from the member is, ignoring the electrode stiffness[18], FPZT = Fin = YPZTd31WV, (4.13) where YPZT is the elastic modulus of PZT, d 31 is the piezoelectric strain coefficient of PZT, W is the width of the member, transverse to the membranes length, and V is the applied voltage. Increasing the width of the PZT member will increase the input force. The arrayability would allow n-actuators to be operate in parallel giving n-times the force output, at a cost of size. If F,, is zero, we can get an equation that relates the stiffness of the structure, Fin 2 = ri sin G [(ki + k2 ) 0 - k 190 1 - k 2 00 2], (4.14) For small length flexural pivots (see Figure 4-1), the torsional spring constant, k, can be approximated as (Howell), YI k= - 1 1 (4.15) and the virtual pivot is at the the halfway point, 1, 2' and Y is the elastic modulus of the pivot material, and I is the area moment of inertia of the cross section, bt 3 I= . 12 (4.16) It is important to note that the use of equation (4.15) is an approximation, of Howell's approximation. Since the design in Figure 3-1 depicts asymmetric notch or circular flexure hinges, the true stiffness of the hinge will be stiffer than equation (4.15) predicts, but the pivot point will be more localized at 1. this proof of concept design. The author uses this relatation with that knowledge for See Lobontiu[12] for a more complete treatment of asymmetric 35 x Z t Figure 4-1: Small length flexural pivot bends primarily in the y-direction when loads are applied with a component in the y-direction circular flexure hinges. The following are the device dimensions: r, = 165 ptm E = 4 GPa (Elastic modulus of SU-8) t b = 2 pm 30 prm L =10 pam A MATLAB script was written to calculate the static deflection values. Using symmetry, the input force equation was multiplied by four, and the displacement magnitudes in the x- and y-directions were multiplied by two to get the full device static displacement. Figures 4-2 and 4-3 show the static mechanics of a design with a 5 respectively. and a 10 initial angle The angular scales on the plots go until the strain limit of PZT is geometrically reached at 0.1% This occurs at a change in x of 0.19 pm since the half length of the active PZT region is 190 pam. Notice that in the d) plots, there is a trend of decreasing amplification ratio with increasing 0, therefore, to maximize amplification, 0 should be as small as possible. Conversely, the input force required decreases with increasing 0. the the 50 plots are much more linear than the 1' plots. with a 5 The devices tested were designed for a safety factor, since residual stresses in the piezoelectric member can affect the initial angle dramatically. for the 5 The last observation is that Minimum amplifcation occurs at the PZT strain limit and is 10.7 design and around 30 for the 1 design, satisfying FR1 . 36 a) Input force versus angle - 00 = 5 degrees b) x and y displacement versus angle - 00 = 5 degrees 4 100 80. .3 60. E2 40- L.L 20 ~1 08 0 0.085 --- ~ 0.085 0.1 0.095 0.09 - 0.09 0 (rad) d) Amplification Ratio versus angle - c) x and y strain versus angle - 00 = 5 degrees 2.5. C 0.095 0.1 0 (rad) 0= 5 degrees 11.6r 2 11 .4 1.5 11.2 1 E 0.5 IU.80r /- 10.61 0.085 0.1 0.095 0.09 0.085 0.09 0 (rad) 0.095 0.1 0 (rad) Figure 4-2: Different plots with an initial angle of 5 . In b) and c), dashed and solid lines are the yand x- direction plots respectively. a) Input force versus angle - 00 = 1 degrees 6 00 b) x and y displacement versus angle - 80 = 1 degrees 12 . 500- 10 1 400 -3 300- E 6 200, A 08 100 0 0.01 4 2 0.02 0.03 0.04 0.05 0z 0 (rad) 0.06 0.01 0.03 0.04 8 (rad) c) x and y strain versus angle - 00 = 1 degrees d) Amplification Ratio versus angle -80 = 1 degrees 8 0.02 0.05 0.06 60 55~ 6 \1 .250 -ii . 45 4 .2 40 E 35 2 30 00.01 0.02 0.03 0.04 0.05 25 0.01 0.06 0 (rad) Figure 4-3: Different plots with an initial angle of and x- direction plots respectively. 10. 37 0.02 0.03 0.04 8 (rad) 0.05 0.06 In b) and c), dashed and solid lines are the y- - 4 3.5 3 E 2.5 E 2 CL 1.5 . 1 0.5 0 C 10 20 30 40 50 60 Force (gN) 70 80 90 Figure 4-4: Displacement versus input force for an initial angle 100 0 = 50. 12 10 8 E 6 E a) CO O, 4 2 n 00 100 200 300 Force (siN) 400 500 Figure 4-5: Displacement versus input force for an initial angle 38 600 o = 10 y r2 r1 k 3 F out Figure 4-6: Dynamic model based on symmetry Figures 4-4 and 4-5 plot the displacement of the end effector versus the required input force under no external load. Notice the linearity of the output for 0o = 50. In equation (4.13), the force generated by the PZT is proportional the voltage applied, and so we can expect that the output displacement should behave like Figures 4-4 and 4-5, with, especially in the case where 0 0 = 50, displacement should be linearly related to applied voltage. Since the exact properties of the thin film PZT (EPZT and d 31 ) used in the design, have yet to be determined experimentally, the conversion is omitted. 