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UNIT
–
I
ELECTRO CHEMISTRY

Introduction to electrochemistry

Types of conductors

Types of electrolytes

Cell terminology

Electrochemical cells (or) galvanic cells

Daniel cell

Representation of a galvanic cell

Reversible and irreversible cells

EMF of a cell

Measurement of emf of a cell

Single electrode potential(E)

Standard electrode potential(E0)

Nernst equation for electrode potential

Problems based on nernst equation

Reference electrodes(or) standard electrodes

Primary reference electrode o
Standard hydrogen electrode

Secondary reference electrode o
Standard calomel electrode

Types of electrodes

Glass electrode(internal reference electrode)

Determination of PH of a solution using glass electrode

Ion selective electrodes (ISE)

Describtion

Types of ion selective electrodes o
Glass membrane electrode o
Solid state membrane electrode o
Liquid membrane electrode o
Heterogenous membrane electrode o
Enzyme electrode

Determination of concentration of a metal ion using ISE

Application of ISE

Limitations

Electro chemical series

Definition

Significance(or) applications of electrochemical series

Potentiometer titrations

Redox titration

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
Conductometric titrations

Acid base titrations.
UNIT
–
II
CORROSION AND CORROSION CONTROL

Introduction to corrosion and its types

Chemical corrosion(dry corrosion) o
Pilling -Bedworth rule o
Mechanism of chemical corrosion o
Corrosion by oxygen o
Corrosion by hydrogen o
Liquid metal corrosion

Electro chemical corrosion (wet corrosion) o
Mechanism of electrochemical corrosion o
Evolution of hydrogen type o
Absorption of oxygen type o
Difference between chemical corrosion and electrochemical corrosion
 types of electrochemical corrosion
 galvanic corrosion
 differential aeration(or) concentration cell corrosion
 factors influencing the rate of corrosion
 nature of the metal
 nature of the environment
 corrosion control
 control of corrosion by modifying the metal
 by cathodic protection o sacrificial anodic protection method o impressed current cathodic protection method
 by modifying the environment
 corrosion inhibitors
 anodic inhibitors
 protective coatings
 types of protective coatings
 paints
 cathodic inhibitors
 vapour phase inhibitors
 constituents and their functions of a paint
 mechanism of drying of drying oil
 metallic coatings
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 electroless plating
 electro plating
 anodization
UNIT
–
III
FUELS AND COMBUSTION

Introduction, analysis of coal

The proximate analysis o
Determination of moisture in coal o
Determination of volatile matter in coal o
Determination of ash in coal o
Determination of fixed carbon

The ultimate analysis o
Determination of carbon and hydrogen in coal o
Determination of hydrogen o
Determination of nitrogen o
Determination of sulphur in coal o
Determination of oxygen in coal

Metallurgical coke

Characteristics of metallurgical coke

Manufacture of metallurgical coke by Otto Hoffmann
’ s

Petroleum of gasoline method

Processing and fractions

Cracking
–
catalytic cracking

Knocking

Octane number

Cetane number

Synthetic petrol

Bergius process (hydrogenation of coal)

Fisher- Tropsch process

Gaseous fuels

Water gas

Producer gas

Compressed natural gas ( CNG)

Liquefied petroleum gas (LPG)

Biogas

Calorific value

Units of calorific value

Determination of calorific value

Gross calorific value and net calorific value

Theoretical calculations of calorific values

Flue gas analysis: Orsat
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UNIT
–
IV
PHASE RULE AND ALLOYS

Introduction, explanation of terms involved

Phase

Component

Degree of freedom

Phase diagram

Phase rule

One component system

Water system

Condensed phase rule

Two component system

Simple eutectic systems (Binary alloys)

Lead
–
silver system

Construction phase diagram by thermal analysis

Copper
–
nickel alloy system

Alloys

Purpose of making alloys

Classification of alloys

Ferrous alloys

Nichrome

Stainless steel

Non ferrous alloys

Brass

Bronze

Heat treatment of steel

Hardening (quenching)

Tempering

Annealing
UNIT
–
V
ANALYTICAL TECHNIQUES

Explanation of terms used in absorption spectra

Beer
’ s
–
lamberts law

Problems

UV and visible spectroscopy

Principle

Instrumentation (block diagram only)

Problems

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
Principles

Instrumentation (block diagram only)

Problems

Colorimetric estimation of few metal ions

Flame photometry

Estimation of iron

Principle

Instrumentation (block diagram only)

Estimation sodium by flame photometry

Atomic absorption spectroscopy

Principle

Instrumentation (block diagram only)

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