MDMA purity Laboratory Test results

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MDMA PURITY LABORATORY
TEST RESULTS
A laboratory analysis of the MDMA Purity test.
M.M.C. INTERNATIONAL B.V.
Frankenthalerstraat 16-18 4816 KA Breda The Netherlands
Phone: +31-765711140
Fax: +31-76-5719300
Email: lab@mmcinter.com
www.narcotictests.com
Introduction
We at M.M.C. International are producers of presumptive colorimetric ampoule tests for the police
and customs officers. These tests give a presumptive identification of a suspected substance. These
tests in no way substitute the need for further confirmation by for example GC-MS analysis. Always
have your sample confirmed by a laboratory. In order to give you, the customer, the best
identification possible we do tests at our laboratory to ensure the quality of our products and to
expose possible cross reactions with our tests. In this report we tested our MDMA purity test.
Chemicals Used
In this test we used the following chemicals:
Chemical
Aplha-D(+)-Glucose
Aspirin
Benzocaine
Boric acid
Caffeine
Creatine
D(+)-Sacharose
D-Mannitol
D-Sorbitol
Ibuprofen
Lactose monohydrate
Levamisole
Lidocaine
Magnesium sulphate
Paracetamol
Phenacitin
Procaine
Vitamine C
Manufacturer
Across Organics
Sigma-Aldrich
Sigma-Aldrich
Carl-Roth
Carl-Roth
Sigma-Aldrich
Carl-Roth
Sigma-Aldrich
Carl-Roth
Sigma-Aldrich
Carl-Roth
Across Organics
Sigma-Aldrich
Carl-Roth
Sigma-Aldrich
Sigma-Aldrich
Sigma-Aldrich
Carl-Roth
Purity
99,0%
99,9%
99,9%
99,9%
99,9%
99,9%
99,7%
98,5%
99,7%
98,3%
99,5%
99,9%
99,9%
99,7%
99,8%
99,9%
97,0%
99,5%
MDMA
Duchefa Farma B.V. 99,5%
Street Samples:
Chemical
BZP+TMFPP
mCPP
MDA
Methylone
PMMA
Amphetamine
Methamphetamine
Analysis results:
Identity confirmed by GC-MS
Identity confirmed by GC-MS
Identity confirmed by GC-MS
Identity confirmed by GC-MS
Identity confirmed by GC-MS
Identity confirmed by GC-MS
Identity confirmed by GC-MS
M.M.C. International B.V.
Laboratory and Production Manager Benji Voesenek
Phone number: +31-76-5711140
Page 1 of 6
Equipment Used
In our analysis we used a Kern ABS 120-4 analytical balance to weigh the chemicals.
Furthermore we used our GC-MS to confirm the identity of the street samples we used to test the
MDMA purity for cross reactions. Below are the specifications of the GC-MS instrument we used.
The GC was an Agilent Technologies 7820A Gas Chromatograph (GC) with 5975 Mass Selective
Detector (MSD). The system uses a split/split less inlet with an HP5-MS column.
Besides the chemicals and electronic equipment we used regular laboratory supplies and our MDMA
purity test.
Semi-Quantitative Analysis
First, the pure MDMA was cut with Caffeine in 6 different ratios:
Percentage of MDMA
0% (Blanc)
10%
25%
50%
75%
100%
Amount of Caffeine
20mg
18mg
15mg
10mg
5mg
0mg
Amount of MDMA
0mg
2mg
5mg
10mg
15mg
20mg
The weight samples were added to the ampoules and the following results were obtained:
From left to right the amount of MDMA increases, this picture is taken after 60 minutes. The
toplayer can be read at 5, 15, 30 and 60 minutes. The longer it stands the clearer the color
differences in color (and concentration) can be determined.
M.M.C. International B.V.
Laboratory and Production Manager Benji Voesenek
Phone number: +31-76-5711140
Page 2 of 6
The chart we made according to the test done with different ratios of MDMA and Caffeine. There
are 4 charts made at 5, 15, 30 and 60 minutes. The top left one is after 5 minutes, the top right one
after 15 minutes, the bottom left one after 30 minutes and the bottom right after 60 minutes.
In the following chapter we will test the cross reactivity of the MDMA Purity test with several other
substances
M.M.C. International B.V.
Laboratory and Production Manager Benji Voesenek
Phone number: +31-76-5711140
Page 3 of 6
Cross-Reactivity
In the following pictures and tables the cross reactivity of the MDMA Purity test is demonstrated.
From left to right:
Number
1
2
3
4
5
6
7
8
9
10
11
Substance
Aplha-D(+)-Glucose
Aspirin
Benzocaine
Reaction
None
None
Very light yellow color
of the bottom layer.
Boric acid
None
Caffeine
None
Creatine
None
D(+)-Sacharose
None
D-Mannitol
None
D-Sorbitol
None
Ibuprofen
None
Lactose monohydrate
None
M.M.C. International B.V.
Laboratory and Production Manager Benji Voesenek
Phone number: +31-76-5711140
Page 4 of 6
From left to right:
Number
12
13
14
15
16
17
18
Substance
Levamisole
Lidocaine
Magnesium sulphate
Paracetamol
Phenacitin
Procaine
Vitamine C
M.M.C. International B.V.
Laboratory and Production Manager Benji Voesenek
Phone number: +31-76-5711140
Reaction
None
None
None
Yellow top and bottom layer
Yellow top and bottom layer
None
None
Page 5 of 6
From left to right:
Number
19
Substance
BZP+TMFPP
20
mCPP
21
22
23
24
25
MDA
Methylone
PMMA
Amphetamine
Methamphetamine
Reaction
Bright yellow top layer, gives residue on the sides of the
ampoule in between the two layers. (MDMA does not
give this residue.)
Bright yellow-orange top layer, gives residue on the
sides of the ampoule in between the two layers. (MDMA
does not give this residue.)
Same reaction as MDMA because it is so similar
None
None
None
None
Conclusion:
The MDMA Purity test allows you to test the purity of MDMA and also allows you to detect some of
the cutting agents by looking at the bottom layer of the test and possible residue occurring at the
sides of the ampoule. Unfortunately if one of those reactions is observed the purity of the MDMA
cannot be determined because these substances interfere with the colour produced by MDMA, but
this only occurs in a few cases. This test is designed to be used alongside the MMC Crystal Meth/XTC
(MDMA) test. If this test is positive for MDMA it is possible to determine the purity with this new
MDMA purity test.
We want to thank the local police for lending us the samples for doing the tests with street samples.
M.M.C. International B.V.
Laboratory and Production Manager Benji Voesenek
Phone number: +31-76-5711140
Page 6 of 6
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