TM
Ultralab Systems
and
Ultrareservoir Containers
TM
Operating Instructions
840012A
Table of Contents
Diagram: Ultrareservoir™ Container Plumbing Assembly
3
1.0
Introduction
4
2.0
Ultralab™ System Description
2.1 Ultrareservoir Container Description
2.2 Ultrapump™ II Description
4
4
4
3.0
Ultralab System Components
4
4.0
Ultrapump II Setup
4.1 Tubing Addition/Replacement
5
5
5.0
Ultrareservoir Setup
5.1 Equipment Required
5.2 Suggested Connection of Ultrareservoir and
Tangential Flow Filtration Device
6
6
6
6.0
Operation of Ultralab System
6.1 Preparation for Start Up
6.2 Rinsing and Preconditioning
6.3 Sample Filtration
6.4 Concentrate Recovery
6.5 Diafiltration Procedure
8
8
8
9
10
10
7.0
Ultrareservoir Shutdown
7.1 Rinsing Procedure
7.2 Cleaning Procedure
7.3 Storage
7.4 Pump and Pump Tubing Care
11
11
12
12
12
8.0
Ultralab Chemical Compatibility
13
9.0
Ultralab System Specifications
9.1 Ultrareservoir Container Specifications
9.2 Ultrapump II Specifications
9.3 Pump Tubing Specifications
14
14
14
14
10.0 Appendix
10.1 Additional Literature
10.2 Ordering Information
10.3 Warranty
15
15
15
17
2
ITEM
1
2
3
4
5
6
7
ULTRALAB™ COMPONENTS
DESCRIPTION
1/8 NPT x 1/4 INCH BARB
1/8 NPT x 5/32 INCH BARB
1/8 FNPT POLYPROPYLENE VALVE
1/8 MNPT NIPPLE
1/8 FNPT POLYPROPYLENE TEE
WIKA 131.11 60 PSI GAUGE
1/8 FNPT 3 -WAY POLYPROPYLENE VALVE
ULTRALAB MANIFOLD 500 mL
2L
5L
QTY
5
5
2
7
1
1
1
1
UltrareservoirTM Container Plumbing Assembly
These components are shipped unassembled to reduce any potential damage during shipment.
3
1.0
Introduction
Ultralab™ System 500 mL, 2 L, and 5 L are specialized reservoir and pump
systems designed to simplify processing of laboratory and pilot scale sample
volumes when using Pall Life Sciences tangential flow filtration devices (TFF).
These products eliminate the need for numerous, cumbersome sample vessels,
connectors, and manual sample transfer steps during concentration,
fractionation, solvent, and buffer exchange operations.
2.0
Ultralab System Description
2.1 Ultrareservoir™ Container Description
The Ultrareservoir containers are constructed of clear acrylic and have
connections in the base plate for simple and convenient hookup to the TFF
filtration device and pump. The polypropylene valves and barb connectors can
isolate the reservoir from either the pump or the device. This allows for quick
changes of pump tubing or replacement of filtration device. A pressure gauge
monitors feed pressure, thereby maintaining control during operation. The
airtight lid creates a siphon for unattended buffer exchange during constant
volume diafiltration.
2.2 Ultrapump™ II Description
Ultrapump II laboratory peristaltic pumps provide controlled recirculating flow
across the membrane surface. The pump features a quick-access pump head
that permits fast and easy tubing replacement. Its self-priming, positivedisplacement operation minimizes sample foaming. A variable speed controller
regulates how much fluid can be pumped by the unit allowing for precise
adjustment of operating conditions during sample processing. An Ultrapump II
pump is also useful for typical liquid transfer operations.
3.0
Ultralab System Components
1 – Ultrareservoir Container
1 - Package with Ultrareservoir components
(refer to Ultrareservoir Container Plumbing Assembly diagram on page 3)
1 - Ultrapump II peristaltic pump
1 - Quick Load* pump head
1 – Ultrasette™ Accessory Kit
(Ultralab Systems with 500 mL Ultrareservoir Containers, include the
Mini-Ultrasette™ Accessory Kit)
NOTE: Use Teflon* tape or PTFE tape on all fittings with threaded parts to ensure proper
seal and prevent leakage.