4.2 Dynamic Analysis For the dynamic anaylsis, a more complicated model is needed as shown in Figure 4-6. 39 Z1 = 2 = 32 Z3 = -ri cos 0i+(- Zi+ Z2 dz~j dt = dt - d7Z3 2 dti (4.17) r1 sin 0)J 22 2(- 2- - r2 (4.18) rl sin O)j, (4.19) (cos Oi + sin Oj), -(-cos Oi sin (4.20) ), rib sin 0i - rib cos O-j - (4.21) 2ribcosoj, (4.22) 0 (sin Oi- (4.23) cos Oj), + -T0(sin + cos Oj), (4.24) j (4.25) = r, sin Oi- r1 cos = -2r 1 cosoj, (4.26) Adding together the kinetic coenergies due to the linear motion of m 1,m 2 , and M 4 , and the rotary motion of the beams M 3 and m 4 we get, T* = = (mi + M 4) 2 2 (ml + m 4 ) r 2 + m 40 2 +2 (1jb2) +2 (2ri0 Cos 0 2+ 2 ()1 j J1 ) (4.27) where J is the angular moment of inertia of the two rotating beams that comprise m m4, about an end, with m3 3 and . = n4 J=2 m 3 (r2 + w2) (4.28) 31 where rl is the length of the beam and w is the width. The potential energy is twice the static condition (8 springs now), V= 4 k1 (0 -- 001)2 + k2 (0- (4.29) 002)2 1 The generalized force, - (4.30) = Finri sin 0 - 2F..tricos 0, Computing the necessary derivatives for the equations of motion, = d af d (Mi + m4) r O + m 2 b (2r 1 cos 0)2±2 2b = = (Ml OS0 2 (JA) (4.31) *2 + M 4 ) r1 0 + m 20 (2r 1 cos 0) + 2M 2 2 (2r 1 cos 0) (-2r1 sin 0) + 2JA, ~r~M1 + M4 + 2J 2 1 = -4m2r 2 + 4m2 cos 0 r1j -8m 2r cos 0 sin9 sin OcosO - -4 [ki (0 - 0 0 1 ) + k2 (0 - 0 2 (4.32) 02 )], (4.33) we get, ao d (aX) 41 (4.34) (2 J M1 + M4 + 2J+ 4m2 cos 2 0 1 = 2- r 2 - 4m2r cos 0 sin 02 + 4 [k1 (0 - 001) + k2 (0 - 002)] Finr1 sin 0 - 2F 0etri cos 0. (4.35) When actuating individual devices, adding actuators in series, and in parallel, will only add mass terms to the equation. When all actuators are actuated at the same time, this equation of motion should hold. If we linearize the equations of motion about an initial angle 0 o, and say 0o plug in 0 = Oo = 001 = 002, we + e, and get, M1 + m 4 + 2 + 4m 2 cos 2 (Go + e)) r 1 -4m = 2 r, cos (Oo + e) sin (Go + e) 2 4 [ki + k2] e Finr1 sin (0o + e) - 2Ftricos (0o + e) . Using the following identities, and knowing that e (4.36) < 1, + e) = cos Oo cose - sin 0o sin e = cos 0o - e sinGo, (4.37) sin(0+e) = sin00cose+cos0osine =sin00+ecos00 (4.38) cos (Oo Simplifying equation 4.36, term by term, and dropping terms that are second order or greater, m+ + m4 + + M4 + 2+ m1 = M1 + M4 + 2J 2 1 4m 2 (cos 0o- e sin 0o) 4m 2 (COS2 +1m cs - 0 42 r E 9) 2E cos 0 0 sin 0 0 + e 2 sin 20) r -4m 2 ri (cos o - e sin Oo) (sin o + ecos o) 52 = 0 Fir1 sin (0o + e) = Finr1 (sin 0o -2Fostri cos (Co + e) = + e cos Go) -2Foutri (cosoo - esin 0). Combining these simplifications, we get the following linearized equation of motion, Mi1 m4 + + 4m 2 cos 2 o) r 2+ 4 [ki + k2 ] e = Finr1 (sin 0 o + 6 cos 0o) - 2Foutri (cos Oo - e sin Go) . (4.39) Since piezoelectric strain is small, the travel of the actuator is limited, so equation (4.39) should be satisfactory. If the input force and output force are set to zero, we can estimate the amplifiers natural frequency from the homogenous differential equation of equation (4.40) E = 0. 4 [ki + k 2] + M1 + M4 + 2J+ 4m2 cOs 2 G (4.40) r Equation (4.40) yields a natural frequency of: Wn - 2 k + k2 'r Ml+M4 (4.41) + 2J+4M2COS2 00) Since the mass of objects is proportional to the volume cubed, in the MEMS world, natural frequencies of this design can be very high and easily picked by clever hinge design to determine the stiffnesses k, and the link length ri. Given a design such that, p = 2240 kg/ m3 is the desity of cured SU-8 (Microchem). A 1 = (70 x 22 x 2 + 30 x 280 + 55 x 174) x (1 x 10-6)2 = 2.105 x 10-8 m 2 , is the surface area of ml. A 2 = (25 x 95) x (I x 10-6)2 = 2.38 x 10--9 M2 , is the surface area of M 2. A 3 = (141 x 20) x (1 x 10-6)2 = 2.82 x 10-9 M2 , is the surface area of M3- 43 b = 30 x 10-6 m, is the thickness of the SU-8. 0= 5 . Given this data, the natural frequecy of the manufactured amplifier should be on the order of 5 kHz. Since the hinges should be stiffer in reality, as mentioned in the previous section, the natural frequency should be slightly greater than this value. Provided 00 < 1, the natural frequency of the device should be fairly constant over different designs. 