SSME experimental and safety setup: XRD D8 Bruker
Experiment explanation
: Phase analysis CaMnO3
Chemicals used inside D8
cabinet prep. table #1
Chemicals needed for
cleaning #1
Hazard statements
(H-Codes from MSDS)
(Or R-Phrases)
: CaMnO3 and possible starting materials CaCO3 and MnO3
Precautionary statements
(P-Codes from MSDS)
(or S-Phrases)
Personal and others
protection
Disposal and cleaning
Standard setup
Furnace
: Ethanol
: CaCO3:
R 37/38: Irritating to respiratory system and skin
R 41: Risk of serious damage to eyes
MnO2:
R 20/22: Harmful by inhalation and if swallowed
CaMnO3: not know
Ethanol:
H225: Highly Flammable liquid and vapour
: CaCO3:
S 26: In case of contact with eyes, rinse immediately with plenty of
water and seek medical advice
S 36/37/39: Wear suitable protective clothing, gloves and eye/face
protection
MnO2:
S 25: Avoid contact with eyes
CaMnO3: not know
Ethanol:
P210: Keep away from heat/sparks/open flames/hot surfaces.
: Gloves, lab coat, mask and eye protection for treating
powders clean spills immediately to protect coworkers from
inhaling the nanoparticles
: Dispose all disposables and paper contaminated with
powders (nanoparticles) in the white waste bin on the
preparation table
Clean the sample holder with paper and ethanol and
dispose in the white waste bin.
: Standard setup
Start and end of experiment
Time per experiment #2
Precaution for out of
working hours
: 15th of september
20th of september
: 2 hours in the morning from 09:00 till 11:00 for all days
: No need all lab work is done within 09:00 and 11:00
Signatures
: Experimentalist:
Daily supervisor:
Amico:
#1 Be aware that use of chemicals or equipment not mentioned here has to be reported to Jacob and
will delay your experiment
#2 Be sure you reserve the equipment beforehand