4
4.0
Ultrapump™ II Setup
4.1 Tubing Addition/Replacement
Pump
Head
Body
Latch
Pump Head
Body
Tubing Retainer
Rotor Assembly
Latch
Latch
Rotor Assembly
Tubing Retainer
Fluted Knob
Figure 1
Fluted
Knob
Figure 2
4.1.1 Attach pump head onto the pump by following the directions that are
supplied inside the box with the pump head.
4.1.2 Unscrew the fluted knob on upper part of the pump head and lift out tubing
retainer. Pull down on the latch on the underside of the pump head until it
snaps open (Figure 1). Swing open the two halves of the pump head as
far as they will go.
4.1.3 Cut approximately 2 ft (0.6 m) of PharMed* thick wall tubing, or
appropriate length of tubing to fit connection desired, and loop the tubing
around the roller on rotor assembly (Figure 2).
CAUTION:
Carefully center tubing on roller of rotor assembly. If not centered
and tubing touches front edge of rotor assembly, wear will be more
severe.
4.1.4 While gently pulling up on the tubing, swing down the two halves of the
pump head and snap the latch into place (Figure 2).
NOTE: To minimize hold-up volume, use the shortest length of tubing possible for operation.
4.1.5 Replace the tubing retainer with the "V" slots facing the tubing and screw
on the fluted knob. Tighten only until the tubing is held firmly in place —
overtightening will restrict flow.
CAUTION: Pall Life Sciences recommends PharMed* or Marprene II* Highperformance tubing for 10-40 psig applications and extended tubing
life. Silicone-type pump tubing should not be used for extended
operation or at pressures greater than 10 psig because tubing may
break.
5
5.0
Ultrareservoir™ Container Setup
5.1 Equipment Required
5.1.1
Vessel to collect filtrate
5.1.2
Vessel to collect final concentrate
5.1.3
Vessel containing diafiltrate solution (if performed)
5.1.4
Vessel containing cleaning solution (see page 11)
5.2 Suggested Connection of Ultrareservoir Container and Tangential Flow
Filtration Device
From Device
Back Pressure
Valve
3-Way Valve
To Pump
From Pump
To Device
Filtrate
Collection
Vessel
Figure 3
5.2.1 Connect the 3-way/Back Pressure Valve assembly to the “From
Device” port on the reservoir. Screw in assembly just enough to ensure
a tight fit. (Refer to Ultrareservoir™ Container Plumbing Assembly
Diagram on page 3.)
CAUTION:
Do not apply excessive force to valve assembly after insertion into
reservoir, as fracture may occur. It is recommended that the valve
assembly always be supported with one hand when opening or closing
the 3-way valve.
5.2.2 Place reservoir on top of pump as shown in Figure 3, or on the
benchtop next to pump as shown in Figure 4.
5.2.3 When facing the pump, take the tubing that extends from the left side
of the pump head and connect it to the “To Pump” barb connector.
Secure the tubing on the barb connector with a tubing clamp.
6
From Device
3-way Valve/Back
Pressure
Assembly
Gauge
Assembly
To Pump
From Pump
To Device
Filtrate from
TFF Device
Figure 4
5.2.4 Take tubing that extends from the right side of the pump head and connect
to the “From Pump” barb connector. Secure the tubing on the barb
connector with a tubing clamp.
5.2.5 Insert the polypropylene tee with gauge assembly to the “To Device” port
on the reservoir. Screw in assembly just enough to ensure a tight fit. (Refer
to Ultrareservoir™ Container Plumbing Assembly diagram on page 3.)
5.2.6 Cut two pieces of PharMed* tubing the appropriate length, attach the
Gauge Assembly and the 3-way/Back Pressure Valve Assembly to the TFF
device. Secure the tubing on each hose barb connector with tubing clamps.
NOTE: To minimize hold-up volume, use the shortest length of tubing possible for operation.
5.2.7 Connect the tubing extending from the Gauge Assembly to the FEED port
of the TFF device (Ultrasette shown in Figure 3 and 4) and the tubing
extending from the 3-way/Back Pressure Valve Assembly to the Retentate
port of the filtration device. Secure with tubing clamps.
5.2.8 Check that both anti-vortexing plugs are seated properly in the bottom of
the reservoir. The open ends of each plug should be parallel to the walls of
the reservoir so that flow is diverted equally in both directions. This will
ensure proper sample exit and return with minimal shear and foaming.