4.3 The coupled device dynamics: expectations In the real device, the actuating member is coupled to the real system, in parallel. Therefore, the stiffness of the actuating member will effect the natural frequency. Due to limited data on the residual strain or elastic properties of the platinum, SiO 2 , and PZT itself we can not be sure of a real value, but the derivation will be included here for a full treatment. The potential energy of the system becomes, using equation (2.11): V = 4 [k1 (0 - 001)2 + k1 (0 )2 + 2kr (cos 0 - cos 00)2 (4.42) It is assumed that the member mass is small, so it's effects on the kinetic coenergy are small, but it is possible to lump it together with ml. = -4m 2 sin 9 cos 0 - 4 [k 2 rO 1 (0 - 00) + k 2 (0 - 00)] + 2kLr2(cos 0 - cos Oo) sin 0, (4.43) For the whole equation of motion we get, + 4m2 cos2 ) rO - 4m2r cos 0 sin 0b2 + m1 +m4 + 2 1 +4 [k 1 (0 - Oo1) + k2 (0 - 00)] - 2kLr2 (cos 0 - cos 0) sin 0 = Fi.r 1 sin 0 - 2Foutricos 0. 44 (4.44) Linearizing, the additional term becomes, -2kLr2 (cos 0 - cos O0) sin 0 = -2kir [cos(Oo + e) sin(Oo + e) - cos Oo sin(Oo + e)] = -2ktr [(cos 00 - e sin 00) (sin 00 +e cos 0o) - cos 0o (sin Oo + e cos Oo)] = -2kLr2 (sin = -2kLr| [-e sin 2 001 - e sin 2 0 0o cos 00 (4.45) + e Cos 2 00 - 62 sin 00 cos 00 - cos Oo sin 00 - 6 cos 2 00) (4.46) Combining these simplifications, we get the following linearized equation of motion, (in1 = Fi, 1 + 4m 2 cos2 + m4 + (sin 0 0 r + (4 [k 1 + k2 ] + 2kLrl sin 2 e cos 00) - 2Fouri (cos 0 0 - e sin 00) . (4.47) The stiffness of the actuating member adds an additional term to RHS acting as a moment offset. In spite of this, looking at the homogeneous equation, the device natural frequency is now, on = 4 [k1 + k 2J + 2kLr2 sin 2 0 (m 1 + M4 + 2J + 4m2 cos 2 0( 1 r1 (4.48) If kL >> k 1 or k2 , then the natural frequency becomes, (4.49) = Sin sn 0 Mi1 + m which is independant of r1, assuming r1 4 + 2 + 4m 2 cos (00 > w. Furthermore, if we take 0 < 1 (maximizing amplification) we get, Wn = 00 2kL (mi-n + 7 m4 + 4M2) (4.50) Essentially, the device has been reduced to a spring-mass system. The natural frequency of the system is linearly related to the initial angle, 00. This seems to be indicative of the fact 45 that the larger the angle, the less force the PZT has to exert to move the device. When Oo approaches E, the PZT member is hardly taxed at all to move the amplifyer, if Oo is precisely zero, the model system could not move, due to the increase in force. The actual device natural frequency can be approximated using estimated material properties of PZT and Pt, ignoring the thin layer of titanium. ThePZT member is made up of a stack of SiO2, Ti, Pt, PZT, Ti, and Pt, with the metals serving as electrodes. YPZT ~~60 GPa Ypt 95 GPa Ysi0 tPZT tpt 0.2 pm tsio 2 0.4 pIm WPZT = 130 /m Wpt1 = 140 pam ~ 60 GPa 2 0.2,pm Wsi0 2 = 140 pm WPt2 = 100 Am L = 380 pm Solving for the natural frequency, we get w, = 60kHz, with a member stiffness kL 2.46 x 10 4 . = This is very large and should be noted that this is under ideal axial actuation of the PZT member. The maximum force that the PZT member can generate is limited by the width of the top electrode. Using approximate values for the PZT to get an estimate we get from equation (2.9), and a d 31 = 100 x 101 2 C/N, and a potential of 15V, we get, FPZT = 9000jiN out of the whole membrane Performing the static analysis we can get a relationship between input force and displacement for the 5' design as shown in Figure 4-7. An input force of 9000pIN should actuate the device to the strain limit of the PZT member. 46 3.53E 2.5E 2- CL .m 1.5- 0.50 0 500 1000 1500 2000 2500 3000 Force (MN) 3500 4000 4500 5000 Figure 4-7: Displacement versus input force for an initial angle 6 o 47 = 50. Chapter 5 Fabrication The fabrication was performed using UV lithographic techniques on 100 mm p-type silicon substrates. Quality, size, and thickness of the silicon substrate is not important, other than that the wafer be at least single-sided polished. The silicon is used as a sacrificial layer only, and plays a limited structural role. Recent advancements in MEMS have demonstrated that SU-8 may be used for the development of in-plane compliant mechanisms[9]. Therefore, it is proposed to use SU-8, as opposed to bulk silicon, to obtain a high-aspect-ratio compliant structure. SU-8 is a photo-curable epoxy-based negative resist. Since it requires no etching to pattern to obtain high-aspect-ratio structures as well as demonstrating excellent mechanical properties[13], it is highly desirable to use in a prototype design. Figures 5-1 through 5-5 show the process flow for device fabrication depicting the top view of a device on the left and a cross section of a device on the right. The fabrication process uses four different masks produced by Advanced Reproduction of Andover, MA on chrome on soda lime glass using an e-beam writer. The first step is a deposition of SiO 2 by thermal oxidation of a silicon substrate. In step two, lift-off is achieved in acetone, to disolve the resist in the regions where no electrode is desired. The bottom electrode, electrode bus, and alignment marks are formed in this step (mask #1). coated, dried (pyrolysis), etched, and then annealed. In step three, the PZT is spin The proper perovskite crystal structure is ensured by etching the PZT prior to annealing, leaving PZT only on top of Pt/Ti regions. If PZT is annealed on top of the SiO 2 , regions of poor crystalization will form, causing stress, cracks and other defects in the PZT (mask #2). 