Microstructurally-driven investigation of twinning & strain localization

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INTRODUCTION

The current automotive industry demand typically targets both weight reduction and fuel economy. To achieve this, while maintaining designability as well as an extended product life cycle, alloying of metals becomes the solution. With efforts of reducing our dependency to hydrocarbon reserves, inevitable weight reduction in the transportation industry is transforming from a need to an urge.

Magnesium is one of the most important metals commercially, since its properties make it easy to weld, forge, cast or machine. Mg alloys have most of the requirements to revolutionize the transportation industry. To this end, understanding of the events listed below is necessary to improve mechanical deformation behaviors.

Door inner:

Mg = 5.4 kg

Engine:

Mg = 15 kg

Al = 22 kg

Steel = 60 kg

Al = 8.2 kg

Wt. Reduction = 33%

Wt. Reduction = 22 to 70%

Steering wheel core:

Mg = 0.9 kg

Steel = 1.4 kg

Wt. Reduction = 33%

Steering column:

Mg = 1.4 kg

Steel = 23 kg

Wt. Reduction = 40%

Microstructurally-driven investigation of twinning & strain localization in magnesium alloys via in-situ testing

Department of Mechanical Engineering & Mechanics, Drexel University College of Engineering

M. Cabal, B. Wisner, K. Baxevanakis, A. Kontsos

MATERIALS & METHODS

Rolled magnesium alloy (Mg–3% Al–1% Zn) known commonly as AZ31 was used to produce test samples machined with a Wire EDM.

Specimens were mechanically ground using 800, 1200, and 2400 SiC papers, followed by a detailed TAMG Mg - polishing procedure.

EBSD data was collected using a Scanning Electron Microscope (SEM FEI XL30) controlled by TSL software. a) b)

Lift gate:

Mg = 3.2 kg

Al = 5.5 kg

Wt. Reduction = 42%

Figure 3.

Compression schematics for the thermomechanical process to develop textures a) b)

Figure 4.

EBSD map of tensile samples. a) ND and b) RD loading directions

Theoretical & Applied Mechanics Group

CONCLUSIONS

Shear band formation at very early stage of plastic deformation

(~0.4% strain) is tightly associated with twinning.

Noticeable differences on the plastic flow were identified through DIC in both textures.

Induced notched geometry affects the s-type behavior in the stress vs. strain curve.

Average

ε

yy strain inside the shear band region exponentially grows up to 2.75x the average strain acquired through the sample. It is then followed by a slow decay..

The results presented can be used to control/optimize the microstructure in Mg alloys, opening a way for tailoring their mechanical behavior needed for commercialization.

In-situ acoustic emission (AE) monitoring, not shown here, was also performed during tensile loading to investigate the characteristics of twin nucleation.

Transfer case:

Mg = 11.4 kg

Steel = 15.6 kg

Wt. Reduction = 28%

Instrument panel:

Mg = 1.8 kg

Steel = 5 kg

Wt. Reduction = 64%

Car seat frame:

Mg = 1.8 kg

Steel = 5 kg

Wt. Reduction = 64%

Figure 1.

Advantages gained through weight reduction achieved with the use of Mg alloys [1]

Despite frequent observations of shear banding, the formation of shear bands, their development, and overall contribution to rolling and recrystallization textures is still not understood from both material and mechanics perspectives.

OBJECTIVE

The objective of this research is to consistently monitor, using several techniques, and quantify the microscopic features during mechanical loading, to obtain critical relationships between microstructural changes and local/global strain distributions of a Mg alloy.

Quantify the effect of texture and twinning in shear band nucleation, development, and eventual damage initiation in

Mg alloys.

ND

Roller

Sheet

Roller

= Small deformation resistance plane

Sheet

RD

= Large deformation resistance plane

Figure 2.

Crystallographic orientation of rolled

AZ31 Magnesium Alloy

Grain Size (diameter)

Grain Size (diameter)

18

10

9

8

12

11

7

6

5

16

14

12

10

8

4

3

6

4

2

2

1

0

0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200

0

0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200

Grain Size (Diameter) [microns] Grain Size (Diameter) [microns]

Figure 5.

Grain size (diameter) and Pole Figures for a) ND and b) RD samples

Figure 6.

Sample geometry for controlled strain localization testing

(units: mm)

RESULTS

Digital Image Correlation (DIC) was used to acquire in-situ full field deformation measurements for both textures as seen in Figure 10.

Average longitudinal strain was measured inside the shear band region and compared to the average longitudinal strain for the complete field of view. Vic-3D line scans are also evidence of a rapid strain localization in the ND texture. a)

1 2 a) 1 2 3 b) 1 2 b)

1 2 3

Figure 7.

Preliminary work linking strain localization and twins [2]

Figure 8.

ABAQUS Preliminary FEA results for a) ND and b) RD specimens a)

Figure 9.

DIC segments of a) ND and b) RD specimens b)

Figure 10.

Vic-3D

ε

yy line scan around shear band region

Figure 11.

Average

ε

yy in both shear band and full field of view for a) ND and b) RD specimens

REFERENCES & ACKNOWLEDGEMENTS

1. M.K. Kulekci; Magnesium and its alloys applications in automotive industry. Int. J. Adv. Manuf. Technol. 39 (2008) 851-865.

2. K. Hazeli, J. Cuadra, P.A. Vanniamparambil, A. Kontsos; In situ identification of twin-related bands near yielding in a magnesium alloy. Scripta Mater. 68 (2013), 83-86

This work couldn’t be possible without the continuous help from:

Jacob Hochhalter – NASA Langley Research Center

LSAMP – BTD (Bridge to Doctorate) Fellowship

FUTURE WORK

Collaboration with for improved insitu surface morphology and topology measurements.

In-situ mechanical testing using a loading stage inside a SEM

Provide experimental data to build a mathematical model that will serve as an input into Finite Element Codes ie. ABAQUS.

Develop/use/implement a constitutive model for shear band formation into Crystal Plasticity Finite Element Methods

(CPFEM)

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