5.2.9 Connect tubing (3/16" I.D.) to the barb fitting on the 3-way valve (which can
be used to collect final concentrate or to direct flush volumes to drain). The
length should be adequate to reach either a drain or another collection
vessel. See Figure 5 on next page.
7
Beaker for final
concentrate or
drainage of flush
volume
3-Way Valve
(positioned for retentate
collection and closed for
recirculation)
Back Pressure Valve
(closed position shown will
not allow for recirculation)
Figure 5
6.0
Operation of Ultralab™ System
6.1 Preparation for Start Up
6.1.1 Plug the line cord of the pump into any grounded, three-wire AC
receptacle making sure speed dial is at zero and the forward/reverse
switch is in the "Off" position. "Forward" position is with the switch
pushed to the right; "Reverse" position is with the switch pushed to the
left; "Off" is between these two positions.
6.1.2 Turn the 3-way Valve and Back Pressure Valve on the reservoir to
allow fluid to recirculate into the reservoir. The recirculation position of
these valves is when the valve stem is parallel to the valve body. Be
aware of the correct position of these valves for retentate recirculation.
6.1.3 Now, position the 3-way Valve as shown in figure 5, so fluid will not
drain from the Ultrareservoir Container when the rinsing or
preconditioning solution is added. (Figure 5 shows the 3-way Valve in
the retentate collection mode, and the Back Pressure Valve in the
closed position.)
6.2 Rinsing and Preconditioning
Follow the rinsing steps below before filtering sample through a new
membrane filtration device or one that has been stored in a storage agent
(0.1 N NaOH). If your sample contains buffer, preconditioning of the
membrane filtration device must be performed (see step 11 of this section).
6.2.1 Using Table 1 below as a reference, fill reservoir with appropriate
volume of deionized (DI) water.
Volume of Deionized Water/Buffer Required
500 mL
2 Liter
5 Liter
Ultrareservoir™ Ultrareservoir Ultrareservoir
Container
Container
Container
Ultrasette™
200 mL
500 mL
1000 mL
Lab
Tangential
Flow Device
Table 1
6.2.2 Flip the forward/reverse switch into the "Forward" position and slowly
turn the speed dial clockwise until the setting corresponds to the
required recirculation rate. See Table 2 on next page.
8
6.2.3
Filter Unit
Channel Type
Pump Recirculation Rates*
Pump
Tubing
*Recirculation Rate
Ultrasette™ Screen
Ultrapump™
1/4" I.D. (#24)
1.0-2.0 Liter/min
Ultrasette
Ultrapump
1/4" I.D. (#24)
1.5-2.5 Liter/min
Suspended Screen
* Recirculation rates apply to PharMed® tubing only
Table 2
6.2.3 Slowly turn the Back Pressure Valve toward the closed position until the
pressure gauge reads 20-35 psi. This will generate filtrate flow rate.
6.2.4 Direct filtrate to drain until 50% of added volume passes through filtrate.
6.2.5 Turn speed dial setting to "0".
6.2.6 Open the Back Pressure Valve and position the 3-way Valve to recirculation
mode.
6.2.7 Turn the pump on and adjust to a very low recirculation rate.
6.2.8 Discard the Dl water that will exit the Sample Port.
6.2.9 Turn the speed dial setting back to "0", position the 3-way Valve in the
recirculation mode, and the Dl water remaining will flow into the reservoir.
6.2.10 Repeat steps (6.2.5 – 6.2.8) above for maximum Dl water removal.
6.2.11 If buffered samples are to be processed, repeat steps 6.2.1 – 6.2.10
above using buffer. This will precondition the Ultralab™ system to the
proper pH and ionic conditions prior to sample filtration.
6.3 Sample Filtration
6.3.1 Add sample to be processed to the Ultrareservoir Container. If
diafiltration is to be performed, press lid firmly into place and refer to the
Diafiltration Procedure (section 6.5).
6.3.2 Position the 3-way Valve in the recirculation mode and open the Back
Pressure Valve.
6.3.3 Flip the forward/reverse switch into the "Forward" position and slowly
turn the speed dial clockwise to get the required recirculation rate.