48 A 2 [Lm gap is left between one end of Figure 5-1: Begin with growing 2000 A of thermal oxide on a silicon substrate M M: Figure 5-2: Pattern and deposit bottom metal layer using liftoff of e-beam evaporated Ti (200 A) and Pt (2000 A) the bottom electrode and the bus, to allow the top electrode to connect to the bus and limit PZT exposure to the SiO 2 . Step four is the same as step two, forming the over lapping (top) electrode of the PZT member (mask #3). The SU-8 deposition occurs in step 5. The SU- 8 is spin coated onto the wafer, and carefully dried using slow ramping speeds to minimize residual stress in the SU-8. The device is released, first by etching away exposed thermal oxide with CF 4 using a short RIE to expose the silicon substrate, followed by an isotropic xenon diflouride (XeF 2 ) etch to remove silicon underneath the device. The etch rate for our particular XeF 2 etcher is roughly 10 pm/min. This all "dry" release is particularly desirable, because it avoids problems associated with wet releases (stiction, etc.). and specific process flows. See the appendix A for detailed The oxide left under the PZT member shifts the neutral axis and will inevitably cause bending of the PZT member. The oxide is left to maintain fabrication simplicity. Figure 5-6 is a model of the finished design as it should appear, minus the transperency of 49 no Igo Cl:40 BOE (buffered oxide etchant). Anneal at Figure 5-3: Spin coat PZT. Dry. Etch in 400 650'C. See appendix Figure 5-4: Pattern and deposit top metal layer using liftoff of e-beam evaporated Ti (200 A) and Pt (2000 A). Figure 5-5: Spin on SU-8, photo-pattern and bake. Release the device by RIE (CF 4 ) of oxide and XeF 2 etch of silicon using SU-8, Pt, and PZT as etch masks. 50 620 microns I.5mm 670 microns Figure 5-6: Solid model of finished actuator. SU-8. The exposed square areas on the left are bond pad areas such that the device can be wire bonded or actuated by probe tips. Prior to releasing, the device appears as in Figure 5-7. For this particular actuator, notice the misalignment of the PZT from the top electrode. This is caused by the difficulties in aligning the chrome mask to the wafer alignment marks because the PZT dries dark. Notice the transparency of SU-8. Figure 5-8 shows an SEM image of a released device. The out of plane bending of the device and upwards curling the electrode bus can be attributed to the fact that SU-8 is non-conducting and the device is not grounded, allowing charge to build up. Devices were observed to fail in 2 the SEM chamber due to this effect. Figure 5-9 shows two 1 cm dies connected with finished actuators. 51 Figure 5-7: Unrealeased actuator. Notice misalignment of the PZT. This particular device was not tested due to the misalignment because of potential leakage problems. Figure 5-8: SEM image of device. Out of plane deflection due to the fact that the device is not grounded. 52 Figure 5-9: Two dies connect. Each die is 1 cm 2 53 Chapter 6 Results and Discussion 6.1 Quality of PZT In order to ensure that the devices work, a verification of the PZT's polarization was performed prior to actuation measurements. The devices were tested using a probe station to determine the unloaded displacement of the device, and the hysteresis curve of the piezoelectric. The hysteresis curve was measured using an RT66A standardized ferroelectric test system from Radiant Technologies, Inc. of Albuquerque, New Mexico, USA., connected to a PC running Radiant Technologies CHARGE program. Force output was not tested due to time constraints. The result in Figure 6-1 compares favorably with literature[20] with a maximum polarization of ~50 pC/cm 2 , for 0.4 pm thick film at 15V with an area of 11.4x10- 4 cm 2 . The leakage current is 2.58x10- 6 A at a resistivity of 1.65x10 8 Ohm-cm, both are within acceptable tolerances. The resistivity is two orders of magnitude lower than desired, but is still high such that little current was drawn. More care during fabrication needs to be maintained to ensure lower leakage. Other process runs demonstrated higher resistivity, so this is an achievable goal. Figure 6-2 shows strong perovskite phases in the XRD. Only perovskite PZT phases peaks are visible, other than a strong platinum peak. The pyrochlore phase, visible around 290 and 340 if present,is not detectable within the instrument resolution. 