(See Table 2)
6.3.4 Slowly turn the Back Pressure Valve toward the closed position until the
pressure gauge reads 20-35 psi. This will generate filtrate flow rate.
6.3.5 The sample in the reservoir will continue to decrease in volume equal to
the volume of filtrate generated. Continue operation until the desired
concentration factor is achieved. For example, 2,000 mL concentrated
to 200 mL is a 10X or ten-fold concentration.
6.3.6 Monitor pressure while maintaining a constant recirculation rate (speed
dial setting). The pressure may increase during concentration due to
viscosity. Adjust pressure if it is above or below 20-35 psi.
6.3.7 Sample has reached maximum volume reduction (final concentrate)
when air begins to be drawn into the pump. Stop filtration at this point.
9
6.4 Concentrate Recovery
6.4.1 When final concentration is attained, turn the pump speed dial setting to
"0" to stop recirculation.
6.4.2 Fully open the Back Pressure Valve and then position the 3-way Valve
to direct the retentate into a collection vessel.
6.4.3 Turn the pump on and adjust to a very low recirculation rate.
6.4.4 Collect the concentrated retentate that will exit the Sample Port.
6.4.5 Turn the speed dial setting back to "0", position the 3-way Valve to
recirculation mode, and begin recirculation at a very low recirculation
rate. The concentrate remaining in the filtration device will flow into the
reservoir.
6.4.6 Repeat steps (6.4.1 – 6.4.5) above for maximum concentrate recovery.
6.5 Diafiltration Procedure
For salt removal, buffer exchange, or macromolecular fractionation, use
diafiltration. See the Diafiltration and Buffer Exchange article referenced on
the Pall Corporation website for more information on this technique.
Figure 6
6.5.1 Gently press the lid onto the reservoir until it is firmly seated.
6.5.2 Cut a 12-20 inch piece of 3/16 inch I.D. tubing and connect to barb
connector located on top of lid. Secure tubing with clamp if necessary.
10
6.5.3 To initiate diafiltration during sample filtration, place end of tubing into
vessel containing either buffer for buffer exchange or water for salt
removal. Once a vacuum is created in the closed system, the solution
will begin moving up the tubing and into the reservoir. The rate the fluid
is drawn into the Ultrareservoir Container is the same as the rate the
filtrate is collected from the Ultrasette TFF Device.
NOTE: For best operation, the tubing end should rest at the bottom of the vessel. If
siphoning does not occur, gently press down on the lid to insure that system is
properly sealed.
6.5.4 The diafiltration technique can be interrupted or stopped by simply
removing the tubing from the diafiltraion fluid.
6.5.5 The sample will begin to concentrate once all the diafiltration volume
has been drawn into the reservoir.
7.0 Ultrareservoir Shutdown
7.1 Rinsing Procedure
To maximize recovery of sample concentrate, a rinsing cycle can be utilized.
7.1.1 Referencing Table 3 below, add appropriate volume of water or buffer
to reservoir.
NOTE: If sample contains buffer, then utilize buffer in the rinsing step to prevent possible
sample loss due to precipitation or denaturization.
Volume of Deionized Water/Buffer Required
Ultralab™ System Ultralab System Ultralab System
2L
5L
500 mL
Ultrasette™
40 mL
50 mL
70 mL
Lab
Tangential
Flow Device
Table 3
7.1.2 Fully open the Back Pressure Valve and position the 3-way Valve for
retentate collection (closed for recirculation mode).
7.1.3 Turn the pump on and adjust to a very low recirculation rate (speed dial
setting 1-3).
7.1.4 Collect the concentrate that will exit the Sample Port.
7.1.5 Turn the speed dial setting back to "0", position the 3-Way Valve in
recirculation mode, and return speed dial setting to 1-3. The
concentrate remaining in the filtration device will flow into the reservoir.
7.1.6 Repeat steps (7.1.2 – 7.1.5) above for maximum concentrate recovery.
11
7.2 Cleaning Procedure
7.2.1 Follow steps 6.2.1 – 6.2.10 in the Rinsing and Preconditioning
procedure (section 6.2) using one of the following cleaning agents in
place of DI (deionized) water or buffer:
Cleaning Agents
Cleaning Agent
Alconox® Powdered Precision Cleaner
Sodium Hydroxide
Tergazyme™ Enzyme-Active Powdered Detergent
Sodium hypochlorite
Concentration
1%
0.1N @ 25°C
1%
0.005%
Table 4
7.2.2 Repeat steps 6.2.1 – 6.2.10 in the Rinsing and Preconditioning
procedure using DI water to remove residual cleaning agents.