54 60Cm 40*,01iIOW4 E 0 0 N -15 -20 -10 5 -0 **-20 - 155 10 2 20 .5 IL -60 J Potential (V) Figure 6-1: PZT hysteresis of a 0.4 pm thick film at 15V PZT/Pt/Ti/SiO,/Si annealed at 650 0 C for 30 m in. 500U - 4000 - 3000 - N CD CD C%4 U, a) 2000 4 -A - aC 1000 - 020 30 40 60 2E Figure 6-2: X-Ray diffraction crystallography of the PZT. 55 60 mum mrn~u - - - Figure 6-3: Side-by-side comparison of the end effector displacement at OV (left) and 14V (right). White lines indicate location. 0 = 5 . Shows a displacement of 6 /Lm. 6.2 Actuation Test The device tested had an initial design dimensions of an angle of 5 on a built-in scale with an 8 pm period, consisting of three actuators in series to make optical recoding of measurements easier. The images were recorded and analyzed in imaging software to measure displacements. The low accuracy of the measurements on the captured images occurs due to focusing limitations of the optical microscope used, and the scale period. Because of this, limited data points (0,5,10, and 14 V) were collected, at an estimated accuracy of +1 pm. Extra data would not provide a significant infromation suing this technique. Figure 6-3 shows the device displacement comparison in a side-by-side manner at the field limit of actuation. While preliminary results are encouraging, clearly, a more precise method of measurement is needed, such as a computermicro-vision system. Figure 6-4 shows the actuator maximum displacement at ~2 ptm/actuator at 14 V, while drawing no current. The analysis used to generate Figure 4-4b is based on geometric analysis and is independent of device material properties. Therefore, if the dynamics of the actuator 56 8 E 2-- - 1- 0* 0 10 5 15 Potential (V) Figure 6-4: Displacement versus voltage of the PZT end effector, for three actuators in series. are behaving as expected, Figures 4-4b and d can be a benchmark. This corresponds to an amplification ratio of ~11 per actuator, if the PZT member has contracted of ~0.18 pim, as shown in Figure 4-4d. However, because the constriction of the PZT member was immeasurble with resources available, it is unclear what the true amplification is. This compares unfavorably (50%) with the estimate of Figure 4-7. The critical factors that influence this discrepancy are out of plane motion (caused by moments induced by the off-neutral axis PZT member), electrodes being too stiff (system dynamics changed), poor PZT quality (d 31 not what was expected), and leakage current between the top and bottom electrodes. Dielectric breakdown occured at around 15V across the 0.4 pm thick PZT film, which corresponds to an electric field of 37.5 V/ pm, similar to the expected value of 40 V/ pm. 57 Chapter 7 Conclusion and Future Work 7.1 Conclusion An in-plane piezoelectric micro-actuator was designed and fabricated. The hybrid actuator demonstrated an amplification ratio estimated to be in excess of 10:1. Also demonstrated was the ability of the actuator to be fabricated in arrays of microactuators, in series, or in parallel, by means of an electrode, or power, bus. New fabrication techniques for PZT were developed, including the patterning of the sol-gel film prior to annealing, and the release of a piezolectric actuator using XeF 2 . A foundation has now been established for the development of devices which use this actuator, and compliant devices using SU-8. 7.2 Future Work To analyze the current design, foremost, more accurate measurements of device dynamics need to be done in order to verify the actuation mode. to be evaluated for a rigorous design treatment. Next, material properties, (like d 31 ) need Device resistivity, while acceptable, is two orders of magnitude larger than desired currently, so increased care needs to be maintained when fabricating the PZT future iterations to improve efficiency, allowing for fields on the order of 100V/ pm. The electrode bus, proven to be fabricable, should be redesigned less conservatively in order to further approach ideal device mechanics. To increase lateral displacement, and out of plane bending, the actuating member could be 58 b) Figure 7-1: Membrane endpoint effects further uncoupled from the amplifiying mechanism. Figure 7-1 shows the effects of different end point conditions connecting the member, represented as a beam, to the amplifying mechanism. Figure 7-1 a) shows the current design with the endpoints fixed to the amplifiyng mechanism. Any out of plane bending of the member gets coupled into the the amplifying mechanism, whereas in b), the member is connected by ideal pivots (in reality, they would be flexural pivots). The moments acting on the amplifying mechanism are decoupled, and only the forces generated by the member would act on the amplifying mechanism. Fully decoupling the member is in the true spirit of the original design, however for the proof of concept stage, this was not attempted. In this way, the PZT member can be designed as a multi-morph, rather that as a pure contractor, to increase device displacement. Second, the development of a true electrode bus, such that individual actuators can be addressed in an array of actuators would be desirable, for fully digital/analog control over a membrane. Serious wiring challenges exist, so perhaps a solution similar to the macro-scale BRAID[19] could be accomplished, such that a "decoder" existed on each device to switch the signal on and off, with the power bus doubling as a communication bus. Lastly, a single-crystal silicon, rather than SU-8, based amplifiying mechanism was conceived and may be desirable for silicon IC material properties. Therefore, it would be important to show that this design can be implemented with different materials. Vast arrays of the actuators can be mechanical membranes, as a precursor to mechanical materials. The actuator can be applied to different applications, including, low power RF switching (see Figure 7-2, early prototype), bio-manipulation, micro-manipulation, and possibly 59 "="g3ft , iamgfi Figure 7-2: An actuated bi-stable beam. Figure 7-3: A two-axis manipulator for nano-metrology and manufacturing (see Figure 7-3, early prototype). Virtually any low and voltage power solution for MEMS can be accomplished, with great response characteristics. Inverting the design, it can be used as a de-amplfying mechanism (gain less than 1) to enable greater control for sub-nanometer alignment. 60 Bibliography [1] S.E park and T.R Shrout, "Characteristics of Relaxor-Based Piezoelectric Single Crystals for Ultrasonic Transducers," IEEE Trans. Ultrasonics, Ferroelectrics, and Frequency Control, Vol.44, No.5, 1997, pp. 1140-1147. [2] J Garcia-Bonito, M J Brennan, S J Elliott, A David and R J Pinnington, "A novel highdisplacement piezoelectric actuator for active vibration control," Smart Mater. 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[21] Kazunari Maki, Nobuyuki Soyama, Satoru Mori, Kensuke Kageyama, Masaya Matsuura, and Katsumi Ogi, "Microstructures of Sol-Gel Derived PZT Thin Films," Proceedings 9th US-Japan Seminar on Dielectric and Piezoelectric Ceramics, 1999, pp 203-206. [22] Don Berlincourt, Ultrasonic transducer materials. Edited by 0. E. Mattiat. Contributors: Don Belincourt, [i.e. Berlincourt] Yoshimitsu Kikuchi [and] A. H. Meitzler. New York, Plenum Press, 1971, p 64,68. [23] Peter Janker, Frank Hermle, Thomas Lorkowski, Stefan Storm, and Marc Wettemann, "Development of High Performing Piezoelectric Actuators for Transport Systems," Ac- tuator 98: 6th International Conference on New Actuators, 17-19 June 1998, Bremen, Germany, pp 181-185. [24] Stephen D. Senturia. Microsystem Design. Kluwer Academic Publishers, Boston, 2001. pp 570-571. [25] S. G. Kim (2) and M. K. Koo. 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Head Island, South Carolina, June 2-6, 2002, pp 50-53. 63 Hilton Appendix A Process Details Table A.1: Metalization process step process Resist 1 2 Prebake description HMDS first Image reverse resist AZ 5214E Dispense speed to 500 rpm 6 sec Spread speed to 750 rpm 6 sec Spin speed 4500 rpm for 30 sec 30 -mm at 90'C in an oven EV1 365-450 nm wavelength at 10 mW/cm2 Exposure total of 1.4 sec 3 4 5 6 Post exposure bake 30 min at 90'C in an oven. Be Flood expose 2 EV1 365-450 nm wavelength at 10 mW/cm Exposure total of 45 sec Develop Developer AZ 422 80 - 90 seconds sure not to bake too long. Electron-Beam Evaporator a dTemescal Semiconductor Products Metal deposition 200 titanium followed by 2000 of platinum at a deposition rate of 1 A/sec. Lift off 8 methanol --+ 2Achieved in acetone -> propanol Dry with nitrogen. Use ultrasound for small features, and change acetone regularly to prevent metal particle adhesion. If particles accumulate, ultrasound in 2-propanol to get rid of them. 64 Table A.2: Fabrication of thick PZT film. Courtesy of Dr. Yong-Bae Jeon and Nicholas Conway For a 1 ,am thick maximum PZT film on platinum 2000 A on 2000 A silicon oxide. [step process PT sol-gel spin [description Mitsubishi Materials Co. 1 coating PT (PbTiO3 ) Sol-gel, 3000 rpm 2 Pyrolysis yStep Heat to 380'C for 1 min on a hot plate down 1 minute at 200'C, 1 minute 80'C PZT 3 sol-gel spin coating PZT sol-gel (F2), 2000 rpm. Pyrolysis Heat to 80'C for 1 min on a hot plate Then 380*C for 5 min on a hot plate Step down 1 minute at 200'C, 1 minute 80'C Go to step 3 n-times Get 0.2 pm per coat when annealed Allow wafer to cool between coats. 