7.2.3 The anti-vortexing plugs may be removed for manual cleaning.
7.2.4 Follow manufacturer’s instructions for cleaning the filtration device.
7.3 Storage
After cleaning, the Ultrareservoir™ Container can be stored dry. If the filter
unit is attached, the system should be stored wet. If stored wet, use 0.1 N
Sodium Hydroxide (NaOH) solution as the storage agent.
Follow manufacturer’s instructions for filtration device storage.
7.4 Pump and Pump Tubing Care
7.4.1 Replace the pump tubing after cleaning or prior to initial operation.
7.4.2 Periodically, wipe off the pump and pump head with soap and water.
NOTE: Check pump tubing frequently for wear.
12
8.0
Ultrareservoir™ Container Chemical Compatibility
√ = Compatible
NR = Not Recommended
Reagent
Acetic Acid (5%)
Acetic Acid (25.5%)
Acetone (≤ 30%)
Acetonitrile (≤ 40%)
Alconox(1%)
Aliphatic and Aromatic Esters
Amines
Ammonium Chloride (1%)
Ammonium Hydroxide (5%)
Aromatic and Chlorinated Hydrocarbons
Butanol (70%)
Butyl Acetate (40%)
Butyl Cellosolve (10%)
Calcium Chloride (5%)
Chloroform (0.8%)
Citric Acid (1%)
Dimethylacetamide (DMAC) (≤ 40%)
Dimethylformamide (≤ 40%)
Dimethyl Sulfoxide (≤ 40%)
Disodium Salt of EDTA (10%)
Ethanol (70%)
Ethers
Ethyl Acetate (≤ 30%)
Formaldehyde (1%)
Formic Acid (5%)
Glutaraldehyde (0.5%)
Glycerin (50%)
Guanidine HCI (6M)
Hydrochloric Acid (0.1N @ 25° C)
Hydrochloric Acid (0.1N @ 50° C)
Hydrochloric Acid (1.0N @ 25° C)
Hydrogen Peroxide (1%)
Isopropyl Acetate (1%)
Isopropyl Alcohol (25%)
Ketone
Lactic Acid (5%)
Mercaptoethanol (0.1%)
Methyl Alcohol (25%)
Methylene Chloride (1%)
Methyl Ethyl Ketone(1%)
N-Methyl Pyrrolidone (1%)
Nitric Acid (£1%)
Oxalic Acid (1%)
Phenol (0.5%)
Phosphate Buffer (pH: 8.2) (1M)
Phosphoric Acid (1N)
Sodium Azide(1%)
Sodium Chloride (5%) (50° C)
Sodium Deoxycholate (5%)
Sodium Dodecyl Sulfate (0.01M)
Sodium Hydroxide (0.1 N @ 25° C)
Sodium Hydroxide (0.1 N @ 50° C)
Sodium Hydroxide (0.5N @ 25° C)
Sodium Hydroxide (1.0N @ 25° C)
Sodium Hypochlorite (0.005%)
Sodium Hypochlorite (0.02%)
Sodium Nitrate
Sulfuric Acid(1%)
TergaZyme™ (1%)
Tetrahydrofuran (5%)
Toluene (1%)
Tris® buffer (pH: 8.2)(1M)
Triton® X-100 (0.002M)
Urea (25%)
Ultrasil® 11 (1%)
Table 5
13
√
NR
NR
NR
√
NR
NR
√
√
NR
NR
NR
NR
√
NR
√
NR
NR
NR
√
√
NR
NR
√
√
√
√
√
√
NR
NR
√
√
√
NR
√
√
√
√
√
√
√
√
√
√
√
√
√
NR
√
√
NR
√
NR
√
NR
√
√
√
NR
√
√
√
√
√
9.0
Ultralab™ System Specifications
9.1 Ultrareservoir™ Container Specifications
Total Volume
Ultrareservoir Container
500 mL
500 mL
Ultrareservoir Container
2 mL
2,000 mL
Ultrareservoir Container
5L
5,000 mL
15-20 mL
20-30 mL
20-30 mL
< 2 mL
4.0 mm (5/32 in.)