4 5 Mitsubishi Materials Co. HMDS first Thick resist AZ 4620 6 Resist 7 Prebake Static dispense for 9 sec -> 1500 rpm 9 sec -- 3500 rpm 60 sec -> 5000 rpm 10 sec. 90"C in oven for 30 min. Exposure EV1 365-450 nm wavelength at 10 mW/cm2 Exposure total of 45 sec at intervals of 15 see with 15 sec wait. 9 Develop Developer AZ 440 for 4 minutes 10 Postbake 90"C in oven for 60 min 8 Etch in 100 HCl (17%):20 BOE (4%): 400 DI Wet 11 etching unannealed PZT Strip 2 resist 12 Annealing 13 of water (77%) for less than 10 sec. Etching is visibly instantaneous. Spray with DI water immediately after etch. Achieved in acetone -+ methanol - 2-propanol, Dry with nitrogen. Ramp up wafer on custom stainless steel heat source on a hot plate at 380'C. Move entire wafer on heat sink into box furnace in air at 650'C for 20 min. The heat source is a 1/16in thick and 5inX5in piece of stock stainless steel with a 100mm wafer recess machined into it. The low thermal conductivity of steel makes it act like a heat source, preventing excessive thermal shock when moving wafer from the hot plate to the box furnace. 65 -wafer seat stainless steel plate Figure A-1: Wafer sink schematic Table A.3: SU-8 50 process step process Spin coating description MicroChem Corp.SU-8 50 Negative Photoresist Pour fast from bottle onto wafer. 500 rpm 5 sec --+ 5000 rpm 30 sec 1 Yields 30 pm thick resist. 2 Single hot plate:20 min at 65'C Ramp to 95*C for 5 min Allow to cool on hot plate slowly Prebake 3 Exposure Post exposure bake 4 EV1 365 -450 nm wavelength at 10 mW/cm' sec Exposure total of 25 sec at intervals of 5 wait. with 15 sec Hot plate: 65'C for 1 min Ramp to 95'C for 4 min Ramp to 105*C for 1 hour Allow to cool on hot plate slowly MicroChem Corp SU-8 Developer PGMEA 5 5 min. Rinse with 2-propanol, and dry with nitrogen 6 Slowly ramp to 105+'C, bake for 30-60 min. Cool slowly on hot plate. Gets rid of excess solvent and hardens. Develop Hard bake 66 Other notes: The oxide etch is accomplished with a PECVD/RIE machine: PlasmaQuest The XeF 2 release etch is accomplished with MEMS Solution ES-2000XM manufactured by SETech. 67 Appendix B MATLAB Scripts % Script for calculating static displacement of the actuator clear all; close all; %Calculation of PZT Force Based on Device dimensions %%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% W = 100e-6; % Active region 100 microns wide d31 = 100e-12; E_PZT = 60e9; V = 10; % Piezoelectric strain coefficient (C/N) approx. % Youngs modulus of PZT, between 10 and 90. % 10 volts - actuation volatage Membranelength = (380e-6/2) % half length of piezoelectric membrane F_PZT = V*EPZT*d31*W; disp(['The PZT membrane maximum force is ' num2str(F.PZT/1e-6) %%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% E = 4e9; % 4 GPa stiffness of SU-8 I = (30e-6)*(2e-6)^3/12; Li = 10e-6; L2 = 10e-6; k1 = E*I/L1; k2 = E*I/L2; ri = 165e-6; r2 = 20e-6; %%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% 68 ' micro-Newtons']) %%%%%%%%%%%%%%%%% For an initial angle of 5 degrees Fin2 = 0; theta02 = 5*pi/180; % 5 degrees theta = theta02:.001:pi/4; for i = 1:length(theta); Fin2(i) = 4*2/r1/sin(theta(i))*((kl+k2)*theta(i)-kl*theta02-k2*theta02); % Factor of 4 because of four quadrants of symmetry F_out2(i) = FPZT*tan(theta(i))-4*2/r1/cos(theta(i))*((kl+k2)*theta(i) -kl*theta02-k2*thetaO2); end deltay = r1*(sin(theta)-sin(theta02)); deltax = abs(rl*(cos(theta)-cos(theta02))); % Find the maximum strain of the PZT based on the geometry xO = rl*cos(theta02); yO = r2+rl*sin(thetaO2)+W/2; xmax = 0.001*Membranelength; % 0.1 % strain i = find(deltax < xmax); i = max(i); % get the index of the max strain /. Plot the input force required as a function of theta %%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% subplot (221) plot(theta(1:i),Fin2(1:i)/1e-6) title('a) Input force versus angle - \theta_0 = 5 degrees') xlabel('\theta (rad)') ylabel('F-i-n (\muN)') % Plot the the relative displacements as a function of theta %figure subplot(222) 7 Factor of two b/c of half symmetry (both sides move); plot(theta(1:i),2*deltay(1:i)/e-6, '--',theta(1:i),2*deltax(1:i)/le-6); 69 title('b) x and y displacement versus angle - \theta_0 = 5 degrees') xlabel('\theta (rad)') ylabel('Displacement (\mum)') % Plot the the relative strain as a function of theta %figure