< 2mL
6.4 mm (1/4 in.)
< 5 mL
6.4 mm (1/4 in.)
Minimum Recirculating
Volume
Hold-up Volume
Barb Connector Size
Materials
Sample Reservoir
Valves
Barb Connectors
Lid
O-ring (Lid)
Gauge
Dimensions
(Excluding Valves)
Weight
Acrylic
Polypropylene
Polypropylene
Polypropylene
EPR
Stainless Steel
12.7 x 12.7 x 19.1 cm
(5 x 5 x 7.5 in.)
0.9 kg (2 lb.)
Acrylic
Polypropylene
Polypropylene
Polypropylene
EPR
Stainless Steel
15.2 x 15.2 x 22.9 cm
(6 x 6 x 9 in.)
1.8 kg (4 Ib.)
Table 6
Acrylic
Polypropylene
Polypropylene
Polypropylene
EPR
Stainless Steel
20.3 x 20.3 x 27.9 cm
(8 x 8 x 11 in.)
3 kg (6.6 lb.)
9.2 Ultrapump™ II Specifications
Pump Drive
RPM Rating
Speed Control
Power (U.S.)
(Non-U.S.)
Enclosure
Dimensions (L x W x H)
Pump Head Housing
Pump Head Rotors
1/10 hp motor, permanent magnet, continuous
duty rated
6-600 RPM
0-10 dial control
115 volt (50/60 Hz)
230 volt (50/60 Hz)
ABS plastic case with polyester label. All
materials withstand standard cleaning solvents
29.2 x 20.3 x 18.4 cm (11.5 x 8 x 7.25 in.)
Polycarbonate
Stainless Steel
Table 7
9.3 Pump Tubing Specifications
Ultrasette™
Tubing Size
Inside diameter (nominal)
Hose barb size (nominal)
#24 Pharmed
6.4 mm (0.25 in.)
6.4 mm (1/4 in.)
Flow Rate Range
w/ 6 to 600 rpm drive (approximate)
17-1,700 mL/min
Maximum Pressure*
Continuous
Intermittent
pH Range
1.7 bar (25 psi)
2.7 bar (35 psi)
1-14
*Actual performance varies depending on tubing - values shown are for firm tubing.
Table 8
14
10.0
Appendix
10.1 Additional Literature
Please visit our website at www.Pall.com/lab for a complete listing of
available literature. You can find the following documents by searching on
the literature part number given below.
PN 33213 Introduction to Tangential Flow Filtration for Laboratory and
Process Applications
PN 33289 Scientific and Technical Report: Diafiltration: A Fast, Efficient
Method for Desalting, or Buffer Exchange of Biological Samples
-available online onlyPN 33366 Minimate™ Tangential Flow Filtration System and Minimate
Capsule
PN 33342 Increased Productivity Using Minimate Capsules to Replace
Stirred Cell Systems
PN 33339 The Partnership of Minimate TFF Capsule with Liquid
Chromatography Systems Facilitates Lab-scale Purifications
and Process Development Through In-line Monitoring
10.2 Ordering Information
Part No.