subplot(223) plot(theta(1:i),100*deltay(1:i)/yO,'--',theta(1:i),100*deltax(1:i)/x); title('c) x and y strain versus angle - \theta_0 = 5 degrees') xlabel('\theta (rad)') ylabel('% Strain') % Plot the Amplification ratio as a function of theta %figure subplot(224) plot(theta(1:i), deltay(1:i)./abs(deltax(1:i))); title('d) Amplification Ratio versus angle - \theta0 = 5 degrees') xlabel('\theta (rad)') ylabel('Amplification Ratio') figure 0/V = FPZT/(EPZT*d31*W); plot(Fin2(1:i)/1e-6, 2*deltay(1:i)/1e-6); %title('Displacement versus Input Voltage - \theta_0 = 5 degrees') xlabel('Force (\muN)') ylabel('Displacement (\mum)') %%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% %%%%%%%%%%/%%%%%% For an initial angle of 1 degree Fin = 0; theta01 = 1*pi/180; % 1 degree theta = theta0l:.001:pi/4; for i = 1:length(theta); Fin(i) = 4*2/r1/sin(theta(i))*((k+k2)*theta(i)-k1*thetaOl-k2*thetaO1); 70 % Factor of 4 because of four quadrants of symmetry (4 times the stiffness) F_out(i) = FPZT*tan(theta(i))-4*2/rl/cos(theta(i))*((kl+k2)*theta(i) -k1*thetaO1-k2*theta01); end deltay = r1*(sin(theta)-sin(theta01)); deltax = abs(rl*(cos(theta)-cos(theta0l))); % Find the maximum strain of the PZT based on the geometry xO = rl*cos(theta0l); yO = r2+rl*sin(theta0l)+W/2; xmax = 0.001*Membranelength; i = find(deltax < xmax); i = max(i); % get the index of the max strain % Plot the input force required as a function of theta %%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%%% figure subplot(221) plot(theta(1:i),Fin(1:i)/1e-6) title('a) Input force versus angle - \theta_0 = 1 degrees') xlabel('\theta (rad)') ylabel('FJi-n (\muN)') % Plot the the relative displacements as a function of theta %figure subplot(222) % Factor of two b/c of half symmetry (both sides move); plot(theta(1:i),2*deltay(1:i)/le-6,'--',theta(1:i),2*deltax(1:i)/le-6); title('b) x and y displacement versus angle - \theta_0 = 1 degrees') xlabel('\theta (rad)') ylabel('Displacement (\mum)') % Plot the the relative strain as a function of theta figure 71 subplot(223) plot(theta(1:i),100*deltay(1:i)/yO,'--',theta(1:i),100*deltax(1:i)/x); title('c) x and y strain versus angle - \theta_0 = 1 degrees') xlabel('\theta (rad)') ylabel('% Strain') % Plot the Amplification ratio as a function of theta %figure subplot(224) plot(theta(1:i), deltay(1:i)./abs(deltax(1:i))); title('d) Amplification Ratio versus angle - \theta_0 = 1 degrees') xlabel('\theta (rad)') ylabel('Amplification Ratio') figure plot(theta(1:i),F-out(1:i)/1e-6) title('Output force versus angle - \theta_0 = 1 degrees') xlabel('\theta (rad)') ylabel('F-o-u-t (\muN)') figure %V = FPZT/(EPZT*d31*W); plot(Fin(1:i)/le-6, 2*deltay(1:i)/ie-6); %title('Displacement versus Input Force - \theta_0 = 1 degrees') xlabel('Force (\muN)') ylabel('Displacement (\mum)') rhoSU8 = 2239; %density of SU-8 kg/m^3 ml = rhoSU8*(70*22*2+30*280+55*174)*30*(le-6)^3; m2 = rhoSU8*(25*95)*30*(le-6)~3; m3 = rhoSU8*(141*20)*30*(1e-6)^3; J = m3*((141e-6)^2+(20e-6)^2)/3 % natural frequency in Hertz wn = 1/rl*sqrt(8*kl/(ml +m3+ J/r1^2+4*m2*(cos(theta02))^2))/(2*pi) 72 Appendix C Miscellaneous The following table shows many types of actuators and their assosiated work per volume performance.4 73 Table C.1: Work Per Unit Volume for Various Microactuators. From P. Krulevitch, A.P. Lee, P.B. Ramsey, J.C. Trevino, J. Hamilton, and M. A. Northrup, "Thin Film Shape Memory Alloy Microactuators," JMEMS Vol. 5, No. 4. 1996 pp 270-282. Actuator Type W/v (J/m 3 ) Equation Comments [ 1. Ni-Ti SMA 2.5x10 7 0- - 6.0x10 6 o- - e max, one-time _-=500MPa, thousands 4.7x10 6 2k e=5% of _a=300MPa, 2 Solid-Liquid Phase Change output: cycles: e=5% k=bulk modulus = 2.2 GPa (H 2 0) 8% volume change (acetamide) 3. Thermopneumatic 1.2x10 6 4. 4.6x10 5 Thermal measured values: F=20 N, 6=50 pam, v =4mm x 4 mm x 50 pm 3 (E E+f (Ao) - AT) 2 Expansion 5. Electromagnetic ideal, 4.0x10 5 F F 2.8x104P 1.6x10 3 1.8x10 5 V F-6 F 8. Muscle C 2 eV4A ideal: V = 100 volts, 6=gap=0.5 /pLm 7.0x10 2 Piezoelec- silicon, measured values, variable reluctance: F= 0.28 mN, 3=250 ptm,v=100x100x250 pm3 measured values, external field: Torque = 0.185 nN-m, v= 400x40x7 ptm 3 3.4x10 3 7. tric on ideal, variable reluctance: v=total gap volume, M,=1V- = sec/m 6. Electrostatic nickel s=substrate, f=filmAT=200 V 1.2x10 5 (d 3 3E): Ef 1.8x10 2 (d 33 E)2 Ef 1.8x104 (- - e) measured values, comb drive: F=0.2mN (60 Volts), v=2x20x3000 Lm 3 (total gap), 6=2 pm measured values, itegrated force array: v=device volume, 120 volts calculated, PZT, Ef=60GPa (bulk), d3 3 =500 (bulk), E=40kV/cm calculated, ZnO, Ef=160GPa (bulk), d3 3 =12 (bulk), E=40kV/cm measured values: o-=350MPa, 6=10% 9 Microbubble 3.4x10 2 measured values: bubble diam.=71 [Lm,F=0.9/pN,6=71 [Lm 74