Description
Pkg
Ultralab Systems with 115 V pump
FS008X75 500 mL Ultralab System (consists of an Ultrareservoir
container, Masterflex* L/S* variable speed peristaltic pump,
Mini-Ultrasette accessory kit)
1/pkg
FS006X75 2 L Ultralab system (consists of an Ultrareservoir™ container,
Masterflex* L/S* variable speed peristaltic pump, and
Ultrasette™ accessory kit; connects to Ultrasette device sold
separately)
1/pkg
FS007X70 5 L Ultralab system (consists of an Ultrareservoir container,
MasterFlex L/S variable speed peristaltic pump, and Ultrasette
accessory kit; connects to Ultrasette device sold separately)
1/pkg
15
Ultralab Systems with 230 V Pump
FS018X75 500 mL Ultralab System (consists of an Ultrareservoir container,
Masterflex* L/S* variable speed peristaltic pump, Mini-Ultrasette 1/pkg
accessory kit)
FS016X75 2 L Ultralab system (consists of an Ultrareservoir container,
MasterFlex L/S variable speed peristaltic pump, and Ultrasette
accessory kit; connects to Ultrasette device sold separately)
1/pkg
FS017X70 5 L Ultralab system (consists of an Ultrareservoir container,
MasterFlex L/S variable speed peristaltic pump, and Ultrasette
accessory kit; connects to Ultrasette device sold separately)
1/pkg
Ultrareservoir Containers
FS005X75 2 L container (includes 0-4.2 bar pressure gauge, 4.0 mm
fittings, 6.4 mm fittings, and 3-way valve); suitable for use with
Ultrasette™ device
1/pkg
FS006X70 5 L container (includes 0-4.2 bar pressure gauge, 4.0 mm
fittings, 6.4 mm fittings, and 3-way valve); suitable for use with
Ultrasette device; fittings supplied are 6.4 mm
1/pkg
FS007X75 500 mL container (includes 0-4.2 bar pressure gauge, 4.0 mm
fittings, 6.4 mm fittings, and 3-way valve); suitable for use with
LV Centramate™ System
1/pkg
Ultrapump™ II
FS003X70 Ultrapump II with Quick Load* pump head, 115 volt
1/pkg
FS004X70 Ultrapump II with Quick Load* pump head, 230 volt
1/pkg
Accessory Kits
FS002X70 Ultrasette Kit: Contains 6 ft of 1/4" I.D. #24 PharMed*
feed/retentate tubing, 2 ft of 3/16" I.D. Tygon® filtrate tubing, (8) 1/pkg
tubing clamps, (1) screw clamp
FS001X75 Mini-Ultrasette Kit: Contains 6 ft PharMed* #15 tubing for
feed/retentate, 1.5 ft of 1/8" I.D. Tygon® filtrate tubing, (8) tubing 1/pkg
clamps, (2) 5/32" barb-to-luer fittings, (1) screw clamp
16
10.3 Warranty, Limitation of Liability and Remedies:
1. There is no warranty of merchantability or fitness for any particular purpose with respect to
any of the products, nor is there any other w arranty expressed or implied, except as provided
for herein.
2. For a period of 12 months from the date of delivery from Seller (the “Warranty Period”), Seller
warrants that products manufactured by Seller, when properly installed and maintained, and
operated at ratings, specifications, and design conditions, will be free from defects in material
and workmanship.
3. Seller’s liability under any warranty is limited solely (in Seller’s discretion) to replacing (F.O.B.
original ship point), repairing, or issuing credit for products which become defective during the
Warranty Period. Purchaser shall notify Seller promptly in writing of any claims and provide
Seller with an opportunity to inspect and test the product claimed to be defective. Buyer shall
provide Seller with a copy of the original invoice for the product, and prepay all freights charges
to return any products to Seller’s factory, or other facility designated by Seller. All claims must be
accompanied by full particulars, including system operating conditions, if applicable.
4. In no event shall Seller be liable for any product altered outside of the Seller’s factory by
someone other than Seller or for a product subjected to misuse, abuse, improper installation,
application, operation, maintenance or repair, alteration, accident or negligence in use, storage,
transportation, or handling.
5. In no event will Seller be liable for any damages, incidental, consequential or otherwise,
whether arising out of or in connection with the manufacture, packaging, delivery, storage, use,
misuse, or nonuse of any of its products or any other cause whatsoever.
PN 840012A
Pall,
, Centramate, Minimate, Mini-Ultrasette, Ultralab, Ultrapump II, Ultrareservoir, and Ultrasette are trademarks of
Pall Corporation. ® Indicates a trademark registration in the USA. Filtration. Separation. Solution is a service mark of Pall
Corporation.
© 2007, Pall Corporation, 08/07
Alconox and Terg-a-zyme are trademarks of Alconox, Inc.
Marprene II is a trademark of Watson Marlow.
Masterflex L/S is a trademark of Cole-Palmer Instrument Co.
PharMed and Tygon are trademarks of Norton Performance Plastic Corp.
Quick Load is a trademark of Cole-Parmer Instrument Co.
Teflon is a tradenmark of I.E. DuPont Co.
Tris and Triton X-100 are trademarks of Rohm & Haas, Inc.
Ultrasil is a trademark of Klenzade, A service of Ecolab.
17